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17 pages, 5565 KiB  
Article
Green Mild Acid Treatment of Recycled Concrete Aggregates: Concentration Thresholds for Mortar Removal While Avoiding Degradation of Original Limestone Aggregate and Concrete
by Shunquan Zhang and Yifan Zhang
Materials 2025, 18(15), 3673; https://doi.org/10.3390/ma18153673 - 5 Aug 2025
Abstract
While acetic acid has proven effective as a mild acidic treatment for removing adhered mortar from recycled concrete aggregate (RCA) surfaces, its potential for dissolving damage to the surface of the original natural coarse aggregate (NCA) within the RCA and its impact on [...] Read more.
While acetic acid has proven effective as a mild acidic treatment for removing adhered mortar from recycled concrete aggregate (RCA) surfaces, its potential for dissolving damage to the surface of the original natural coarse aggregate (NCA) within the RCA and its impact on the resultant concrete properties require careful consideration. This investigation systematically evaluates the effects of varying concentrations of dilute acetic acid solutions, commonly used in RCA treatment protocols, through a multi-methodological approach that includes comprehensive physical characterization, stylus and 3D optical profilometry, scanning electron microscopy (SEM), and nanoindentation analysis. The results show that even dilute acid solutions have an upper concentration limit, as excessive acid concentration, specifically 0.4 M, induces significant textural dislocations on NCA surfaces, creating millimeter-scale erosion pits that increase aggregate water absorption by 18.5%. These morphological changes significantly impair concrete workability and reduce compressive strength performance. Furthermore, microstructural analysis reveals a 45.24% expansion in interfacial transition zone (ITZ) thickness, accompanied by notable reductions in elastic modulus and microhardness characteristics. In practical RCA treatment applications, for RCA containing limestone-based NCA, it is recommended to use acetic acid concentrations between 0.1 and 0.3 M to avoid substantial physical and microstructural degradation of aggregates and concrete. Full article
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22 pages, 10739 KiB  
Article
Effects of Natural Seashell Presence on the Engineering Performance of Sea Sand Concrete
by Anuradha Koswaththa, Pasindu Abeyaratne, Samith Buddika, Hiran Yapa and Satheeskumar Navaratnam
Buildings 2025, 15(15), 2751; https://doi.org/10.3390/buildings15152751 - 4 Aug 2025
Abstract
Processed sea sand has emerged as a viable alternative to traditional fine aggregates in the Sri Lankan construction industry. Despite its economic and environmental advantages, concerns over residual seashell content have limited its widespread adoption by local contractors. Residual seashell content, typically ranging [...] Read more.
Processed sea sand has emerged as a viable alternative to traditional fine aggregates in the Sri Lankan construction industry. Despite its economic and environmental advantages, concerns over residual seashell content have limited its widespread adoption by local contractors. Residual seashell content, typically ranging from 1% to 3% after processing, has raised concerns about its impact on the performance of concrete. This study systematically investigates the influence of seashell fragments, with a content of up to 5%, on the fresh, mechanical, and durability properties of sea sand concrete and mortar. Experimental results indicate that workability remains stable, with minor variations across the tested range of shell content. Compressive strength remains relatively consistent from 0% to 5% seashells, indicating that seashell content does not significantly impact the strength within this range. Durability tests reveal minimal effects of shell content on concrete performance within the tested shell range, as indicated by results for water absorption, rapid chloride penetration, and acid exposure testing. Accelerated corrosion indicates that the typical shell content does not increase corrosion risk; however, high shell content (>3%) can compromise corrosion durability. Overall, these findings demonstrate that the mechanical and durability performance of sea sand concrete remains uncompromised at typical seashell content levels (1–3%), supporting the use of processed sea sand as a sustainable and viable alternative to traditional fine aggregates in Sri Lankan construction. Full article
(This article belongs to the Collection Advanced Concrete Materials in Construction)
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16 pages, 1572 KiB  
Article
Application of ANN in the Performance Evaluation of Composite Recycled Mortar
by Shichao Zhao, Yaohua Liu, Geng Xu, Hao Zhang, Feng Liu and Binglei Wang
Buildings 2025, 15(15), 2752; https://doi.org/10.3390/buildings15152752 - 4 Aug 2025
Abstract
To promote the large-scale utilization of construction and industrial solid waste in engineering, this study focuses on developing accurate prediction and optimization methods for the unconfined compressive strength (UCS) of composite recycled mortar. Innovatively incorporating three types of recycled powder (RP)—recycled clay brick [...] Read more.
