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Keywords = softened welded joints

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17 pages, 7855 KB  
Article
Microstructural Evaluation and Tensile Properties for GTAW Weldments of Stainless Steel 304 Seam Pipes
by Eunhye Park and Byounglok Jang
Metals 2026, 16(6), 565; https://doi.org/10.3390/met16060565 - 22 May 2026
Abstract
This study examines the microstructural characteristics and tensile properties of autogenous orbital gas tungsten arc (GTA) circumferential butt welds produced on commercially rolled 304 stainless steel seam pipes (outer diameter 38.1 mm, wall thickness 2.0 mm) for high-purity fluid distribution systems. A three-segment [...] Read more.
This study examines the microstructural characteristics and tensile properties of autogenous orbital gas tungsten arc (GTA) circumferential butt welds produced on commercially rolled 304 stainless steel seam pipes (outer diameter 38.1 mm, wall thickness 2.0 mm) for high-purity fluid distribution systems. A three-segment current profile was employed using an AMI 8-4000 orbital system, with peak currents of 70, 67, and 65 A for the penetration, remelting, and downslope (crater-fill) segments, respectively, under high-purity Ar (99.999%) shielding with back purging. Electron backscatter diffraction (EBSD) analysis, including image quality (IQ), inverse pole figure (IPF), and kernel average misorientation (KAM) mapping, showed that the weld metal consists of epitaxially grown columnar austenite grains strongly oriented along the solidification direction, whereas the heat-affected zone (HAZ) exhibits finer equiaxed grains with an increased Σ3 twin boundary fraction and elevated low-angle boundary fraction, indicative of partial recrystallization. Only sparse, discontinuous δ-ferrite stringers were detected in the fusion zone, and no non-metallic inclusions were observed on fracture surfaces, supporting the weld metal’s suitability for semiconductor-grade cleanliness. Vickers microhardness profiles revealed modest hardness differences (typically within 10–20 HV) between the weld metal, HAZ, and base metal, with no pronounced HAZ softening. Cross-weld tensile tests conducted in accordance with ASTM E8/E8M-22 yielded yield strengths above 200 MPa, ultimate tensile strengths of 650–680 MPa, and total elongations approaching 40%, comparable to the as-received pipe. Scanning electron fractography confirmed fully ductile failure via microvoid coalescence without evidence of cleavage, intergranular decohesion, or weld-defect-induced embrittlement. Collectively, these results demonstrate that the three-segment autogenous orbital GTAW procedure produces structurally sound, particle-clean joints suitable for 304 stainless steel seam pipes used in high-purity industrial piping. Full article
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22 pages, 35997 KB  
Article
Process Parameters Optimization of Rotary Friction Welding of Silicon Bronze CuSi3Fe2Zn3 Alloy Using Response Surface Methodology
by Henrique Pereira Machado, Francisco Yastami Nakamoto, Givanildo Alves dos Santos, Gilmar Ferreira Batalha, Vinicius Torres do Santos, Marcio Rodrigues da Silva and Flávia Gonçalves Lobo
Materials 2026, 19(9), 1877; https://doi.org/10.3390/ma19091877 - 2 May 2026
Viewed by 301
Abstract
This study investigates the optimization of selected process parameters in the rotary friction welding (RFW) process of CuSi3Fe2Zn3 silicon bronze alloys using Response Surface Methodology (RSM) with tensile strength as the primary response. The effects of rotation speed, [...] Read more.
