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23 pages, 5172 KB  
Article
Valorization of Recycled Gypsum from CDW in Green Binder Systems
by Roumiana Zaharieva and Borislav Simonov
Materials 2025, 18(21), 4849; https://doi.org/10.3390/ma18214849 - 23 Oct 2025
Viewed by 373
Abstract
The circular economy in construction requires the valorization of gypsum waste from construction and demolition. Waste from gypsum plasterboards is considerable, yet it is still viewed more as a problem than as a mineral resource. This study investigates the potential for utilizing recycled [...] Read more.
The circular economy in construction requires the valorization of gypsum waste from construction and demolition. Waste from gypsum plasterboards is considerable, yet it is still viewed more as a problem than as a mineral resource. This study investigates the potential for utilizing recycled gypsum (RG) from waste plasterboards in the production of blended green binders. Four gypsum–cement–pozzolanic binders are designed with two pozzolanic additives (natural zeolite and recycled brick powder) in two ratios to cement—0.6 and 1.0. The structural mineral compounds of the binders are analyzed by XRD and DTA/TG, while the performance of both fresh and hardened paste is evaluated by standardized methods for binders to determine possible construction applications of these green binders. Results show that RG can be used to produce blended fast-setting binders with a gypsum content of above 40%. Systems with natural zeolite achieve higher strength (up to 30 MPa at 90 days) and sufficient water resistance, thus suitable even as substitutes for cement binders. The developed blended binders with recycled brick powder can be used in low-moisture environments only as substitutes for gypsum binders in plasters, masonry units, and lightweight composites. Full article
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28 pages, 6292 KB  
Article
Analysis of Radiation Hardening Effect of Ferritic Martensitic Steel Based on Bayesian Optimization
by Yue He, Jiaming Bao, Shi Wu, Bing Bai, Xinfu He and Wen Yang
Crystals 2025, 15(10), 864; https://doi.org/10.3390/cryst15100864 - 30 Sep 2025
Viewed by 284
Abstract
Ferritic/martensitic (F/M) steel is a candidate material for key structures in fourth-generation nuclear energy systems (such as fusion reactors and fast reactors). Irradiation hardening behavior is a core index to evaluate the material’s stable performance in a high-neutron-irradiation environment. In this study, based [...] Read more.
Ferritic/martensitic (F/M) steel is a candidate material for key structures in fourth-generation nuclear energy systems (such as fusion reactors and fast reactors). Irradiation hardening behavior is a core index to evaluate the material’s stable performance in a high-neutron-irradiation environment. In this study, based on 2048 composition and property data, a correlation model between key elements and their interactions and irradiation hardening in F/M steel was constructed using a Bayesian optimization neural network, which realized quantitative prediction of the effect of composition on hardening behavior. Studies have shown that the addition of about 9.0% Cr, about 0.8% Si, Mo content higher than about 0.25%, and the addition of Ti, Mn can effectively suppress the irradiation hardening of F/M steel, while the addition of N, Ta, and C will aggravate its irradiation hardening, and the addition of W and V has little effect on the irradiation hardening of F/M steel. There is an interaction between the two elements. C-Cr has a strong synergistic mechanism, which will cause serious hardening when the content is higher than 0.05% and the Cr content is higher than 10%. Cr-Si has a strong antagonistic mechanism, which can achieve the comprehensive irradiation hardening effect in the 9Cr-0.8Si combination. N-Mn needs N controlled lower than 0.01%. Mo-W needs to control Mo content higher than 0.5% to alleviate irradiation hardening. There is a weak synergistic effect in Si-V; when the content is between 0.3% and 0.8% and the V content is between 0.2% and 0.3%, it can assist in optimizing the composition of F/M steel. Through the optimization of multi-element combination, the composition of F/M steel with lower irradiation hardening can be designed. Full article
(This article belongs to the Special Issue Microstructure and Characterization of Crystalline Materials)
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11 pages, 400 KB  
Article
Metabolic Dysregulation in Postmenopause: Implications for Knee Joint Health
by Ivana Minaković, Jelena Zvekić-Svorcan, Mirjana Smuđa, Bela Kolarš, Darko Mikić, Tanja Janković, Monika Šili, Miljanka Vuksanović, Nevena Đukić and Vesna Mijatović Jovin
J. Clin. Med. 2025, 14(18), 6442; https://doi.org/10.3390/jcm14186442 - 12 Sep 2025
Viewed by 559
Abstract
Background/Objectives: Osteoarthritis is a slowly evolving joint disorder defined by cartilage degradation, synovial inflammation, subchondral bone hardening, and the growth of osteophytes. Increasing evidence highlights the role of metabolic factors in osteoarthritis onset and progression. This study investigated the link between metabolic [...] Read more.