To promote the large-scale utilization of construction and industrial solid waste in engineering, this study focuses on developing accurate prediction and optimization methods for the unconfined compressive strength (UCS) of composite recycled mortar. Innovatively incorporating three types of recycled powder (RP)—recycled clay brick powder (RCBS), recycled concrete powder (RCBP), and recycled gypsum powder (RCGP)—we systematically investigated the effects of RP type, replacement rate, and curing period on mortar UCS. The core objective and novelty lie in establishing and comparing three artificial intelligence models for high-precision UCS prediction. Furthermore, leveraging GA-BP’s functional extremum optimization theory, we determined the optimal UCS alongside its corresponding mix proportion and curing scheme, with experimental validation of the solution reliability. Key findings include the following: (1) Increasing total RP content significantly reduces mortar UCS; the maximum UCS is achieved with a 1:1 blend ratio of RCBP:RCGP, while a 20% RCBS replacement rate and extended curing periods markedly enhance strength. (2) Among the prediction models, GA-BP demonstrates superior performance, significantly outperforming BP models with both single and double hidden layer. (3) The functional extremum optimization results exhibit high consistency with experimental validation, showing a relative error below 10%, confirming the method’s effectiveness and engineering applicability. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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31 pages, 1741 KiB  
Review
Recycled Concrete Aggregate in Asphalt Mixtures: A Review
by Juan Gabriel Bastidas-Martínez, Hugo Alexander Rondón-Quintana and Luis Ángel Moreno-Anselmi
Recycling 2025, 10(4), 155; https://doi.org/10.3390/recycling10040155 - 2 Aug 2025
Viewed by 88
Abstract
Effective management and handling of construction and demolition waste (CDW) can yield significant technical and environmental benefits for road pavement construction. This article aims to provide a comprehensive and up-to-date chronological review of studies on the mechanical performance of asphalt mixtures—primarily hot mix [...] Read more.
Effective management and handling of construction and demolition waste (CDW) can yield significant technical and environmental benefits for road pavement construction. This article aims to provide a comprehensive and up-to-date chronological review of studies on the mechanical performance of asphalt mixtures—primarily hot mix asphalt (HMA)—incorporating recycled concrete aggregate (RCA). Since the main limitation of RCA is the presence of residual adhered mortar, the review also includes studies that applied various surface treatments (mechanical, chemical, and thermal, among others) to enhance mixture performance. The article summarizes the experimental procedures used and highlights the key findings and conclusions of the reviewed research. Although the results are varied and sometimes contradictory—mainly due to the source variability and heterogeneity of RCA—the use of these materials is technically viable. Moreover, their application can provide environmental, social, and economic advantages, particularly in the construction of low-traffic roadways. Finally, the article identifies research gaps and offers recommendations for future researches. Full article
(This article belongs to the Special Issue Recycled Materials in Sustainable Pavement Innovation)
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18 pages, 3916 KiB  
Article
Bond Behavior Between Fabric-Reinforced Cementitious Matrix (FRCM) Composites and Different Substrates: An Experimental Investigation
by Pengfei Ma, Shangke Yuan and Shuming Jia
J. Compos. Sci. 2025, 9(8), 407; https://doi.org/10.3390/jcs9080407 - 1 Aug 2025
Viewed by 156
Abstract
This study investigates the bond behavior of fabric-reinforced cementitious matrix (FRCM) composites with three common masonry substrates—solid clay bricks (SBs), perforated bricks (PBs), and concrete hollow blocks (HBs)—using knitted polyester grille (KPG) fabric. Through uniaxial tensile tests of the KPG fabric and FRCM [...] Read more.