This study investigates the optimization of selected process parameters in the rotary friction welding (RFW) process of CuSi3Fe2Zn3 silicon bronze alloys using Response Surface Methodology (RSM) with tensile strength as the primary response. The effects of rotation speed, friction time and friction pressure were evaluated, and the steepest ascent method was applied to determine the best parameters. The results indicated that rotation speed and friction time were the most influential parameters for enhancing tensile strength. A maximum tensile of 424 MPa was achieved under conditions of 3300 rpm, friction time of 25 s, friction pressure of 0.5 MPa, forging time of 16 s, and forging pressure of 8 MPa. However, confirmation experiments exhibited noticeable variability, indicating limitations in process repeatability. Tensile properties, hardness evaluation, microstructural characterization, and thermographic analysis were conducted to assess the quality of the welded joints. Microstructural analysis revealed recrystallized equiaxed grains in the welding center zone, consistent with severe plastic deformation, while microcracks and microvoids were observed and likely contributed for failure during tensile testing. Despite grain refinement, a reduction in microhardness was detected, suggesting the influence of thermal softening mechanisms. Thermographic analysis indicated that the average temperature at the welding center zone reached 564 °C. In conclusion, RSM proved to be a useful tool for identifying trends and guiding process optimization. The results highlight the importance of process stability and control in achieving consistent performance in RFW of copper-based alloys. Full article
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24 pages, 11341 KB  
Article
An RSM-Based Investigation on the Process–Performance Correlation and Microstructural Evolution of Friction Stir Welded 7055 Al/2195 Al-Li Dissimilar T-Joints
by Binbin Lin, Yanjie Han, Duquan Zuo, Nannan Wang, Yuanxiu Zhang, Haoran Fu and Chong Gao
Materials 2026, 19(6), 1260; https://doi.org/10.3390/ma19061260 - 23 Mar 2026
Viewed by 452
Abstract
Friction stir welding (FSW) is a key technology for manufacturing T-shaped thin-walled structures and avoiding fusion welding defects. However, the quantitative relationship between its process parameters and the microstructure properties of the joint remains unclear. To address this, this study established regression models [...] Read more.
Friction stir welding (FSW) is a key technology for manufacturing T-shaped thin-walled structures and avoiding fusion welding defects. However, the quantitative relationship between its process parameters and the microstructure properties of the joint remains unclear. To address this, this study established regression models via response surface methodology (RSM) relating rotational speed (w), welding speed (v), and plunge depth (h) to the mechanical properties of T-joints. The optimal process parameters (400 rpm, 60 mm/min, 0.21 mm) were determined, under which the ultimate tensile strength (UTS) and weld nugget hardness (WNH) of the joint reached 74.1% (377 MPa) and 94.4% (153 Hv) of the base materials (BM) respectively, with v showing the most significant influence on joint mechanical properties. Microstructural observations revealed that from the BM to the stirring zone (SZ), the grains underwent a continuous evolution from coarsening, partial recrystallization to complete dynamic recrystallization (DRX). In the SZ, due to severe plastic deformation and high heat input, the continuous dynamic recrystallization (CDRX) was the dominant mechanism, and the grain was significantly refined. The heat input in the thermomechanical affected zone (TMAZ) is relatively low, mainly geometric dynamic recrystallization (GDRX). DRX-driven grain refinement was the primary strengthening factor in the joint, with hardness closely related to grain size. However, thermal cycling induced softening in the heat-affected zone (HAZ) and promoted the precipitation of brittle compounds such as Al3Mg2 and MgZn2, which caused crack initiation exhibiting intergranular brittle fracture. Subsequently, under stress drive, it extends to SZ, mainly characterized by ductile fracture. Full article
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18 pages, 7082 KB  
Article
Microstructure and Mechanical Properties of Al-Mg-Zn-Er-Zr Alloy via Multi-Pass Metal Inert Gas (MIG) Welding
by Haoran Che, Wu Wei, Feiran Zhang, Jieming Gao, Li Cui, Ying Han, Ting Li, Hui Huang, Shengping Wen, Wei Shi and Zuoren Nie
Metals 2026, 16(3), 286; https://doi.org/10.3390/met16030286 - 3 Mar 2026
Viewed by 535
Abstract
The microstructure and mechanical properties of the joint of a novel Al-Mg-Zn-Er-Zr alloy fabricated by multi-pass MIG welding using ER5E61 filler wire were investigated first. The results show that multi-pass MIG welding induces heterogeneous grains in the weld metal: equiaxed grains, columnar grains, [...] Read more.