Background/Objectives: Osteoarthritis is a slowly evolving joint disorder defined by cartilage degradation, synovial inflammation, subchondral bone hardening, and the growth of osteophytes. Increasing evidence highlights the role of metabolic factors in osteoarthritis onset and progression. This study investigated the link between metabolic syndrome and the level of knee impairment in postmenopausal respondents suffering from knee osteoarthritis. Methods: A total of 200 participants aged 60–75 years with knee pain were enrolled in this observational cross-sectional study conducted between 2022 and 2023. The case group comprised 120 women with radiographically verified knee osteoarthritis (Kellgren–Lawrence grades II–IV), while 80 age-matched women without radiographic changes served as controls. Clinical and anthropometric measures, metabolic indicators, and radiographic findings were collected. Functional status was assessed using the Lower Extremity Functional Scale and the Lequesne Index. Results: The groups differed significantly with respect to the presence of metabolic syndrome, diastolic blood pressure, and fasting glucose level (p < 0.05). The metabolic syndrome showed modest but significant associations with radiographic knee damage (effect size 4.7%). After adjusting for smoking status and physical activity level, metabolic syndrome remained significantly associated with radiographic damage (effect sizes: 4.8 and 2.2%, respectively). Participants with osteoarthritis but without metabolic syndrome had better functional knee status compared to those with metabolic syndrome (p < 0.05). Conclusions: In postmenopausal women, metabolic syndrome is independently associated with radiographic knee damage and contributes to poorer functional outcomes in participants with knee osteoarthritis, underscoring its potential role as a modifiable risk factor. Full article
(This article belongs to the Section Obstetrics & Gynecology)
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20 pages, 3199 KB  
Article
When Robust Isn’t Resilient: Quantifying Budget-Driven Trade-Offs in Connectivity Cascades with Concurrent Self-Healing
by Waseem Al Aqqad
Network 2025, 5(3), 35; https://doi.org/10.3390/network5030035 - 3 Sep 2025
Viewed by 574
Abstract
Cascading link failures continue to imperil power grids, transport networks, and cyber-physical systems, yet the relationship between a network’s robustness at the moment of attack and its subsequent resiliency remains poorly understood. We introduce a dynamic framework in which connectivity-based cascades and distributed [...] Read more.
Cascading link failures continue to imperil power grids, transport networks, and cyber-physical systems, yet the relationship between a network’s robustness at the moment of attack and its subsequent resiliency remains poorly understood. We introduce a dynamic framework in which connectivity-based cascades and distributed self-healing act concurrently within each time-step. Failure is triggered when a node’s active-neighbor ratio falls below a threshold φ; healing activates once the global fraction of inactive nodes exceeds trigger T and is limited by budget B. Two real data sets—a 332-node U.S. airport graph and a 1133-node university e-mail graph—serve as testbeds. For each graph we sweep the parameter quartet (φ,B,T,attackmode) and record (i) immediate robustness R, (ii) 90% recovery time T90, and (iii) cumulative average damage. Results show that targeted hub removal is up to three times more damaging than random failure, but that prompt healing with B0.12 can halve T90. Scatter-plot analysis reveals a non-monotonic correlation: high-R states recover quickly only when B and T are favorable, whereas low-R states can rebound rapidly under ample budgets. A multiplicative fit T90Bβg(T)h(R) (with β1) captures these interactions. The findings demonstrate that structural hardening alone cannot guarantee fast recovery; resource-aware, early-triggered self-healing is the decisive factor. The proposed model and data-driven insights provide a quantitative basis for designing infrastructure that is both robust to failure and resilient in restoration. Full article
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14 pages, 1882 KB  
Article
Carbon-Negative Construction Material Based on Rice Production Residues
by Jüri Liiv, Catherine Rwamba Githuku, Marclus Mwai, Hugo Mändar, Peeter Ritslaid, Merrit Shanskiy and Ergo Rikmann
Materials 2025, 18(15), 3534; https://doi.org/10.3390/ma18153534 - 28 Jul 2025
Viewed by 748
Abstract
This study presents a cost-effective, carbon-negative construction material for affordable housing, developed entirely from locally available agricultural wastes: rice husk ash, wood ash, and rice straw—materials often problematic to dispose of in many African regions. Rice husk ash provides high amorphous silica, acting [...] Read more.