This study investigates the bond behavior of fabric-reinforced cementitious matrix (FRCM) composites with three common masonry substrates—solid clay bricks (SBs), perforated bricks (PBs), and concrete hollow blocks (HBs)—using knitted polyester grille (KPG) fabric. Through uniaxial tensile tests of the KPG fabric and FRCM system, along with single-lap and double-lap shear tests, the interfacial debonding modes, load-slip responses, and composite utilization ratio were evaluated. Key findings reveal that (i) SB and HB substrates predominantly exhibited fabric slippage (FS) or matrix–fabric (MF) debonding, while PB substrates consistently failed at the matrix–substrate (MS) interface, due to their smooth surface texture. (ii) Prism specimens with mortar joints showed enhanced interfacial friction, leading to higher load fluctuations compared to brick units. PB substrates demonstrated the lowest peak stress (69.64–74.33 MPa), while SB and HB achieved comparable peak stresses (133.91–155.95 MPa). (iii) The FRCM system only achieved a utilization rate of 12–30% in fabric and reinforcement systems. The debonding failure at the matrix–substrate interface is one of the reasons that cannot be ignored, and exploring methods to improve the bonding performance between the matrix–substrate interface is the next research direction. HB bricks have excellent bonding properties, and it is recommended to prioritize their use in retrofit applications, followed by SB bricks. These findings provide insights into optimizing the application of FRCM reinforcement systems in masonry structures. Full article
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17 pages, 2616 KiB  
Article
Investigation of the Dynamic Characterization of Traditional and Modern Building Materials Using an Impact Excitation Test
by Anil Ozdemir
Buildings 2025, 15(15), 2682; https://doi.org/10.3390/buildings15152682 - 30 Jul 2025
Viewed by 237
Abstract
This study presents a comprehensive non-destructive evaluation of a broad range of construction materials using the impulse excitation of vibration (IEV) technique. Tested specimens included low- and normal-strength concrete, fiber-reinforced concrete (with basalt, polypropylene, and glass fibers), lime mortars (NHL-2 and -3.5), plaster, [...] Read more.
This study presents a comprehensive non-destructive evaluation of a broad range of construction materials using the impulse excitation of vibration (IEV) technique. Tested specimens included low- and normal-strength concrete, fiber-reinforced concrete (with basalt, polypropylene, and glass fibers), lime mortars (NHL-2 and -3.5), plaster, and clay bricks (light and dark). Compressive and flexural strength tests complemented dynamic resonance testing on the same samples to ensure full mechanical characterization. Flexural and torsional resonance frequencies were used to calculate dynamic elastic modulus, shear modulus, and Poisson’s ratio. Strong correlations were observed between dynamic elastic modulus and shear modulus, supporting the compatibility of dynamic results with the classical elasticity theory. Flexural frequencies were more sensitive to material differences than torsional ones. Fiber additives, particularly basalt and polypropylene, significantly improved dynamic stiffness, increasing the dynamic elastic modulus/compressive strength ratio by up to 23%. In contrast, normal-strength concrete exhibited limited stiffness improvement despite higher strength. These findings highlight the reliability of IEV in mechanical properties across diverse material types and provide comparative reference data for concrete and masonry applications. Full article
(This article belongs to the Special Issue Advanced Studies in Structure Materials—2nd Edition)
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25 pages, 9769 KiB  
Article
Mesoscale Mechanical Analysis of Concrete Based on a 3D Random Aggregate Model
by Shuaishuai Wei, Huan Zhang, Ding Wang, Xuchun Wang and Mengdi Cao
Coatings 2025, 15(8), 883; https://doi.org/10.3390/coatings15080883 - 29 Jul 2025
Viewed by 310
Abstract
The shape, size, and interfacial transition zone (ITZ) of aggregates significantly impact the nonlinear mechanical behavior of concrete. This study investigates concrete’s mechanical response and damage mechanisms by developing a three-dimensional, three-phase mesoscale model comprising coarse aggregates, mortar, and ITZ to explore the [...] Read more.
