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17 pages, 572 KiB  
Article
Enhancing Mathematics Instruction Through Laboratory Exercises
by Md. Rasheduzzaman, Jingjing Tong, Hiranmayee Panchangam and Brad Deken
Educ. Sci. 2025, 15(8), 1008; https://doi.org/10.3390/educsci15081008 - 6 Aug 2025
Abstract
This paper describes creating a new course for engineering technology students at Southeast Missouri State University that focuses on application-based mathematics instruction through laboratory experiments. The course structure comprises beginning the semester with pre-calculus and trigonometry and progressing to calculus and differential equations. [...] Read more.
This paper describes creating a new course for engineering technology students at Southeast Missouri State University that focuses on application-based mathematics instruction through laboratory experiments. The course structure comprises beginning the semester with pre-calculus and trigonometry and progressing to calculus and differential equations. The topics are covered from the engineering and engineering technology applications standpoint, with examples from electrical and mechanical systems. A hands-on, problem-based learning approach is selected for teaching the application of mathematics to engineering technology students. This entails students being presented with real-world problems, solving them using mathematical concepts, and then verifying results by using software tools. Specifically, twelve laboratory exercises using Scilab have been incorporated into the course. For engineering students, using engineering examples improves both their ability to understand the material’s relevance and their understanding of mathematical techniques that may be applied to real-world problems that they will likely encounter in their future jobs. Full article
(This article belongs to the Special Issue Technology-Enhanced Education for Engineering Students)
34 pages, 1294 KiB  
Perspective
Electromagnetic Radiation Shielding Using Carbon Nanotube and Nanoparticle Composites
by Bianca Crank, Brayden Fricker, Andrew Hubbard, Hussain Hitawala, Farhana Islam Muna, Olalekan Samuel Okunlola, Alexandra Doherty, Alex Hulteen, Logan Powers, Gabriel Purtell, Prakash Giri, Henry Spitz and Mark Schulz
Appl. Sci. 2025, 15(15), 8696; https://doi.org/10.3390/app15158696 (registering DOI) - 6 Aug 2025
Abstract
This paper showcases current developments in the use of carbon nanotube (CNT) and nanoparticle-based materials for electromagnetic radiation shielding. Electromagnetic radiation involves different types of radiation covering a wide spectrum of frequencies. Due to their good electrical conductivity, small diameter, and light weight, [...] Read more.
This paper showcases current developments in the use of carbon nanotube (CNT) and nanoparticle-based materials for electromagnetic radiation shielding. Electromagnetic radiation involves different types of radiation covering a wide spectrum of frequencies. Due to their good electrical conductivity, small diameter, and light weight, individual CNTs are good candidates for shielding radio and microwaves. CNTs can be organized into macroscale forms by dispersing them in polymers or by wrapping CNT strands into fabrics or yarn. Magnetic nanoparticles can also be incorporated into the CNT fabric to provide excellent shielding of electromagnetic waves. However, for shielding higher-frequency X-ray and gamma ray radiation, the situation is reversed. Carbon’s low atomic number means that CNTs alone are less effective than metals. Thus, different nanoparticles such as tungsten are added to the CNT materials to provide improved shielding of photons. The goal is to achieve a desired combination of light weight, flexibility, safety, and multifunctionality for use in shielding spacecraft, satellites, nuclear reactors, and medical garments and to support lunar colonization. Future research should investigate the effect of the size, shape, and configuration of nanoparticles on radiation shielding. Developing large-scale low-cost methods for the continuous manufacturing of lightweight multifunctional nanoparticle-based materials is also needed. Full article
(This article belongs to the Section Nanotechnology and Applied Nanosciences)
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15 pages, 961 KiB  
Article
Analysis of Chemical Composition and Odor Characteristics in Particleboards Decorated by Resin-Impregnated Paper, Polypropylene Film and Polyvinyl Chloride Film
by Liming Zhu, Minghui Yang, Lina Tang, Qian Chen, Xiaorui Liu, Xianwu Zou, Yuejin Fu and Bo Liu
Polymers 2025, 17(15), 2145; https://doi.org/10.3390/polym17152145 - 5 Aug 2025
Abstract
Analysis of changes in TVOC and VOCs chemical composition or odor characteristics of particleboard before and after decoration treatment with resin-impregnated paper (RIP), polypropylene (PP) film and polyvinyl chloride (PVC) film were studied. The effects of these three decoration treatments on masking or [...] Read more.