This study presents a cost-effective, carbon-negative construction material for affordable housing, developed entirely from locally available agricultural wastes: rice husk ash, wood ash, and rice straw—materials often problematic to dispose of in many African regions. Rice husk ash provides high amorphous silica, acting as a strong pozzolanic agent. Wood ash contributes calcium oxide and alkalis to serve as a reactive binder, while rice straw functions as a lightweight organic filler, enhancing thermal insulation and indoor climate comfort. These materials undergo natural pozzolanic reactions with water, eliminating the need for Portland cement—a major global source of anthropogenic CO2 emissions (~900 kg CO2/ton cement). This process is inherently carbon-negative, not only avoiding emissions from cement production but also capturing atmospheric CO2 during lime carbonation in the hardening phase. Field trials in Kenya confirmed the composite’s sufficient structural strength for low-cost housing, with added benefits including termite resistance and suitability for unskilled laborers. In a collaboration between the University of Tartu and Kenyatta University, a semi-automatic mixing and casting system was developed, enabling fast, low-labor construction of full-scale houses. This innovation aligns with Kenya’s Big Four development agenda and supports sustainable rural development, post-disaster reconstruction, and climate mitigation through scalable, eco-friendly building solutions. Full article
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25 pages, 6014 KB  
Article
Research on Synergistic Enhancement of UHPC Cold Region Repair Performance by Steel Fibers and Early-Strength Agent
by Ming Xie, Zhangdong Wang, Li’e Yin and Hao Li
Buildings 2025, 15(15), 2630; https://doi.org/10.3390/buildings15152630 - 25 Jul 2025
Cited by 1 | Viewed by 586
Abstract
This study looked at the performance requirements of repair materials for concrete structures in cold regions, systematically analyzing the effects of steel fiber dosage (0.7–2.1%), early-strength agent PRIORITY dosage (6–10%), and their coupling effects on the workability, interfacial bond strength, and freeze–thaw resistance [...] Read more.
This study looked at the performance requirements of repair materials for concrete structures in cold regions, systematically analyzing the effects of steel fiber dosage (0.7–2.1%), early-strength agent PRIORITY dosage (6–10%), and their coupling effects on the workability, interfacial bond strength, and freeze–thaw resistance of rapid-hardening ultra-high-performance concrete (UHPC). Through fluidity testing, bond interface failure analysis, freeze–thaw cycle testing, and pore analysis, the mechanism of steel fibers and early-strength agent on the multi-dimensional performance of fast-hardening UHPC was revealed. The results showed that when the steel fiber dosage exceeded 1.4%, the flowability was significantly reduced, while a PRIORITY dosage of 8% improved the flowability by 20.5% by enhancing the paste lubricity. Single addition of steel fibers decreased the interfacial bond strength, but compound addition of 8% PRIORITY offset the negative impact by optimizing the filling effect of hydration products. Under freeze–thaw cycles, excessive steel fibers (2.1%) exacerbated the mass loss (1.67%), whereas a PRIORITY dosage of 8% increased the retention rate of relative dynamic elastic modulus by 10–15%. Pore analysis shows that the synergistic effect of 1.4% steel fiber and 8% PRIORITY can reduce the number of pores, optimize the pore distribution, and make the structure denser. The study determined that the optimal compound mixing ratio was 1.4% steel fibers and 8% PRIORITY. This combination ensures construction fluidity while significantly improving the interfacial bond durability and freeze–thaw resistance, providing a theoretical basis for the design of concrete repair materials in cold regions. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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20 pages, 8458 KB  
Article
Characterization of Defects by Non-Destructive Impulse Excitation Technique for 3D Printing FDM Polyamide Materials in Bending Mode
by Fatima-Ezzahrae Jabri, Imi Ochana, François Ducobu, Rachid El Alaiji and Anthonin Demarbaix
Appl. Sci. 2025, 15(15), 8266; https://doi.org/10.3390/app15158266 - 25 Jul 2025
Viewed by 699
Abstract
The presented article analyzes the impact of internal defects on the modal responses of polyamide parts subjected to bending. Samples with defects of various sizes (0, 3, 5, 7, and 10 mm) located at the neutral bending line were tested. Modal properties were [...] Read more.