The shape, size, and interfacial transition zone (ITZ) of aggregates significantly impact the nonlinear mechanical behavior of concrete. This study investigates concrete’s mechanical response and damage mechanisms by developing a three-dimensional, three-phase mesoscale model comprising coarse aggregates, mortar, and ITZ to explore the compressive performance of concrete. A method for simulating the random distribution of aggregates based on three-dimensional grid partitioning is proposed, where the value of each grid point represents the maximum aggregate radius that can be accommodated if the point serves as the aggregate center. Aggregates are generated by randomly selecting grid points that meet specific conditions, avoiding overlapping distributions and significantly improving computational efficiency as the generation progresses. This model effectively enhances the precision and efficiency of aggregate distribution and provides a reliable tool for studying the random distribution characteristics of aggregates in concrete. Additionally, an efficient discrete element model (DEM) was established based on this mesoscale model to simulate the compressive behavior of concrete, including failure modes and stress–strain curves. The effects of aggregate shape and maximum aggregate size on the uniaxial compressive failure behavior of concrete specimens were investigated. Aggregate shape has a particular influence on the compressive strength of concrete, and the compressive strength decreases with an increase in maximum aggregate size. Combined with existing experimental results, the proposed mesoscale model demonstrates high reliability in analyzing the compressive performance of concrete, providing valuable insights for further research on the mechanical properties of concrete. Full article
(This article belongs to the Special Issue Advances in Pavement Materials and Civil Engineering)
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26 pages, 11239 KiB  
Review
Microbial Mineral Gel Network for Enhancing the Performance of Recycled Concrete: A Review
by Yuanxun Zheng, Liwei Wang, Hongyin Xu, Tianhang Zhang, Peng Zhang and Menglong Qi
Gels 2025, 11(8), 581; https://doi.org/10.3390/gels11080581 - 27 Jul 2025
Viewed by 225
Abstract
The dramatic increase in urban construction waste poses severe environmental challenges. Utilizing waste concrete to produce recycled aggregates (RA) for manufacturing recycled concrete (RC) represents an effective strategy for resource utilization. However, inherent defects in RA, such as high porosity, microcracks, and adherent [...] Read more.
The dramatic increase in urban construction waste poses severe environmental challenges. Utilizing waste concrete to produce recycled aggregates (RA) for manufacturing recycled concrete (RC) represents an effective strategy for resource utilization. However, inherent defects in RA, such as high porosity, microcracks, and adherent old mortar layers, lead to significant performance degradation of the resulting RC, limiting its widespread application. Traditional methods for enhancing RA often suffer from limitations, including high energy consumption, increased costs, or the introduction of new pollutants. MICP offers an innovative approach for enhancing RC performance. This technique employs the metabolic activity of specific microorganisms to induce the formation of a three-dimensionally interwoven calcium carbonate gel network within the pores and on the surface of RA. This gel network can improve the inherent defects of RA, thereby enhancing the performance of RC. Compared to conventional techniques, this approach demonstrates significant environmental benefits and enhances concrete compressive strength by 5–30%. Furthermore, embedding mineralizing microbial spores within the pores of RA enables the production of self-healing RC. This review systematically explores recent research advances in microbial mineral gel network for improving RC performance. It begins by delineating the fundamental mechanisms underlying microbial mineralization, detailing the key biochemical reactions driving the formation of calcium carbonate (CaCO3) gel, and introducing the common types of microorganisms involved. Subsequently, it critically discusses the key environmental factors influencing the effectiveness of MICP treatment on RA and strategies for their optimization. The analysis focuses on the enhancement of critical mechanical properties of RC achieved through MICP treatment, elucidating the underlying strengthening mechanisms at the microscale. Furthermore, the review synthesizes findings on the self-healing efficiency of MICP-based RC, including such metrics as crack width healing ratio, permeability recovery, and restoration of mechanical properties. Key factors influencing self-healing effectiveness are also discussed. Finally, building upon the current research landscape, the review provides perspectives on future research directions for advancing microbial mineralization gel techniques to enhance RC performance, offering a theoretical reference for translating this technology into practical engineering applications. Full article
(This article belongs to the Special Issue Novel Polymer Gels: Synthesis, Properties, and Applications)
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22 pages, 12147 KiB  
Technical Note
Effects of the Aggregate Shape and Petrography on the Durability of Stone Mastic Asphalt
by Alain Stony Bile Sondey, Vincent Aaron Maleriado, Helga Ros Fridgeirsdottir, Damian Serwin, Carl Christian Thodesen and Diego Maria Barbieri
Infrastructures 2025, 10(8), 198; https://doi.org/10.3390/infrastructures10080198 - 26 Jul 2025
Viewed by 320
Abstract
Compared to traditional dense asphalt concrete mixtures, stone mastic asphalt (SMA) generally offers superior performance in terms of its mechanical resistance and extended pavement lifespan. Focusing on the Norwegian scenario, this laboratory-based study investigated the durability of SMA considering the influence of the [...] Read more.