The microstructure and mechanical properties of the joint of a novel Al-Mg-Zn-Er-Zr alloy fabricated by multi-pass MIG welding using ER5E61 filler wire were investigated first. The results show that multi-pass MIG welding induces heterogeneous grains in the weld metal: equiaxed grains, columnar grains, and cover-pass feather-like grains. The weld metal exhibits coarse grains (45.81 ± 19.68 μm), a high proportion of high-angle grain boundaries (83.3%), and a low dislocation density compared with the base metal. The joint achieves 316 MPa ultimate tensile strength, 10.5% elongation, and 0.80 joint efficiency with minimum hardness (77.2 HV) in the weld metal. Strengthening mechanism analysis reveals that joint softening mainly stems from the disappearance of deformed structure, reduced dislocation density, and the coarsening and reduction in Al3(Er, Zr) nanophases. Diffuse precipitation of the Al3(Er, Zr) nanophases (19.61 nm, 0.53%) under multi-pass MIG welding compensates for the softening of the welded joint, leading to the retention of high tensile strength despite marked hardness loss, thus demonstrating effective strength preservation. Full article
(This article belongs to the Special Issue Advances in Welding of Metallic Materials)
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25 pages, 54359 KB  
Article
Optimizing Mechanical Structures Through Butt Joining of Dissimilar Materials for Lightweight Components
by Jarosław Szusta, Łukasz Derpeński, Özler Karakaş and Nail Tüzün
Materials 2026, 19(1), 18; https://doi.org/10.3390/ma19010018 - 20 Dec 2025
Viewed by 827
Abstract
The joining of dissimilar steels is crucial for designing lightweight, high-performance structures but poses significant challenges due to uneven material properties. This study optimizes the butt-welding process for a dissimilar pair of S355J2 and Strenx 700E steels. Cold Metal Transfer welding was employed, [...] Read more.
The joining of dissimilar steels is crucial for designing lightweight, high-performance structures but poses significant challenges due to uneven material properties. This study optimizes the butt-welding process for a dissimilar pair of S355J2 and Strenx 700E steels. Cold Metal Transfer welding was employed, and the effects of surface preparation, linear energy, and joint gap on joint integrity were systematically investigated via tensile testing, digital image correlation, fractography, and microhardness analysis. The results demonstrate that mechanical surface cleaning combined with a low linear energy of 0.334 kJ/mm and a 0.5 mm gap yields optimal performance. This parameter set produced a joint with a tensile strength of 616 MPa, representing a 32% increase compared to uncleaned samples, and promoted uniform plastic deformation across the joint. Microstructural analysis confirmed a narrower heat-affected zone and the absence of significant softening in the high-strength steel. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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22 pages, 12895 KB  
Article
The Role of Rotational Tool Speed in the Joint Performance of AA2024-T4 Friction Stir Spot Welds at a Short 3-Second Dwell Time
by Yousef G. Y. Elshaghoul, Mahmoud F. Y. Shalaby, Mohamed M. El-Sayed Seleman, Ahmed Elkelity, Hagar A. Reyad and Sabbah Ataya
Crystals 2025, 15(12), 1054; https://doi.org/10.3390/cryst15121054 - 12 Dec 2025
Cited by 3 | Viewed by 676
Abstract
This study explores Friction Stir Spot Welding (FSSW), a well-established solid-state joining technique, for high-strength aluminum alloys like AA2024-T4, which present significant challenges for conventional welding techniques. This research focuses on the impact of relatively low rotational speeds, specifically within a range of [...] Read more.