The presented article analyzes the impact of internal defects on the modal responses of polyamide parts subjected to bending. Samples with defects of various sizes (0, 3, 5, 7, and 10 mm) located at the neutral bending line were tested. Modal properties were measured via an acoustic and a vibration sensor, using impulse excitation and fast Fourier transform (FFT) analysis. Modal properties include peak frequency, damping and amplitude. Non-defective samples show lower peak frequency and stronger amplitude for both detectors. Moreover, defects larger than 3 mm have minimal impact on peak frequency. The vibration detector is more sensitive to delamination presented at 7 and 10 mm defects. In addition, elevated peak frequency at 3 mm is the result of local hardening at the defect edge. Moreover, a neutral line position reduces damping when the defect size approaches 5 mm. Conversely, acoustic detectors ignore delamination and reveal lower damping and amplitude at 7 and 10 mm defects. Furthermore, internal sound diffusion from 3 and 5 mm defects enhances air losses and damping. Acoustic detectors only evaluate fault size and position, whereas vibrational detectors may detect local reinforcement and delamination more easily. These results highlight the importance of choosing the right detector according to the location, size, and specific modal characteristics of defects. Full article
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15 pages, 4528 KB  
Article
Changes in the Structure and Mechanical Properties of the SAV-1 Alloy and Structural Fe-Cr-Ni Steels After Long-Term Service as Core Materials in Nuclear Reactors
by Alexey Dikov, Sergey Kislitsin, Boris Ivanov, Ruslan Kiryanov and Egor Maksimkin
Materials 2025, 18(14), 3391; https://doi.org/10.3390/ma18143391 - 19 Jul 2025
Viewed by 574
Abstract
This article presents the results of studies of the degradation of the structure and mechanical properties of the core materials BN-350 fast neutron and research WWR-K reactors required to justify the service life extension of early-generation power and research reactors. Extending the service [...] Read more.
This article presents the results of studies of the degradation of the structure and mechanical properties of the core materials BN-350 fast neutron and research WWR-K reactors required to justify the service life extension of early-generation power and research reactors. Extending the service life of nuclear reactors is a modern problem, since most operating reactors are early-generation reactors that have exhausted their design lifespan. The possibility of extending the service life is largely determined by the condition of the structural materials of the nuclear facility, i.e., their residual resources must ensure safe operation of the reactor. For the SAV-1 alloy, the structural material of the WWR-K reactor, studies were conducted on witness samples which were in the active zone during its operation for 56 years. It was found that yield strength and tensile strength of the irradiated SAV-1 alloy decreased by 24–48%, and relative elongation decreased by ~2% compared to the unirradiated alloy. Inside the grains and along their boundaries, there were particles of secondary phases enriched with silicon, which is typical for aged aluminum alloys. For irradiated structural steels of power reactors, studied at 350–450 C, hardening and a damping nature of creep were revealed, caused by dispersion hardening and the Hall–Petch effect. Full article
(This article belongs to the Section Energy Materials)
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11 pages, 11226 KB  
Article
Transformation Mechanism of Undercooled Austenite and Deformation Behavior of a 1.2 GPa High-Strength Medium Mn Steel
by Ying Dong, Jiachen Xu, Lingming Meng, Qinghao Miao, Haobo Cui, Jiaxin Chen, Yu Du, Tao Liu, Qingdong Feng and Chengjun Zhu
Crystals 2025, 15(5), 487; https://doi.org/10.3390/cryst15050487 - 21 May 2025
Viewed by 710
Abstract
In this study, the phase transformation mechanism during the decomposition of undercooled austenite and its effect on the deformation behavior of a high-strength medium Mn steel were studied. The results indicate that the austenite formation during heating (α → γ) is a relatively [...] Read more.