Compared to traditional dense asphalt concrete mixtures, stone mastic asphalt (SMA) generally offers superior performance in terms of its mechanical resistance and extended pavement lifespan. Focusing on the Norwegian scenario, this laboratory-based study investigated the durability of SMA considering the influence of the aggregate shape and petrography. The rock aggregates were classified according to three different-shaped refinement stages involving vertical shaft impact crushing. Further, the aggregates were sourced from three distinct locations (Jelsa, Tau and Dirdal) characterized by different petrographic origins: granodiorite, quartz diorite and granite, respectively. Two mixtures with maximum aggregate sizes of 16 mm (SMA 16) and 11 mm (SMA 11) were designed according to Norwegian standards and investigated in terms of their durability performance. In this regard, two main functional tests were performed for the asphalt mixture, namely resistance against permanent deformation and abrasion by studded tyres, and one for the asphalt mortar, namely water sensitivity. Overall, the best test results were related to the aggregates sourced from Jelsa and Tau, thus highlighting that the geological origin exerts a major impact on SMA’s durability performance. On the other hand, the different aggregate shapes related to the crushing refinement treatments seem to play an effective but secondary role. Full article
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26 pages, 6714 KiB  
Article
Study on the Shear Performance of MMOM Stay-in-Place Formwork Beams Reinforced with Perforated Steel Pipe Skeleton
by Lingling Li, Chuanhe Shang and Xiaodong Wang
Buildings 2025, 15(15), 2638; https://doi.org/10.3390/buildings15152638 - 26 Jul 2025
Viewed by 267
Abstract
The simulation analysis of a novel stay-in-place formwork (SIPF) beam reinforced with perforated steel pipe skeleton was conducted. The SIPF beam consists of a modified magnesium oxysulfide mortar (MMOM) formwork, a square steel pipe skeleton with holes dug on the sides and top, [...] Read more.
The simulation analysis of a novel stay-in-place formwork (SIPF) beam reinforced with perforated steel pipe skeleton was conducted. The SIPF beam consists of a modified magnesium oxysulfide mortar (MMOM) formwork, a square steel pipe skeleton with holes dug on the sides and top, and cast-in-place concrete. The finite element (FE) analysis model of the SIPF beam was established by using the ABAQUS CAE 2021 software, and simulation analysis was conducted with the shear span ratio (SSR), the distance between the remaining steel strips, and the strength of concrete as the variation parameters. The results show that the stiffness and shear capacity of the SIPF beam decrease with the increase in SSR and increase with the decrease in strip spacing. Under the same conditions, when the concrete strength grade is increased from C30 to C50, the shear bearing capacity of the SIPF beam increases by 11.8% to 16.2%. When the spacing of the steel strips is reduced from 200 mm to 150 mm, the shear bearing capacity can be increased by 12.7% to 31.5%. When the SSR increases from 1.5 to 3.0, the shear bearing capacity decreases by 26.9% to 37.3%. Moreover, with the increase in the SSR, the influence of the steel strip spacing on the shear bearing capacity of the SIPF beam improves, while the influence of the concrete strength on the shear bearing capacity decreases. Taking parameters such as SSR, steel strip spacing, and concrete strength as variables, the influence of steel pipe constraining the core concrete on the shear bearing capacity was considered. The calculation formula for the shear bearing capacity of the SIPF beam with perforated steel pipe skeleton was established. The calculation results fit well with the laboratory test and simulation test results and can be used for the design and calculation of engineering structures. Full article
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41 pages, 1835 KiB  
Review
A Comprehensive Review of Vertical Forest Buildings: Integrating Structural, Energy, Forestry, and Occupant Comfort Aspects in Renovation Modeling
by Vachan Vanian, Theodora Fanaradelli and Theodoros Rousakis
Fibers 2025, 13(8), 101; https://doi.org/10.3390/fib13080101 - 25 Jul 2025
Viewed by 146
Abstract
This current review examines modeling approaches for renovating reinforced concrete (RC) buildings for vertical forest (VF) application, taking into account structural retrofitting, energy systems, forestry integration, and occupant comfort. The study assesses research conducted with an advanced 3D finite element analysis and the [...] Read more.