Analysis of changes in TVOC and VOCs chemical composition or odor characteristics of particleboard before and after decoration treatment with resin-impregnated paper (RIP), polypropylene (PP) film and polyvinyl chloride (PVC) film were studied. The effects of these three decoration treatments on masking or suppressing the release of VOCs and odorants from particleboard were explored. The substances that were covered or suppressed and newly introduced before and after processing were identified to provide a basis for reducing the odor emissions of PVC-, PP- and RIP-decorated particleboard. Taking undecorated particleboard and particleboard treated by three types of decorative materials as research subjects, the air permeability of the three decorative materials was tested using the Gurley Permeability Tester. TVOC emissions from the boards were evaluated using the 1 m3 environmental chamber method. Qualitative and quantitative analyses of the samples were conducted via thermal desorption–gas chromatography–mass spectrometry (TD-GCMS). The contribution of odor substances was determined using odor activity value (OAV). The results indicated that the permeability from high to low was PVC film, PP film and RIP. Compared with undecorated particleboard, the TVOC emissions of PVC-decorated boards decreased by 93%, PP-decorated particleboard by 83% but the TVOC emissions of RIP-decorated particleboard increased by 67%. PP decoration treatment masked or suppressed the release of 20 odor substances but introduced xylene, which can increase potentially the health risks for PP-decorated particleboard. PVC decoration treatment masked or suppressed 19 odor substances, but it introduced 12 new compounds, resulting in an overall increase in TVOC emissions. RIP treatment did not introduce new odor substances. After PP film and RIP treatments, both the variety of VOCs released and the number of key odor-contributing compounds and modifying odorants decreased. In contrast, the number of modifying odorants and potential odorants increased after PVC treatment. VOC emissions were effectively masked or suppressed by three decoration treatments, same as the release of substances contributing to overall odor of particleboard was reduced. Among them, PP and RIP decorative materials demonstrate better effects. Full article
(This article belongs to the Special Issue Eco-Friendly Supramolecular Polymeric Materials, 2nd Edition)
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28 pages, 15022 KiB  
Review
Development and Core Technologies of Long-Range Underwater Gliders: A Review
by Xu Wang, Changyu Wang, Ke Zhang, Kai Ren and Jiancheng Yu
J. Mar. Sci. Eng. 2025, 13(8), 1509; https://doi.org/10.3390/jmse13081509 - 5 Aug 2025
Abstract
Long-range underwater gliders (LRUGs) have emerged as essential platforms for sustained and autonomous observation in deep and remote marine environments. This paper provides a comprehensive review of their developmental status, performance characteristics, and application progress. Emphasis is placed on two critical enabling technologies [...] Read more.
Long-range underwater gliders (LRUGs) have emerged as essential platforms for sustained and autonomous observation in deep and remote marine environments. This paper provides a comprehensive review of their developmental status, performance characteristics, and application progress. Emphasis is placed on two critical enabling technologies that fundamentally determine endurance: lightweight, pressure-resistant hull structures and high-efficiency buoyancy-driven propulsion systems. First, the role of carbon fiber composite pressure hulls in enhancing energy capacity and structural integrity is examined, with attention to material selection, fabrication methods, compressibility compatibility, and antifouling resistance. Second, the evolution of buoyancy control systems is analyzed, covering the transition to hybrid active–passive architectures, rapid-response actuators based on smart materials, thermohaline energy harvesting, and energy recovery mechanisms. Based on this analysis, the paper identifies four key technical challenges and proposes strategic research directions, including the development of ultralight, high-strength structural materials; integrated multi-mechanism antifouling technologies; energy-optimized coordinated buoyancy systems; and thermally adaptive glider platforms. Achieving a system architecture with ultra-long endurance, enhanced energy efficiency, and robust environmental adaptability is anticipated to be a foundational enabler for future long-duration missions and globally distributed underwater glider networks. Full article
(This article belongs to the Section Ocean Engineering)
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33 pages, 4132 KiB  
Review
Mechanical Properties of Biodegradable Fibers and Fibrous Mats: A Comprehensive Review
by Ehsan Niknejad, Reza Jafari and Naser Valipour Motlagh
Molecules 2025, 30(15), 3276; https://doi.org/10.3390/molecules30153276 - 5 Aug 2025
Abstract
The growing demand for sustainable materials has led to increased interest in biodegradable polymer fibers and nonwoven mats due to their eco-friendly characteristics and potential to reduce plastic pollution. This review highlights how mechanical properties influence the performance and suitability of biodegradable polymer [...] Read more.