In this study, the phase transformation mechanism during the decomposition of undercooled austenite and its effect on the deformation behavior of a high-strength medium Mn steel were studied. The results indicate that the austenite formation during heating (α → γ) is a relatively fast reaction. However, the transformation of undercooled prior austenite above the martensite start (Ms) temperature (γ → α) is difficult due to its high thermal stability. Only martensite transformation occurred during the final air-cooling stage following a 120-h isothermal treatment at 360 °C (slightly above Ms). The growth of martensite laths was limited by the boundaries of prior austenite grains and martensite packets. High-strength tensile properties were achieved, with a yield strength of 955 MPa, ultimate tensile strength of 1228 MPa, and total elongation of 11.6%. These properties result from the synergistic hardening effects of grain refinement, high-density lattice distortion, and an increased boundary length per unit area. The composition design with medium Mn content increased the processing window for high-strength martensite transformation, providing a theoretical basis for an energy-saving approach that depends on the decomposition transformation of undercooled austenite. Full article
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24 pages, 7375 KB  
Article
Effect of Silicone Rubbers on the Properties of RDX-Based PBXs and Their Application in the Explosive Hardening of Steel
by Konrad Szydło, Agnieszka Stolarczyk, Tomasz Jarosz, Barbara Lisiecka, Sylwia Waśkiewicz, Krzysztof Lukaszkowicz, Klaudiusz Gołombek, Jakub Polis and Mateusz Polis
Materials 2025, 18(10), 2311; https://doi.org/10.3390/ma18102311 - 15 May 2025
Viewed by 930
Abstract
Modern energetic materials (EMs) have many different civil applications. One of their most promising applications in civil engineering is explosive hardening, which facilitates the fast and cost-effective improvement of mechanical properties in the treated material. In this work, we present the results of [...] Read more.
Modern energetic materials (EMs) have many different civil applications. One of their most promising applications in civil engineering is explosive hardening, which facilitates the fast and cost-effective improvement of mechanical properties in the treated material. In this work, we present the results of our investigation on the explosive hardening of S235JR Steel with PBX formulations containing silicone binders and 1,3,5-trinitro-1,3,5-triazinane (RDX). In terms of safety, the impact (5–15 J) and friction (240–360 N) sensitivity of the tested plastic-bonded explosives (PBXs) was verified, simultaneously with DSC tests, energy of activation calculations, and critical diameter measurement. The developed material, prepared with techniques similar to the anticipated working conditions, is characterized by a high detonation velocity (up to 7300 m/s), low sensitivity for mechanical factors (10 J, 288 N), and a small critical diameter (3.3 mm). The developed PBX based on a silicone binder demonstrated grain fragmentation, recrystallization, and an increase in the surface hardness of S235JR steel, which was confirmed with SEM, EBSD, microstructure analysis, and microhardness studies. Full article
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16 pages, 8060 KB  
Article
Low-Power and High-Performance Double-Node-Upset-Tolerant Latch Using Input-Splitting C-Element
by Qi Chen, Binyu He, Renjie Kong, Pengjia Qi and Yanyun Dai
Sensors 2025, 25(8), 2435; https://doi.org/10.3390/s25082435 - 12 Apr 2025
Viewed by 642
Abstract
Data accuracy is critical for sensor systems. As essential components of digital circuits within sensor systems, nanoscale CMOS latches are particularly susceptible to single-node upsets (SNUs) and double-node upsets (DNUs), which can lead to data errors. In this paper, a highly robust Double-Node-Upset-Tolerant [...] Read more.
