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Molbank 2008, 2008(2), M569; doi:10.3390/M569
Short Note

Synthesis of 4,4'-(Cyclohexane-1,1-diyl)bis(1-methyl- 1H-pyrazol-5-ol)

*  and
Received: 1 July 2008; Accepted: 19 August 2008 / Published: 22 August 2008
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Abstract: Methyl (2E)-3-methoxyacrylate and excess methylhydrazine yield crude 1- methyl-2-pyrazolin-5-one which is reacted with cyclohexanone to obtain the title compound in 86% yield. Detailed spectroscopic data (1H NMR, 13C NMR, 15N NMR, and MS) are presented.
Keywords: Pyrazolones; cyclohexanone adduct; NMR spectroscopy Pyrazolones; cyclohexanone adduct; NMR spectroscopy
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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MDPI and ACS Style

Eller, G.A.; Holzer, W. Synthesis of 4,4'-(Cyclohexane-1,1-diyl)bis(1-methyl- 1H-pyrazol-5-ol). Molbank 2008, 2008, M569.

AMA Style

Eller GA, Holzer W. Synthesis of 4,4'-(Cyclohexane-1,1-diyl)bis(1-methyl- 1H-pyrazol-5-ol). Molbank. 2008; 2008(2):M569.

Chicago/Turabian Style

Eller, Gernot A.; Holzer, Wolfgang. 2008. "Synthesis of 4,4'-(Cyclohexane-1,1-diyl)bis(1-methyl- 1H-pyrazol-5-ol)." Molbank 2008, no. 2: M569.


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