This study explores Friction Stir Spot Welding (FSSW), a well-established solid-state joining technique, for high-strength aluminum alloys like AA2024-T4, which present significant challenges for conventional welding techniques. This research focuses on the impact of relatively low rotational speeds, specifically within a range of 700 to 1300 rpm, on the mechanical and microstructural properties of the welded joints. By employing a short dwell time of 3 s, this study aims to enhance productivity in the automotive and aerospace industries. The experimental work evaluated the joints’ thermal cycles, macrostructure, microstructure, hardness and load-carrying capacity. Results indicated a linear relationship between rotational speed and heat input. Although all welds exhibited a significant grain size reduction in the stir zone (SZ) compared to the base material (29.7 ± 6.1 μm), the SZ grain size increased with rotational speed, ranging from 4.7 ± 1.4 to 8.3 ± 1.3 μm. This study identified 900 rpm as the optimal parameter, achieving the highest load-carrying capacity (7.35 ± 0.4 kN) and a high SZ hardness (99 ± 1.5 HV). These findings confirm that joint strength is a balance between grain refinement and thermal softening. The presence of precipitates and the fractography of the tensile–shear tested specimens were also investigated and discussed. Full article
(This article belongs to the Special Issue Development of Light Alloys and Their Applications)
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21 pages, 17711 KB  
Article
Effect of Anodizing and Welding Parameters on Microstructure and Mechanical Properties of Laser-Welded A356 Alloy
by Baiwei Zhu, Hongwei Yuan, Jun Liu, Gong Chen, Tianyun Feng and Erliang Liu
Coatings 2025, 15(12), 1461; https://doi.org/10.3390/coatings15121461 - 10 Dec 2025
Viewed by 781
Abstract
This study investigates the effects of anodizing and welding parameters on the microstructure and mechanical properties of laser-welded die-cast A356 aluminum alloy. The influence of different surface oxidation conditions, namely, no anodized film (NAF), single-sheet anodized film (SSAF), and double-sheet anodized films (DSAF), [...] Read more.
This study investigates the effects of anodizing and welding parameters on the microstructure and mechanical properties of laser-welded die-cast A356 aluminum alloy. The influence of different surface oxidation conditions, namely, no anodized film (NAF), single-sheet anodized film (SSAF), and double-sheet anodized films (DSAF), was assessed. The porosity, elemental distribution, and mechanical behavior was systematically analyzed. The results indicate that anodizing reduces the fusion zone (FZ) size by approximately 5%–15% and increases porosity, primarily due to the thermal-barrier effect, energy consumption during film decomposition, and hydrogen release. Welding speed and defocusing amount have a significant impact on heat input and melt-pool dynamics. Quantitative analysis revealed that lower welding speeds and positive defocusing amount increased the FZ size by 15% and porosity by 2%–5%. In contrast, optimized conditions (welding speed of 4 m/min and 0 mm defocus) enhanced gas evacuation and minimized pore formation. Elemental analysis showed that anodizing promoted Si enrichment and increased oxygen incorporation, with oxygen content rising by 10%–15%, from 0.78 wt% (NAF) to 1.31 wt% (DSAF). Microhardness testing revealed a reduction in heat-affected zone (HAZ) hardness due to thermal softening induced by anodizing, while FZ hardness peaked under optimized welding conditions, reaching a maximum value of 95.66 HV. Tensile testing indicated that anodized films enhance the yield strength (YS) of the fusion zone (FZ) but may reduce ductility. Under optimized welding conditions (4 m/min, 0 mm), the joints exhibited the best overall performance, achieving the YS of 125.28 ± 10.57 MPa, an ultimate tensile strength (UTS) of 193.18 ± 3.66 MPa, and an elongation of 3.46 ± 0.25%. These findings provide valuable insights for optimizing both anodizing and welding parameters to improve the mechanical properties of A356 joints. Full article
(This article belongs to the Special Issue Cutting Performance of Coated Tools)
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13 pages, 3064 KB  
Article
Investigation of Weld Formation, Microstructure and Mechanical Properties of Small Core Diameter Single Mode Fiber Laser Welding of Medium Thick 6061 Aluminum Alloy
by Binyan He, Guojin Chen, Jianming Zheng and Pu Huang
Photonics 2025, 12(12), 1204; https://doi.org/10.3390/photonics12121204 - 7 Dec 2025
Viewed by 850
Abstract
In this study, a small core diameter single mode fiber laser was applied to weld an 8 mm thick plate of 6061-T6 aluminum alloy. The microstructural evolution and mechanical properties of the laser welded aluminum alloy specimens were investigated in detail. The results [...] Read more.