The growing demand for sustainable materials has led to increased interest in biodegradable polymer fibers and nonwoven mats due to their eco-friendly characteristics and potential to reduce plastic pollution. This review highlights how mechanical properties influence the performance and suitability of biodegradable polymer fibers across diverse applications. This covers synthetic polymers such as polylactic acid (PLA), polyhydroxyalkanoates (PHAs), polycaprolactone (PCL), polyglycolic acid (PGA), and polyvinyl alcohol (PVA), as well as natural polymers including chitosan, collagen, cellulose, alginate, silk fibroin, and starch-based polymers. A range of fiber production methods is discussed, including electrospinning, centrifugal spinning, spunbonding, melt blowing, melt spinning, and wet spinning, with attention to how each technique influences tensile strength, elongation, and modulus. The review also addresses advances in composite fibers, nanoparticle incorporation, crosslinking methods, and post-processing strategies that improve mechanical behavior. In addition, mechanical testing techniques such as tensile test machine, atomic force microscopy, and dynamic mechanical analysis are examined to show how fabrication parameters influence fiber performance. This review examines the mechanical performance of biodegradable polymer fibers and fibrous mats, emphasizing their potential as sustainable alternatives to conventional materials in applications such as tissue engineering, drug delivery, medical implants, wound dressings, packaging, and filtration. Full article
(This article belongs to the Section Materials Chemistry)
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18 pages, 5280 KiB  
Article
A Drilling Debris Tracking and Velocity Measurement Method Based on Fine Target Feature Fusion Optimization
by Jinteng Yang, Yu Bao, Zumao Xie, Haojie Zhang, Zhongnian Li and Yonggang Li
Appl. Sci. 2025, 15(15), 8662; https://doi.org/10.3390/app15158662 (registering DOI) - 5 Aug 2025
Abstract
During unmanned drilling operations, the velocity of drill cuttings serves as an important indicator of drilling conditions, which necessitates real-time and accurate measurements. To address challenges such as the small size of cuttings, weak feature representations, and complex motion trajectories, we propose a [...] Read more.
During unmanned drilling operations, the velocity of drill cuttings serves as an important indicator of drilling conditions, which necessitates real-time and accurate measurements. To address challenges such as the small size of cuttings, weak feature representations, and complex motion trajectories, we propose a novel velocity measurement method integrating small-object detection and tracking. Specifically, we enhance the multi-scale feature fusion capability of the YOLOv11 detection head by incorporating a lightweight feature extraction module, Ghost Conv, and a feature-aligned fusion module, FA-Concat, resulting in an improved model named YOLOv11-Dd (drilling debris). Furthermore, considering the robustness of the ByteTrack algorithm in retaining low-confidence targets and handling occlusions, we integrate ByteTrack into the tracking phase to enhance tracking stability. A velocity estimation module is introduced to achieve high-precision measurement by mapping the pixel displacement of detection box centers across consecutive frames to physical space. To facilitate model training and performance evaluation, we establish a drill-cutting splash simulation dataset comprising 3787 images, covering a diverse range of ejection angles, velocities, and material types. The experimental results show that the YOLOv11-Dd model achieves a 4.65% improvement in mAP@80 over YOLOv11, reaching 76.04%. For mAP@75–95, it improves by 0.79%, reaching 41.73%. The proposed velocity estimation method achieves an average accuracy of 92.12% in speed measurement tasks, representing a 0.42% improvement compared to the original YOLOv11. Full article
(This article belongs to the Special Issue AI from Industry 4.0 to Industry 5.0: Engineering for Social Change)
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13 pages, 3691 KiB  
Article
Analysis of Kinetic Effects of Nanofibrillated Cellulose on MMA Polymerization via Temperature Monitoring
by David Victoria-Valenzuela, Ana Beatriz Morales-Cepeda and Sergio Alejandro De La Garza-Tenorio
Processes 2025, 13(8), 2476; https://doi.org/10.3390/pr13082476 - 5 Aug 2025
Abstract
This study investigates the influence of cellulose nanofibrils (CNFs) on the polymerization kinetics of methyl methacrylate (MMA) during in situ suspension polymerization at 70 °C (343.15 K). Four CNF concentrations were evaluated and compared to a reference system without CNFs. Polymerizations were carried [...] Read more.