Data accuracy is critical for sensor systems. As essential components of digital circuits within sensor systems, nanoscale CMOS latches are particularly susceptible to single-node upsets (SNUs) and double-node upsets (DNUs), which can lead to data errors. In this paper, a highly robust Double-Node-Upset-Tolerant Latch-Based on Input Splitting C-Elements (DNUISC) is proposed. The DNUISC latch is designed by interconnecting three sets of input-splitting C-elements to form a feedback loop, and it incorporates clock gating and fast-path techniques to minimize power consumption and delay. Simulations are conducted using the 28 nm process in HSPICE. The simulation results show that the DNUISC can self-recover from any single-node upset and is tolerant of any double-node upset. Compared with existing hardened latches, the DNUISC achieves a 55.21% reduction in area-power-delay product (APDP). Furthermore, the proposed DNUIS demonstrates high reliability and low sensitivity under varying process, voltage, and temperature conditions. Full article
(This article belongs to the Section Nanosensors)
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32 pages, 2960 KB  
Article
Comparing Application-Level Hardening Techniques for Neural Networks on GPUs
by Giuseppe Esposito, Juan-David Guerrero-Balaguera, Josie E. Rodriguez Condia and Matteo Sonza Reorda
Electronics 2025, 14(5), 1042; https://doi.org/10.3390/electronics14051042 - 6 Mar 2025
Viewed by 1296
Abstract
Neural networks (NNs) are essential in advancing modern safety-critical systems. Lightweight NN architectures are deployed on resource-constrained devices using hardware accelerators like Graphics Processing Units (GPUs) for fast responses. However, the latest semiconductor technologies may be affected by physical faults that can jeopardize [...] Read more.
Neural networks (NNs) are essential in advancing modern safety-critical systems. Lightweight NN architectures are deployed on resource-constrained devices using hardware accelerators like Graphics Processing Units (GPUs) for fast responses. However, the latest semiconductor technologies may be affected by physical faults that can jeopardize the NN computations, making fault mitigation crucial for safety-critical domains. The recent studies propose software-based Hardening Techniques (HTs) to address these faults. However, the proposed fault countermeasures are evaluated through different hardware-agnostic error models neglecting the effort required for their implementation and different test benches. Comparing application-level HTs across different studies is challenging, leaving it unclear (i) their effectiveness against hardware-aware error models on any NN and (ii) which HTs provide the best trade-off between reliability enhancement and implementation cost. In this study, application-level HTs are evaluated homogeneously and independently by performing a study on the feasibility of implementation and a reliability assessment under two hardware-aware error models: (i) weight single bit-flips and (ii) neuron bit error rate. Our results indicate that not all HTs suit every NN architecture, and their effectiveness varies depending on the evaluated error model. Techniques based on the range restriction of activation function consistently outperform others, achieving up to 58.23% greater mitigation effectiveness while keeping the introduced overhead at inference time low while requiring a contained effort in their implementation. Full article
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10 pages, 1544 KB  
Article
Rapid Solidification of Plant Latices from Campanula glomerata Driven by a Sudden Decrease in Hydrostatic Pressure
by Arne Langhoff, Astrid Peschel, Christian Leppin, Sebastian Kruppert, Thomas Speck and Diethelm Johannsmann
Plants 2025, 14(5), 798; https://doi.org/10.3390/plants14050798 - 4 Mar 2025
Cited by 1 | Viewed by 1021
Abstract
By monitoring the solidification of droplets of plant latices with a fast quartz crystal microbalance with dissipation monitoring (QCM-D), droplets from Campanula glomerata were found to solidify much faster than droplets from Euphorbia characias and also faster than droplets from all technical latices tested. [...] Read more.