In this study, a small core diameter single mode fiber laser was applied to weld an 8 mm thick plate of 6061-T6 aluminum alloy. The microstructural evolution and mechanical properties of the laser welded aluminum alloy specimens were investigated in detail. The results indicated that fully penetrated welded specimens, free of welding defects like porosity, melt sagging, and hot cracking could be achieved by optimizing the processing parameters through response surface methodology. The upper part of the fusion zone consisted mainly of fine equiaxed dendrites, with secondary dendrite arm spacing (SDAS) of approximately 3–5 μm. While the lower region of the fusion zone exhibited pronounced microstructural coarsening, made up mostly of coarse columnar grains, along with some localized equiaxed grains, and an SDAS ranging from 8 to 12 μm. Both the fusion zone and heat affected zone (HAZ) were characterized by a “softened” hardness profile. The fusion zone featured a narrow region with the lowest microhardness across the welded joint with the microhardness value reducing to ~72% of the base metal (BM). Meanwhile, the microhardness of the HAZ was ~87.4% of the BM. The ultimate tensile strength of laser welded specimens was ~243.6 MPa, amounting to approximately 78.3% of the base metal. This study provides a fresh approach for welding medium-thick aluminum alloy plate using a high-quality laser beam, even at the kilowatt level with a fiber laser, and it shows a strong promise for applications in light-alloy manufacturing sectors such as automotive, rail transportation, aerospace, and beyond. Full article
(This article belongs to the Special Issue Laser Processing and Modification of Materials)
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18 pages, 4208 KB  
Article
Investigation of Single-Pass Laser Remelted Joint of Mo-5Re Alloy: Microstructure, Residual Stress and Angular Distortion
by Yifeng Wang, Danmin Peng, Xi Qiu, Mingwei Su, Shuwei Hu, Wenjie Li and Dean Deng
Metals 2025, 15(10), 1145; https://doi.org/10.3390/met15101145 - 15 Oct 2025
Viewed by 763
Abstract
Molybdenum-rhenium (Mo-Re) alloys, especially those with low Re content, have great potential in fabricating nuclear components. However, the extremely high melting point and high brittleness of Mo-Re alloys make them difficult to weld. In this study, laser welding was used to prepare single-pass [...] Read more.
Molybdenum-rhenium (Mo-Re) alloys, especially those with low Re content, have great potential in fabricating nuclear components. However, the extremely high melting point and high brittleness of Mo-Re alloys make them difficult to weld. In this study, laser welding was used to prepare single-pass remelted joint of Mo-5Re alloy with welding parameters of laser power 2800 W, welding speed 2 m·min−1 and argon gas flow rate 20 L·min−1. The microstructure of the remelted joint was investigated by the optical microscopy and the scanning electron microscopy. The microhardness distribution of the joint was analyzed. In addition, the temperature field, residual stress, and angular distortion of the joint were investigated by both numerical and experimental methods. The results show that columnar grains grew from the fusion boundary toward the center of the weld pool, and equiaxed grains formed in the central region of the fusion zone (FZ). In the heat-affected zone (HAZ), the grains transformed from initial elongated into equiaxed grains. The electron backscatter diffraction (EBSD) results revealed that high-angle grain boundaries (HAGBs) dominated in FZ. Oxide/carbide particles at grain boundaries and inside the grains can be inferred from contrast results. The average microhardness of FZ was 170 ± 5 (standard deviation) HV, which was approximately 80 HV lower than that of the base metal (250 ± 2 HV). Softening phenomenon was also observed in HAZ. The calculated weld pool shape showed high consistency with the experimental observation. The peak temperature (296 °C) of the simulated thermal cycling curve was ~8% higher than the measured value (275 °C). The residual stress calculation results indicated that FZ and its vicinity exhibited high levels of longitudinal tensile residual stresses. The simulated peak longitudinal residual stress (509 MPa) was ~30% higher than the measured value (393 MPa). Furthermore, both the simulation and experimental results demonstrated that the single-pass remelted joint of Mo-5Re alloy produced only minor angular distortion. The obtained results are very useful in understanding the basic phenomena and problems in laser welding of Mo alloys with low Re content. Full article
(This article belongs to the Special Issue Properties and Residual Stresses of Welded Alloys)
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18 pages, 13090 KB  
Article
Optimizing Laser Weldability of Heat-Treatable and Non-Heat-Treatable Aluminum Alloys: A Comprehensive Study
by Jean-Denis Béguin, Yannick Balcaen, Jade Pécune, Nathalie Aubazac and Joël Alexis
J. Manuf. Mater. Process. 2025, 9(9), 290; https://doi.org/10.3390/jmmp9090290 - 25 Aug 2025
Cited by 3 | Viewed by 1936
Abstract
Laser welding, a vital process in modern industry, offers significant technical and economic benefits, including improved part quality, precision, productivity, and cost reduction. This study significantly enhances our understanding of heat-treatable weldability (AA2024, AA2017, AA6061) and non-heat-treatable AA5083 aluminum alloys. It establishes a [...] Read more.