This study investigates the influence of cellulose nanofibrils (CNFs) on the polymerization kinetics of methyl methacrylate (MMA) during in situ suspension polymerization at 70 °C (343.15 K). Four CNF concentrations were evaluated and compared to a reference system without CNFs. Polymerizations were carried out in a thermostatted flask immersed in an ethylene glycol bath and covered to ensure thermal stability. The temperature profiles of both the reaction medium and the surrounding bath were continuously recorded, allowing for the calculation of heat flow, polymerization rate (Rp), and monomer conversion. The incorporation of CNFs led to a significant increase in Rp and faster MMA conversion. This effect was attributed to the presence of nanocellulose within the polymerizing medium, which restricted diffusion and contributed to the onset of the phenomenon of autoacceleration. Additionally, CNFs promoted a higher total heat release, underscoring the need for thermal control during scale-up. The resulting material qualifies as a biocomposite, as biobased nanofibrils became integrated into the polymer matrix. These findings demonstrate that CNFs act as effective kinetic promoters in MMA polymerizations and may serve as functional additives to enhance both reaction performance and sustainability. However, safety considerations remain critical when transferring this approach to industrial processes. Full article
(This article belongs to the Special Issue Biopolymer Processing, Utilization and Applications)
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29 pages, 2636 KiB  
Review
Review on Tribological and Vibration Aspects in Mechanical Bearings of Electric Vehicles: Effect of Bearing Current, Shaft Voltage, and Electric Discharge Material Spalling Current
by Rohan Lokhande, Sitesh Kumar Mishra, Deepak Ronanki, Piyush Shakya, Vimal Edachery and Lijesh Koottaparambil
Lubricants 2025, 13(8), 349; https://doi.org/10.3390/lubricants13080349 - 5 Aug 2025
Abstract
Electric motors play a decisive role in electric vehicles by converting electrical energy into mechanical motion across various drivetrain components. However, failures in these motors can interrupt the motor function, with approximately 40% of these failures stemming from bearing issues. Key contributors to [...] Read more.
Electric motors play a decisive role in electric vehicles by converting electrical energy into mechanical motion across various drivetrain components. However, failures in these motors can interrupt the motor function, with approximately 40% of these failures stemming from bearing issues. Key contributors to bearing degradation include shaft voltage, bearing current, and electric discharge material spalling current, especially in motors powered by inverters or variable frequency drives. This review explores the tribological and vibrational aspects of bearing currents, analyzing their mechanisms and influence on electric motor performance. It addresses the challenges faced by electric vehicles, such as high-speed operation, elevated temperatures, electrical conductivity, and energy efficiency. This study investigates the origins of bearing currents, damage linked to shaft voltage and electric discharge material spalling current, and the effects of lubricant properties on bearing functionality. Moreover, it covers various methods for measuring shaft voltage and bearing current, as well as strategies to alleviate the adverse impacts of bearing currents. This comprehensive analysis aims to shed light on the detrimental effects of bearing currents on the performance and lifespan of electric motors in electric vehicles, emphasizing the importance of tribological considerations for reliable operation and durability. The aim of this study is to address the engineering problem of bearing failure in inverter-fed EV motors by integrating electrical, tribological, and lubrication perspectives. The novelty lies in proposing a conceptual link between lubricant breakdown and damage morphology to guide mitigation strategies. The study tasks include literature review, analysis of bearing current mechanisms and diagnostics, and identification of technological trends. The findings provide insights into lubricant properties and diagnostic approaches that can support industrial solutions. Full article
(This article belongs to the Special Issue Tribology of Electric Vehicles)
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17 pages, 415 KiB  
Review
Advanced Wood Composites with Recyclable or Biodegradable Polymers Embedded—A Review of Current Trends
by Paschalina Terzopoulou, Dimitris S. Achilias and Evangelia C. Vouvoudi
J. Compos. Sci. 2025, 9(8), 415; https://doi.org/10.3390/jcs9080415 - 4 Aug 2025
Abstract
Wood polymer composites (WPCs) represent a rapidly growing class of sustainable materials, formed by combining lignocellulosic fibers with thermoplastic or thermoset polymeric matrices. This review summarizes the state of the art in WPC development, emphasizing the use of recyclable (or recycled) and biodegradable [...] Read more.
