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Molbank 2009, 2009(4), M638; doi:10.3390/M638
Short Note

6-(4-(2-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-10-oxa-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione)

Small Molecule Synthesis Facility, Duke University, Durham, NC 27708, USA
Received: 9 October 2009 / Accepted: 2 November 2009 / Published: 5 November 2009
Download PDF [147 KB, uploaded 5 November 2009]

Abstract

Microwave irradiation of maleimide with an excess of furan in water exclusively yields the corresponding exo-cycloadduct in good yield (87%) in 1 hour at 90 oC. Alkylation of the imido nitrogen with tetraethylene glycol under Mitsunobu conditions gives the ROMP monomer in 81% yield.
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MDPI and ACS Style

Gooden, D.M. 6-(4-(2-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-10-oxa-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione). Molbank 2009, 2009, M638.

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