Laser welding, a vital process in modern industry, offers significant technical and economic benefits, including improved part quality, precision, productivity, and cost reduction. This study significantly enhances our understanding of heat-treatable weldability (AA2024, AA2017, AA6061) and non-heat-treatable AA5083 aluminum alloys. It establishes a “weldability window” based on power density and interaction time, identifying three key domains: insufficient penetration, full penetration with regular weld, and irregular weld or cutoff. The study’s findings reveal that heat-treatable alloys soften in the fusion zone due to the dissolution of reinforcing precipitates during welding. In contrast, non-heat-treatable alloys exhibit hardening due to a fine dendritic microstructure. The fusion zone features fine dendrites, and in the heat-affected zone (HAZ), coarse particles and liquation at the fusion line are observed, particularly in AA6061 and 2024 alloys. The study also shows that the joint efficiency, a measure of the weld’s load-bearing capacity, is approximately 90% for the AA5083 alloy and 80% for the heat-treatable alloys. These findings significantly contribute to our understanding of welding processes. They can be used to optimize laser welding processes, thereby ensuring the production of high-quality and reliable joints in industrial applications. Full article
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44 pages, 14734 KB  
Article
Influence of Zn Content on the Corrosion and Mechanical Properties of Cast and Friction Stir-Welded Al-Si-Mg-Fe-Zn Alloys
by Xiaomi Chen, Kun Liu, Quan Liu, Jing Kong, Valentino A. M. Cristino, Kin-Ho Lo, Zhengchao Xie, Zhi Wang, Dongfu Song and Chi-Tat Kwok
Materials 2025, 18(14), 3306; https://doi.org/10.3390/ma18143306 - 14 Jul 2025
Cited by 3 | Viewed by 1874
Abstract
With the ongoing development of lightweight automobiles, research on new aluminum alloys and welding technology has gained significant attention. Friction stir welding (FSW) is a solid-state joining technique for welding aluminum alloys without melting. In this study, novel squeeze-cast Al-Si-Mg-Fe-Zn alloys with different [...] Read more.
With the ongoing development of lightweight automobiles, research on new aluminum alloys and welding technology has gained significant attention. Friction stir welding (FSW) is a solid-state joining technique for welding aluminum alloys without melting. In this study, novel squeeze-cast Al-Si-Mg-Fe-Zn alloys with different Zn contents (0, 3.4, 6.5, and 8.3 wt%) were friction stir welded (FSWed) at a translational speed of 200 mm/min and a rotational speed of 800 rpm. These parameters were chosen based on the observations of visually sound welds, defect-free and fine-grained microstructures, homogeneous secondary phase distribution, and low roughness. Zn can affect the microstructure of Al-Si-Mg-Fe-Zn alloys, including the grain size and the content of secondary phases, leading to different mechanical and corrosion behavior. Adding different Zn contents with Mg forms the various amount of MgZn2, which has a significant strengthening effect on the alloys. Softening observed in the weld zones of the alloys with 0, 3.4, and 6.5 wt% Zn is primarily attributed to the reduction in Kernel Average Misorientation (KAM) and a decrease in the Si phase and MgZn2. Consequently, the mechanical strengths of the FSWed joints are lower as compared to the base material. Conversely, the FSWed alloy with 8.3 wt% Zn exhibited enhanced mechanical properties, with hardness of 116.3 HV0.2, yield strength (YS) of 184.4 MPa, ultimate tensile strength (UTS) of 226.9 MP, percent elongation (EL%) of 1.78%, and a strength coefficient exceeding 100%, indicating that the joint retains the strength of the as-cast one, due to refined grains and more uniformly dispersed secondary phases. The highest corrosion resistance of the FSWed alloy with 6.5%Zn is due to the smallest grain size and KAM, without MgZn2 and the highest percentage of {111} texture (24.8%). Full article
(This article belongs to the Special Issue Study on Electrochemical Behavior and Corrosion of Materials)
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20 pages, 6918 KB  
Article
Phase Transformation Kinetics During Post-Weld Heat Treatment in Weldments of C-250 Maraging Steel
by Mercedes Andrea Duran, Pablo Peitsch and Hernán Gabriel Svoboda
Materials 2025, 18(12), 2820; https://doi.org/10.3390/ma18122820 - 16 Jun 2025
Cited by 1 | Viewed by 1215
Abstract
Welding of maraging steels leads to a microstructural gradient from base material (BM) to weld metal (WM). During post-weld heat treatment (PWHT) the precipitation and reverted austenite (γr) reactions will occur defining the mechanical properties. These reactions are affected by the [...] Read more.
