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Molbank, Volume 2008, Issue 1 (March 2008)

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Open AccessShort Note Microwave Synthesis of (4-hydroxy Phenyl) 3-oxo butanoate
Molbank 2008, 2008(1), M561; doi:10.3390/M561
Received: 2 May 2007 / Revised: 20 November 2007 / Accepted: 15 January 2008 / Published: 25 March 2008
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Abstract
The product 3 was previously prepared [1] using C6H6 in the presence of pyridine. A mixture of hydroquinone 1 (0.66 g, 6 mmol), ethyl acetoacetate 2 (0.78 g, 6 mmol) and monmorillonite K10 (0.43 g, 30 % by weight of
[...] Read more.
The product 3 was previously prepared [1] using C6H6 in the presence of pyridine. A mixture of hydroquinone 1 (0.66 g, 6 mmol), ethyl acetoacetate 2 (0.78 g, 6 mmol) and monmorillonite K10 (0.43 g, 30 % by weight of the total reactants) [2,3] was placed in a pyrex tube which was then introduced into a Maxidigest MX 350 Prolabo microwave monomode reactor fitted with a rotational system [4]. Full article
Open AccessShort Note Oxygen-Containing 10-, 15-, and 20-Membered Macrocyclic Cobalt Complexes from Co2(CO)6-Bispropargylic Alcohol
Molbank 2008, 2008(1), M562; doi:10.3390/M562
Received: 6 November 2007 / Revised: 22 January 2007 / Accepted: 23 January 2008 / Published: 25 March 2008
Cited by 4 | PDF Full-text (127 KB) | HTML Full-text | XML Full-text | Supplementary Files
Abstract
Novel 10-, 15-, and 20-membered oxygen-containing macrocyclic cobalt complexes (3, 4, and 5 respectively) were obtained in moderate combined yield via double nucleophilic substitution of the hexacarbonyldicobalt-coordinated monoyne diol [{Co2(CO)6(μ-η2-HOCH2C≡CCH2OH)}] (1) upon BF
[...] Read more.
Novel 10-, 15-, and 20-membered oxygen-containing macrocyclic cobalt complexes (3, 4, and 5 respectively) were obtained in moderate combined yield via double nucleophilic substitution of the hexacarbonyldicobalt-coordinated monoyne diol [{Co2(CO)6(μ-η2-HOCH2C≡CCH2OH)}] (1) upon BF3·OEt2 treatment in the presence of (Z)-2-butene-1,4-diol (2) at room temperature. The products distribution was found to be highly concentration dependent. Full article
Open AccessShort Note Synthesis of 3,5-di-(4-pyridyl)-1H-1,2,4-triazole
Molbank 2008, 2008(1), M563; doi:10.3390/M563
Received: 3 August 2007 / Revised: 2 October 2007 / Published: 25 March 2008
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Open AccessShort Note New Route to Metformin Hydrochloride (N,N-dimethylimidodicarbonimidic diamide hydrochloride) Synthesis
Molbank 2008, 2008(1), M564; doi:10.3390/M564
Received: 27 August 2007 / Revised: 16 January 2008 / Accepted: 23 January 2008 / Published: 25 February 2008
Cited by 2 | PDF Full-text (101 KB) | HTML Full-text | XML Full-text | Supplementary Files
Abstract
In this work, microwave (MW) assisted synthesis of metformin hydrochloride was performed on thin layer chromatography (TLC) plates. This versatile, simple and economical green methodology is readily amendable to parallel synthesis of metformin hydrochloride libraries. Full article
Open AccessShort Note Synthesis of New β-enaminones of Isoquinolines with 5,5-dimethyl-cyclohexanedione
Molbank 2008, 2008(1), M565; doi:10.3390/M565
Received: 3 August 2007 / Accepted: 23 January 2008 / Published: 25 March 2008
Cited by 2 | PDF Full-text (97 KB) | HTML Full-text | XML Full-text | Supplementary Files

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