This current review examines modeling approaches for renovating reinforced concrete (RC) buildings for vertical forest (VF) application, taking into account structural retrofitting, energy systems, forestry integration, and occupant comfort. The study assesses research conducted with an advanced 3D finite element analysis and the use of retrofitting modeling techniques, including textile-reinforced mortar (TRM), fiber-reinforced polymer (FRP), seismic joints, and green concrete applications. The energy system modeling methods are reviewed, taking into account the complexity of incorporating vegetation and seasonal variations. During forestry integration, three main design parameters are identified, namely, root systems, trunks, and crowns, for their critical role in the structural stability and optimal environmental performance. The comfort models are identified evolving from static to adaptive models incorporating thermal, acoustic, visual and air quality parameters. The current review consists of more than one hundred studies indicating that the integration of natural systems to buildings requires a multidimensional and multidisciplinary approach with sophisticated systems. The findings of this review provide the basis for implementing VF models to RC buildings, while highlighting areas requiring further research and validation. Full article
(This article belongs to the Collection Review Papers of Fibers)
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20 pages, 2239 KiB  
Article
Synthesis of Biomass Polycarboxylate Superplasticizer and Its Performance on Cement-Based Materials
by Zefeng Kou, Kaijian Huang, Muhua Chen, Hongyan Chu, Linye Zhou and Tianqi Yin
Materials 2025, 18(14), 3416; https://doi.org/10.3390/ma18143416 - 21 Jul 2025
Viewed by 370
Abstract
Polycarboxylate superplasticizer (PCE) is an important part of improving the overall performance of concrete. However, its synthetic raw materials are overly dependent on petrochemical products, and it also causes problems such as environmental pollution. With the development of the building material industry, the [...] Read more.
Polycarboxylate superplasticizer (PCE) is an important part of improving the overall performance of concrete. However, its synthetic raw materials are overly dependent on petrochemical products, and it also causes problems such as environmental pollution. With the development of the building material industry, the demand for petrochemical resources required for synthetic water-reducing agents will increase rapidly. Therefore, there is an urgent need to transition the synthetic raw materials of PCE from petrochemicals to biomass materials to reduce the consumption of nonrenewable resources as well as the burden on the environment. Biomass materials are inexpensive, readily available and renewable. Utilizing biomass resources to develop good-performing water-reducing agents can reduce the consumption of fossil resources. This is conducive to carbon emission reduction in the concrete material industry. In addition, it promotes the high-value utilization of biomass resources. Therefore, in this study, a biomass polyether monomer, acryloyl hydroxyethyl cellulose (AHEC), was synthesized from cellulose via the reaction route of ethylene oxide (EO) etherification and acrylic acid (AA) esterification. Biomass polycarboxylate superplasticizers (PCE-Cs) were synthesized through free radical polymerization by substituting AHEC for a portion of the frequently utilized polyether monomer isopentenyl polyoxyethylene ether (TPEG). This study primarily focused on the properties of PCE-Cs in relation to cement. The findings of this study indicated that the synthesized PCE-C5 at a dosing of 0.4% (expressed as mass fraction of cement) when the AHEC substitution ratio was 5% achieved good water reduction properties and significant delays. With the same fluidity, PCE-C5 could enhance the mechanical strength of cement mortar by 30% to 40%. This study utilized green and low-carbon biomass resources to develop synthetic raw materials for water-reducing agents, which exhibited effective water-reducing performance and enhanced the utilization rate of biomass resources, demonstrating significant application value. Full article
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17 pages, 2531 KiB  
Article
Evaluation of the Alkali–Silica Reaction Potential of Korean Aggregates: Experimental Insights and Mitigation Strategies for Concrete Durability
by Chul Seoung Baek and Byoung Woon You
Materials 2025, 18(14), 3373; https://doi.org/10.3390/ma18143373 - 18 Jul 2025
Viewed by 362
Abstract
The alkali–silica reaction (ASR) is an important mechanism of concrete deterioration, whereby reactive silica in aggregate interacts with cement alkalis to form expanding gel, which compromises the structural integrity of the concrete. Although the Republic of Korea has historically been classified as a [...] Read more.