Welding of maraging steels leads to a microstructural gradient from base material (BM) to weld metal (WM). During post-weld heat treatment (PWHT) the precipitation and reverted austenite (γr) reactions will occur defining the mechanical properties. These reactions are affected by the microstructure and local chemical composition of each zone in the “as welded” (AW) condition. This effect has not been clearly described yet nor the evolution of the microstructure. The objective of this work was to analyse the phase transformations at the different zones of the welded joint during the PWHT to explain the microstructure obtained at each zone. Samples of C250 maraging steel were butt-welded by GTAW-P (Gas Tungsten Arc Welding—Pulsed) process without filler material. The AW condition showed an inhomogeneous microhardness profile, associated with a partial precipitation hardening in the subcritical heat affected zone (SC-HAZ) followed by a softening in the intercritical (IC-HAZ) and recrystallized heat affected zone (R-HAZ). A loop-shaped phase was observed between low temperature IC-HAZ and SC-HAZ, associated with γr, as well as microsegregation at the weld metal (WM). The microstructural evolution during PWHT (480 °C) was evaluated on samples treated to different times (1–360 min). Microhardness profile along the welded joint was mostly homogeneous after 5 min of PWHT due to precipitation reaction. The microhardness in the WM was lower than in the rest of the joint due to the depletion of Ni, Ti and Mo in the martensite matrix related with the γr formation. The isothermal kinetics of precipitation reaction at 480 °C was studied using Differential Scanning Calorimetry (DSC), obtaining a JMAK expression. The average microhardness for each weld zone was proposed for monitoring the precipitation during PWHT, showing a different behaviour for the WM. γr in the WM was also quantified and modelled, while in the IC-HAZ tends to increase with PWHT time, affecting the microhardness. Full article
(This article belongs to the Special Issue Advances on Welded Joints: Microstructure and Mechanical Properties)
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15 pages, 8046 KB  
Article
Mechanical and Microstructural Properties of High-Speed Friction Stir Welding of AA 7020 Aluminum Alloy Using Multi-Pin Tool
by Ramin Delir Nazarlou, Samita Salim, Michael Wiegand, Christian Wolf and Stefan Böhm
Metals 2025, 15(5), 511; https://doi.org/10.3390/met15050511 - 30 Apr 2025
Cited by 5 | Viewed by 2609
Abstract
High-speed friction stir welding (HSFSW) has emerged as a promising technique for improving the manufacturing efficiency of aluminum alloy structures by enabling faster welding while maintaining the quality of welded joints. This study investigates the mechanical properties and microstructural characteristics of AA 7020-T651 [...] Read more.
