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Molbank 2008, 2008(3), M577; doi:10.3390/M577

One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole

1
Chemistry Department, Science Faculty, Arak Islamic Azad University, P. O. Box 38135-567, Arak, Iran
2
Young Club Researchers of Arak, Islamic Azad University, P.O. Box 38135-567, Arak, Iran
*
Author to whom correspondence should be addressed.
Received: 28 July 2008 / Accepted: 1 September 2008 / Published: 4 September 2008
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Abstract

In this study, a fast and good yield one-pot microwave-assisted synthesis (45 seconds) of 1H-phenanthro[9,10-d][1,2,3]triazole by a 1,3-dipolar cycloaddition reaction of sodium azide and 9-bromophenanthrene in the presence of potassium tert-butoxide in DMSO as solvent is reported.
Keywords: Microwave assisted synthesis; 1; 3-Dipolar cycloadditions; Benzyne intermediate; 1H-Phenanthro[9; 10-d][1; 2; 3]triazole; 1; 2; 3-Triazoles Microwave assisted synthesis; 1; 3-Dipolar cycloadditions; Benzyne intermediate; 1H-Phenanthro[9; 10-d][1; 2; 3]triazole; 1; 2; 3-Triazoles
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Taherpour, A.A.; Faraji, M. One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole. Molbank 2008, 2008, M577.

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