The alkali–silica reaction (ASR) is an important mechanism of concrete deterioration, whereby reactive silica in aggregate interacts with cement alkalis to form expanding gel, which compromises the structural integrity of the concrete. Although the Republic of Korea has historically been classified as a low-risk region for ASR due to its geological stability, documented examples of concrete damage since the late 1990s have necessitated a rigorous reassessment of local aggregates. This study evaluated the ASR potential of 84 aggregate samples sourced from diverse Korean geological regions using standardized protocols, including ASTM C 1260 for mortar bar expansion and ASTM C 289 for chemical reactivity, supplemented by soundness, acid drainage, and weathering index analyses. The results indicate expansion within the range of 0.1–0.2%, classified as potentially deleterious, for some rock types. In addition to ASR reactivity, isolated high anomalies (e.g., high soundness, acid producing, and weathering) suggest the existence of other durability risks. Consequently, while Korean aggregates predominantly have a low ASR reactivity, the adoption of various validated ASR tests as a routine test and the integration of supplementary cementitious materials are recommended to ensure long-term concrete durability, highlighting the need for sustained monitoring and further investigation into mitigation strategies. Full article
(This article belongs to the Section Construction and Building Materials)
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20 pages, 8022 KiB  
Article
Corrosion Response of Steel to Penetration of Chlorides in DC-Treated Hardened Portland Cement Mortar
by Milan Kouřil, Jan Saksa, Vojtěch Hybášek, Ivona Sedlářová, Jiří Němeček, Martina Kohoutková and Jiří Němeček
Materials 2025, 18(14), 3365; https://doi.org/10.3390/ma18143365 - 17 Jul 2025
Viewed by 241
Abstract
Electrochemical treatment by means of direct current (DC) is usually used as a measure for steel rebar corrosion protection, e.g., cathodic protection (CP), electrochemical chloride extraction (ECE), and re-alkalization (RA). However, the passage of an electrical charge through the pore system of concrete [...] Read more.
Electrochemical treatment by means of direct current (DC) is usually used as a measure for steel rebar corrosion protection, e.g., cathodic protection (CP), electrochemical chloride extraction (ECE), and re-alkalization (RA). However, the passage of an electrical charge through the pore system of concrete or mortar, coupled with the migration of ions, concentration changes, and resulting phase changes, may alter its chloride penetration resistance and, subsequently, the time until rebar corrosion activation. Porosity changes in hardened Portland cement mortar were studied by means of mercury intrusion porosimetry (MIP) and electrochemical impedance spectroscopy (EIS), and alterations in the mortar surface phase composition were observed by means of X-ray diffraction (XRD). In order to innovatively investigate the impact of DC treatment on the properties of the mortar–electrolyte interface, the cathode-facing mortar surface and the anode-facing mortar surface were analyzed separately. The corrosion of steel coupons embedded in DC-treated hardened mortar was monitored by means of the free corrosion potential (Eoc) and polarization resistance (Rp). The results showed that the DC treatment affected the surface porosity of the hardened Portland cement mortar at the nanoscale. Up to two-thirds of the small pores (0.001–0.01 µm) were replaced by medium-sized pores (0.01–0.06 µm), which may be significant for chloride ingress. Although the porosity and phase composition alterations were confirmed using other techniques (EIS and XRD), corrosion tests revealed that they did not significantly affect the time until the corrosion activation of the steel coupons in the mortar. Full article
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15 pages, 588 KiB  
Review
Archaeometry of Ancient Mortar-Based Materials in Roman Regio X and Neighboring Territories: A First Review
by Simone Dilaria
Minerals 2025, 15(7), 746; https://doi.org/10.3390/min15070746 - 16 Jul 2025
Viewed by 346
Abstract
This review synthesizes the corpus of archaeometric and analytical investigations focused on mortar-based materials, including wall paintings, plasters, and concrete, in the Roman Regio X and neighboring territories of northeastern Italy from the mid-1970s to the present. Organized into three principal categories—wall paintings [...] Read more.
This review synthesizes the corpus of archaeometric and analytical investigations focused on mortar-based materials, including wall paintings, plasters, and concrete, in the Roman Regio X and neighboring territories of northeastern Italy from the mid-1970s to the present. Organized into three principal categories—wall paintings and pigments, structural and foundational mortars, and flooring preparations—the analysis highlights the main methodological advances and progress in petrographic microscopy, mineralogical analysis, and mechanical testing of ancient mortars. Despite extensive case studies, the review identifies a critical need for systematic, statistically robust, and chronologically anchored datasets to fully reconstruct socio-economic and technological landscapes of this provincial region. This work offers a programmatic research agenda aimed at bridging current gaps and fostering integrated understandings of ancient construction technologies in northern Italy. The full forms of the abbreviations used throughout the text to describe the analytical equipment are provided at the end of the document in the “Abbreviations” section. Full article
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