High-speed friction stir welding (HSFSW) has emerged as a promising technique for improving the manufacturing efficiency of aluminum alloy structures by enabling faster welding while maintaining the quality of welded joints. This study investigates the mechanical properties and microstructural characteristics of AA 7020-T651 aluminum alloy joints welded using a novel multi-pin tool at high feed rates ranging from 2500 to 6000 mm/min under a constant rotational speed of 4000 rpm. Defect-free welds were successfully fabricated, as confirmed by metallographic analysis and micro-computed tomography (µ-CT). The multi-pin tool facilitated consistent material flow and heat distribution, which contributed to reliable joint formation across all feed rates. At the highest feed rate, the tensile strength reached 76% of the base material. A consistent softening in the nugget zone (NZ) was observed, and electron backscatter diffraction (EBSD) analysis showed a more than 70% grain size reduction in this zone, averaging ~3 µm, due to dynamic recrystallization. These findings underscore the suitability of HSFSW with multi-pin tools for high-speed industrial applications, offering enhanced productivity without compromising structural integrity. Full article
(This article belongs to the Section Welding and Joining)
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18 pages, 12155 KB  
Article
The Fatigue Behavior of TC4 and Ti60 Dissimilar Titanium Alloy Joints Welded by Electron Beam
by Shiqing Wang, Xiangyong Zhu, Wenyan Zhai, Qian Gao and Yongxin Lu
Crystals 2025, 15(3), 224; https://doi.org/10.3390/cryst15030224 - 26 Feb 2025
Cited by 1 | Viewed by 1381
Abstract
During use, titanium alloy structural components may experience sudden overloads or occasional loads, which can reduce their fatigue life and accelerate structural failure. To study the fatigue behavior of TC4/Ti60 joints, this paper uses electron beam welding technology to obtain TC4/Ti60 dissimilar joints. [...] Read more.
During use, titanium alloy structural components may experience sudden overloads or occasional loads, which can reduce their fatigue life and accelerate structural failure. To study the fatigue behavior of TC4/Ti60 joints, this paper uses electron beam welding technology to obtain TC4/Ti60 dissimilar joints. The results show that the microstructure changes during the welding process, with the weld zone being relatively uniform, primarily consisting of coarse α′ phase. The near heat-affected zone on the TC4 side consists of α′, while on the Ti60 side, in addition to the α′ phase, there is a small amount of residual α phase. Fatigue tests reveal that as the pre-deformation increases, the fatigue life gradually decreases. During the early stages of fatigue, the joint exhibits cyclic hardening, which transitions to cyclic softening as the test progresses, ultimately leading to failure. Fatigue fracture analysis reveals that all fatigue samples failed on the TC4 side, with no failure observed in the weld zone. This is likely due to the presence of martensite, which gives the weld zone higher strength than the TC4 base materials. Additionally, fatigue cracks initiated from surface or near-surface defects, with ductile fractures being predominant. Full article
(This article belongs to the Special Issue Development of Light Alloys and Their Applications)
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16 pages, 8715 KB  
Article
Enhancing Strength and Ductility in the Nugget Zone of Friction Stir Welded X80 Pipeline Steel via Applying Cooling Medium
by Ruihai Duan, Guangming Xie, Xiaonan Qi, Zhaojie Wang, Shujin Chen and Ying Dong
Coatings 2025, 15(3), 260; https://doi.org/10.3390/coatings15030260 - 21 Feb 2025
Viewed by 1118
Abstract
Fusion welding easily causes microstructural coarsening and tempering softening in the heat-affected zone (HAZ) of high-strength pipeline steel joints, which considerably deteriorates the strength and toughness. Here, X80 pipeline steel was subjected to friction stir welding (FSW), and external cooling was used to [...] Read more.
Fusion welding easily causes microstructural coarsening and tempering softening in the heat-affected zone (HAZ) of high-strength pipeline steel joints, which considerably deteriorates the strength and toughness. Here, X80 pipeline steel was subjected to friction stir welding (FSW), and external cooling was used to tailor the microstructure to optimize the strength–ductility combination of the nugget zone (NZ). Coarse granular bainite (GB) appeared at air cooling, whereas a fine ferrite/martensite microstructure was achieved at solid CO2 cooling. The highest ratio of high-angle boundaries was obtained at solid CO2 cooling because the variants were evenly distributed within the four close-packed (CP) groups. The low yield strength (YS) of 595 MPa was obtained in the NZ under air cooling, whereas a high YS of 755 MPa was achieved in the NZ under solid CO2 cooling due to dislocation strengthening and fine-grain strengthening. Furthermore, an ultra-high tensile strength of 910 MPa and utilizable elongation of 15% were obtained in the NZ under solid CO2 cooling, which was attributed to the fine effective grains and ferrite/martensite microstructure facilitating a ductile fracture. Full article
(This article belongs to the Special Issue Research in Laser Welding and Surface Treatment Technology)
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