Wood polymer composites (WPCs) represent a rapidly growing class of sustainable materials, formed by combining lignocellulosic fibers with thermoplastic or thermoset polymeric matrices. This review summarizes the state of the art in WPC development, emphasizing the use of recyclable (or recycled) and biodegradable polymers as matrix materials. The integration of waste wood particles into the production of WPCs addresses global environmental challenges, including plastic pollution and deforestation, by offering an alternative to conventional wood-based and petroleum-based products. Key topics covered in the review include raw material sources, fiber pre-treatments, compatibilizers, mechanical performance, water absorption behavior, thermal stability and end-use applications. Full article
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34 pages, 4273 KiB  
Review
Efficient Approaches to the Design of Six-Membered Polyazacyclic Compounds—Part 1: Aromatic Frameworks
by Elena A. Gyrgenova, Yuliya Y. Titova and Andrey V. Ivanov
Molecules 2025, 30(15), 3264; https://doi.org/10.3390/molecules30153264 - 4 Aug 2025
Abstract
This review summarises the possible applications and basic methodologies for the synthesis of six-membered polyazo heterocycles, namely, diazines, triazines, and tetrazines. The time period covered by the analysed works ranges from the beginning of the 20th century to the present day. This period [...] Read more.
This review summarises the possible applications and basic methodologies for the synthesis of six-membered polyazo heterocycles, namely, diazines, triazines, and tetrazines. The time period covered by the analysed works ranges from the beginning of the 20th century to the present day. This period was chosen because it was during this time that synthetic chemistry, as defined by physicochemical research methods, became capable of solving such complex problems as efficiently as possible. The first part of the review describes the applications of polyazo heterocyclic compounds, whose frameworks are found in the composition of drugs, dyes, and functional molecules for materials chemistry, as well as in a wide variety of natural compounds and their synthetic analogues. The review also systematises the methods for assembling six-membered aromatic polyazo heterocycles, including intramolecular and sequential cyclisation, which determine the possible structural and functional diversity based on the presence and arrangement of nitrogen atoms and the position of the corresponding substituents. Full article
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22 pages, 2066 KiB  
Article
Optimizing In Vitro Establishment Protocols for ‘Merensky 2’ Avocado Rootstock (Persea americana Mill.)
by Fernanda García-Cabrera, Mónica Castro, Ricardo Cautin, Carmen Estay, Leda Guzmán, María José Marchant and Francesca Guerra
Horticulturae 2025, 11(8), 900; https://doi.org/10.3390/horticulturae11080900 (registering DOI) - 3 Aug 2025
Viewed by 192
Abstract
In vitro propagation of avocado faces several limitations. To optimize the establishment phase, we evaluated three plant material types: etiolated shoots, 30-day covered field shoots, and uncovered field shoots, collected at two time points. Biochemical and anatomical analyses were conducted to understand material [...] Read more.
In vitro propagation of avocado faces several limitations. To optimize the establishment phase, we evaluated three plant material types: etiolated shoots, 30-day covered field shoots, and uncovered field shoots, collected at two time points. Biochemical and anatomical analyses were conducted to understand material performance during establishment. Across both collection times, etiolated shoots exhibited minimal oxidation, enhanced bud sprouting, reduced malondialdehyde (MDA) and reactive oxygen species (ROS) levels, increased peroxidase (POD) activity, and improved xylem development, consistently outperforming field-derived materials. Using etiolated shoots, we optimized disinfection and in vitro multiplication protocols. Pre-disinfection with 3 mL L−1 Phyton 27® and 2% sodium hypochlorite yielded the highest survival rates. In multiplication experiments, varying concentrations of 6-benzylaminopurine (BAP) and meta-topolin (MT), supplemented with gibberellic acid (GA3), did not significantly affect growth variation. However, 8.88 µM BAP with 0.29 µM GA3 resulted in the greatest number of sprouted buds. Full article
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19 pages, 582 KiB  
Article
Xylitol Antioxidant Properties: A Potential Effect for Inflammation Reduction in Menopausal Women?—A Pilot Study
by Ilona Górna, Magdalena Kowalówka, Barbara Więckowska, Michalina Banaszak, Grzegorz Kosewski, Olivia Grządzielska, Juliusz Przysławski and Sławomira Drzymała-Czyż
Curr. Issues Mol. Biol. 2025, 47(8), 611; https://doi.org/10.3390/cimb47080611 - 2 Aug 2025
Viewed by 199
Abstract
Introduction: Oxidative stress is a key factor in the pathogenesis of many chronic diseases, especially in postmenopausal women. Xylitol, a sugar alcohol with potential antioxidant properties, may affect oxidative balance when used as a sugar substitute. Aim: This pilot study aimed to assess [...] Read more.