By monitoring the solidification of droplets of plant latices with a fast quartz crystal microbalance with dissipation monitoring (QCM-D), droplets from Campanula glomerata were found to solidify much faster than droplets from Euphorbia characias and also faster than droplets from all technical latices tested. A similar conclusion was drawn from optical videos, where the plants were injured and the milky fluid was stretched (sometimes forming fibers) after the cut. Rapid solidification cannot be explained with physical drying because physical drying is transport-limited and therefore is inherently slow. It can, however, be explained with coagulation being triggered by a sudden decrease in hydrostatic pressure. A mechanism based on a pressure drop is corroborated by optical videos of both plants being injured under water. While the liquid exuded by E. characias keeps streaming away, the liquid exuded by C. glomerata quickly forms a plug even under water. Presumably, the pressure drop causes an influx of serum into the laticifers. The serum, in turn, triggers a transition from a liquid–liquid phase separated state (an LLPS state) of a resin and hardener to a single-phase state. QCM measurements, optical videos, and cryo-SEM images suggest that LLPS plays a role in the solidification of C. glomerata. Full article
(This article belongs to the Section Plant Physiology and Metabolism)
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10 pages, 10676 KB  
Article
Research on Fast Nanoindentation Technology to Analyze the Non-Homogeneity of IF Steel
by Xiaodan Zhang, Chao Zhang, Yunling Li, Zhaobo Wu, Jikang Li and Qilu Ge
Metals 2024, 14(12), 1429; https://doi.org/10.3390/met14121429 - 13 Dec 2024
Viewed by 1898
Abstract
Fast nanoindentation technology is a new method used to generate performance maps showing the hardness and elastic modulus distribution of each position, and it has become a research focus. In this paper, nanoindentation combined with scanning electron backscatter diffraction (EBSD) is used to [...] Read more.
Fast nanoindentation technology is a new method used to generate performance maps showing the hardness and elastic modulus distribution of each position, and it has become a research focus. In this paper, nanoindentation combined with scanning electron backscatter diffraction (EBSD) is used to analyze the micro-regional properties of single-phase interstitial-free (IF) steel. Hardness, elastic modulus and the orientation of a 200 μm × 200 μm area were characterized in situ. The relationships between hardness, elastic modulus and orientation were analyzed. The experimental results showed that the hardness varied from 1.25 GPa to 2.57 GPa, while the modulus varied from 122 GPa to 227 GPa with different crystallographic orientations. The hardness value of the (111) crystal plane was particularly high, with an average hardness of about 1.84 GPa, which is due to its higher work hardening rate. This result is consistent with the EBSD kernel average misorientation (KAM) micrograph. The harder locations with greater misorientation are more difficult to deform compared to locations with small hardness regions, for example, the (001) crystal plane. However, there seems to be no obvious strong relationship between modulus and orientation. The modulus of the regions with lower hardness seems to be smaller. The results of the KAM diagram are consistent with those of hardness mapping. Full article
(This article belongs to the Special Issue Green Super-Clean Steels)
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14 pages, 19855 KB  
Article
Effect of Deformed Prior Austenite Characteristics on Reverse Phase Transformation and Deformation Behavior of High-Strength Medium-Mn Steel
by Ying Dong, Jingwen Zhang, Tao Liu, Mingxing Ma, Lei Zhu, Chengjun Zhu and Linxiu Du
Materials 2024, 17(22), 5618; https://doi.org/10.3390/ma17225618 - 17 Nov 2024
Viewed by 1306
Abstract
In this study, microstructure evolution during prior austenite decomposition and reverse phase transformation processes was revealed in a high-strength medium-Mn steel. Furthermore, the relationship between deformed prior austenite characteristics and deformation behavior was studied. The results indicated that the recovery and recrystallization of [...] Read more.
In this study, microstructure evolution during prior austenite decomposition and reverse phase transformation processes was revealed in a high-strength medium-Mn steel. Furthermore, the relationship between deformed prior austenite characteristics and deformation behavior was studied. The results indicated that the recovery and recrystallization of the deformed prior austenite were significantly inhibited during hot rolling in the non-recrystallized zone, the grain size was obviously refined along the normal direction (ND), and that the strain hardening of prior austenite via hot deformation could increase the resistance of shear transformation, resulting in the preservation of high-density lattice defects in the quenched martensite matrix. Before the nucleation of intercritical austenite, the dislocation and grain boundary can provide fast diffusion paths for C and Mn, and the enrichment of C and Mn before intercritical austenite formation can reduce the critical temperature of ferrite/austenite transformation. The nucleated sites and driving force for intercritical austenite were strongly increased by rolling in the non-recrystallization region. The resistance of crack propagation was found to be enhanced by the sustained transformation-induced plasticity (TRIP) effect (via retained austenite with different stability) and for the laminated microstructure, the optimum properties were obtained as being a combination of yield strength of 748 MPa, tensile strength of 952 MPa, and total elongation of 26.2%. Full article
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