Introduction: Oxidative stress is a key factor in the pathogenesis of many chronic diseases, especially in postmenopausal women. Xylitol, a sugar alcohol with potential antioxidant properties, may affect oxidative balance when used as a sugar substitute. Aim: This pilot study aimed to assess the effect of replacing sucrose with xylitol on serum antioxidant capacity in postmenopausal women. Methods: This study included 34 women aged 50 to 65 years who successively consumed 5 g/d, 10 g/d, and 15 g/d of xylitol. The dietary intervention lasted a total of 6 weeks, with each phase covering a 2-week period. Diet was assessed twice based on a 7-day dietary interview (Diet 6.0, NIZP–PZH, Warsaw). The material for this study was venous blood. Antioxidant capacity was determined using the DPPH radical scavenging method and the ABTS cation radical scavenging method. Results: In both methods, a significant increase in serum antioxidant potential was observed after replacing sugar with xylitol (p < 0.0001). An increase in the ability to neutralize free radicals was observed in almost all women studied. Additional analysis of the effect of selected nutrients on the obtained effects of the nutritional intervention showed that the most significant effect could potentially be exerted by manganese, maltose, sucrose, and mercury, and the strongest positive correlation was exerted by vitamin A, retinol, and vitamin E. Although the values obtained in the constructed models were not statistically significant, the large effect indicates potentially significant relationships that could have a significant impact on serum antioxidant potential in the studied group of women. Conclusions: The results suggest a potential role of xylitol in enhancing antioxidant defense mechanisms in menopausal women. Although the sample size was relatively small, this study was powered at approximately 80% to detect large effects, supporting the reliability of the observed results. Nevertheless, given the pilot nature of this study, further research with larger cohorts is warranted to confirm these preliminary observations and to clarify the clinical significance of xylitol supplementation in populations exposed to oxidative stress. Full article
(This article belongs to the Special Issue Role of Natural Products in Inflammatory Diseases)
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17 pages, 2459 KiB  
Article
Comparative Life Cycle Assessment of Rubberized Warm-Mix Asphalt Pavements: A Cradle-to-Gate Plus Maintenance Approach
by Ana María Rodríguez-Alloza and Daniel Garraín
Coatings 2025, 15(8), 899; https://doi.org/10.3390/coatings15080899 (registering DOI) - 1 Aug 2025
Viewed by 190
Abstract
In response to the escalating climate crisis, reducing greenhouse gas emissions (GHG) has become a top priority for both the public and private sectors. The pavement industry plays a key role in this transition, offering innovative technologies that minimize environmental impacts without compromising [...] Read more.
In response to the escalating climate crisis, reducing greenhouse gas emissions (GHG) has become a top priority for both the public and private sectors. The pavement industry plays a key role in this transition, offering innovative technologies that minimize environmental impacts without compromising performance. Among these, the incorporation of recycled tire rubber and warm-mix asphalt (WMA) additives represents a promising strategy to reduce energy consumption and resource depletion in road construction. This study conducts a comparative life cycle assessment (LCA) to evaluate the environmental performance of an asphalt pavement incorporating recycled rubber and a WMA additive—referred to as R-W asphalt—against a conventional hot-mix asphalt (HMA) pavement. The analysis follows the ISO 14040/44 standards, covering material production, transport, construction, and maintenance. Two service-life scenarios are considered: one assuming equivalent durability and another with a five-year extension for the R-W pavement. The results demonstrate environmental impact reductions of up to 57%, with average savings ranging from 32% to 52% across key impact categories such as climate change, land use, and resource use. These benefits are primarily attributed to lower production temperatures and extended maintenance intervals. The findings underscore the potential of R-W asphalt as a cleaner engineering solution aligned with circular economy principles and climate mitigation goals. Full article
(This article belongs to the Special Issue Surface Protection of Pavements: New Perspectives and Applications)
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16 pages, 2858 KiB  
Article
Reactive Aerosol Jet Printing of Ag Nanoparticles: A New Tool for SERS Substrate Preparation
by Eugenio Gibertini, Lydia Federica Gervasini, Jody Albertazzi, Lorenzo Maria Facchetti, Matteo Tommasini, Valentina Busini and Luca Magagnin
Coatings 2025, 15(8), 900; https://doi.org/10.3390/coatings15080900 (registering DOI) - 1 Aug 2025
Viewed by 118
Abstract
The detection of trace chemicals at low and ultra-low concentrations is critical for applications in environmental monitoring, medical diagnostics, food safety and other fields. Conventional detection techniques often lack the required sensitivity, specificity, or cost-effectiveness, making real-time, in situ analysis challenging. Surface-enhanced Raman [...] Read more.
The detection of trace chemicals at low and ultra-low concentrations is critical for applications in environmental monitoring, medical diagnostics, food safety and other fields. Conventional detection techniques often lack the required sensitivity, specificity, or cost-effectiveness, making real-time, in situ analysis challenging. Surface-enhanced Raman spectroscopy (SERS) is a powerful analytical tool, offering improved sensitivity through the enhancement of Raman scattering by plasmonic nanostructures. While noble metals such as Ag and Au are currently the reference choices for SERS substrates, fabrication methods should balance enhancement efficiency, reproducibility and scalability. In this study, we propose a novel approach for SERS substrate fabrication using reactive Aerosol Jet Printing (r-AJP) as an innovative additive manufacturing technique. The r-AJP process enables in-flight Ag seed reduction and nucleation of Ag nanoparticles (NPs) by mixing silver nitrate and ascorbic acid aerosols before deposition, as suggested by computational fluid dynamics (CFD) simulations. The resulting coatings were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM) analyses, revealing the formation of nanoporous crystalline Ag agglomerates partially covered by residual matter. The as-prepared SERS substrates exhibited remarkable SERS activity, demonstrating a high enhancement factor (106) for rhodamine (R6G) detection. Our findings highlight the potential of r-AJP as a scalable and cost-effective fabrication strategy for next-generation SERS sensors, paving the way for the development of a new additive manufacturing tool for noble metal material deposition. Full article
(This article belongs to the Section Surface Characterization, Deposition and Modification)
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18 pages, 4332 KiB  
Article
Soils of the Settlements of the Yamal Region (Russia): Morphology, Diversity, and Their Environmental Role
by Evgeny Abakumov, Alexandr Pechkin, Sergey Kouzov and Anna Kravchuk
Appl. Sci. 2025, 15(15), 8569; https://doi.org/10.3390/app15158569 (registering DOI) - 1 Aug 2025
Viewed by 113
Abstract
The landscapes of the Arctic seem endless. But they are also subject to anthropogenic impact, especially in urbanized and industrial ecosystems. The population of the Arctic zone of Russia is extremely urbanized, and up to 84% of the population lives in cities and [...] Read more.
The landscapes of the Arctic seem endless. But they are also subject to anthropogenic impact, especially in urbanized and industrial ecosystems. The population of the Arctic zone of Russia is extremely urbanized, and up to 84% of the population lives in cities and industrial settlements. In this regard, we studied the background soils of forests and tundras and the soils of settlements. The main signs of the urbanogenic morphogenesis of soils associated with the transportation of material for urban construction are revealed. The peculiarities of soils of recreational, residential, and industrial zones of urbanized ecosystems are described. The questions of diversity and the classification of soils are discussed. The specificity of bulk soils used in the construction of industrial structures in the context of the initial stage of soil formation is considered. For the first time, soils and soil cover of settlements in the central and southern parts of the Yamal region are described in the context of traditional pedology. It is shown that the construction of new soils and grounds can lead to both decreases and increases in biodiversity, including the appearance of protected species. Surprisingly, the forms of urban soil formation in the Arctic are very diversified in terms of morphology, as well as in the ecological functions performed by soils. The urbanization of past decades has drastically changed the local soil cover. Full article
(This article belongs to the Section Environmental Sciences)
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