Search Results (24)

The trends in the building industry related to sustainability and environmental footprint make timber structures more appealing than ever. Many challenges in understanding the behaviour of structural timber can be addressed by combining experimental and numerical methods. However, sophisticated numerical tools require a complete description of the behaviour at the material level. Even though there are vast databases on the properties of different species, there are only limited studies on the mechanical response with complete stress–strain curves for all relevant directions. In order to bridge this gap, the present study investigates the mechanical response of European oak (hardwood) and Norway spruce (softwood). Uniaxial tensile and compressive tests were performed on small clear wood specimens. The behaviour was investigated for the direction parallel (longitudinal) and perpendicular to the grain (radial and tangential). Both species exhibit brittle tensile behaviour in all material directions, in contrast to the ductile performance under compression. The tensile strength lies at 70 MPa and 80 MPa for spruce and oak, respectively, whereas both species exhibit a compressive strength of approximately 50 MPa in the longitudinal direction. Due to the narrow range of the investigated density, growth-ring angle and growth-ring width, only a limited effect of these parameters was observed on the tensile behaviour in the longitudinal direction. Full article

The Loess Plateau region of China has an anomalous climate and frequent geological disasters. Hipparion laterite in seasonally frozen regions exhibits heightened susceptibility to freeze–thaw (F-T) cycling, which induces progressive structural weakening and significantly elevates the risk of slope instability through mechanisms including pore water phase transitions, aggregate disintegration, and shear strength degradation. This study focuses on the slip zone Hipparion laterite from the Nao panliang landslide in Fugu County, Shaanxi Province. We innovatively integrated F-T cycling tests with ring-shear experiments to establish a hydro-thermal–mechanical coupled multi-scale evaluation framework for assessing F-T damage in the slip zone material. The microstructural evolution of soil architecture and pore characteristics was systematically analyzed through scanning electron microscopy (SEM) tests. Quantitative characterization of mechanical degradation mechanisms was achieved using advanced microstructural parameters including orientation frequency, probabilistic entropy, and fractal dimensions, revealing the intrinsic relationship between pore network anisotropy and macroscopic strength deterioration. The experimental results demonstrate that Hipparion laterite specimens undergo progressive deterioration with increasing F-T cycles and initial moisture content, predominantly exhibiting brittle deformation patterns. The soil exhibited substantial strength degradation, with total reduction rates of 51.54% and 43.67% for peak and residual strengths, respectively. The shear stress–displacement curves transitioned from strain-softening to strain-hardening behavior, indicating plastic deformation-dominated shear damage. Moisture content critically regulates pore microstructure evolution, reducing micropore proportion to 23.57–28.62% while promoting transformation to mesopores and macropores. At 24% moisture content, the areal porosity, probabilistic entropy, and fractal dimension increased by 0.2263, 0.0401, and 0.0589, respectively. Temperature-induced pore water phase transitions significantly amplified mechanical strength variability through cyclic damage accumulation. These findings advance the theoretical understanding of Hipparion laterite’s engineering geological behavior while providing critical insights for slope stability assessment and landslide risk mitigation strategies in loess plateau regions. Full article

Cemented tailings backfill (CTB) plays an important role in mine filling operations. In order to study the long-term stability of CTB under the dynamic disturbance of deep wells, ultrafine cemented tailings backfill was taken as the research object, and the true triaxial hydraulic fracturing antireflection-wetting dynamic experimental system of coal and rock was used to carry out a static true triaxial compression test, a true triaxial compression test under unidirectional disturbance, and a true triaxial compression test under bidirectional disturbance. At the same time, the acoustic emission monitoring and positioning tests of the CTB were carried out during the compression test. The evolution law of the mechanical parameters and deformation and failure characteristics of CTB under different confining pressures is analyzed, and the damage constitutive model of the filling body is established using stochastic statistical theory. The results show that the compressive strength of CTB increases with an increase in intermediate principal stress. According to the change process of the acoustic emission ringing count over time, the triaxial compression test can be divided into four stages: the initial active stage, initial calm stage, pre-peak active stage, and post-peak calm stage. When the intermediate principal stress is small, the specimen is dominated by shear failure. With an increase in the intermediate principal stress, the specimen changes from brittle failure to plastic failure. The deformation and failure strength of CTB are closely related to its loading and unloading methods. Under a certain stress intensity, compared with unidirectional unloading, bidirectional unloading produces a greater deformation of the rock mass, and the failure strength of the rock mass is higher. This study only considers the confining pressure within the compressive limit of the specimen. Future research can be directed at a wider range of stresses to improve the applicability and reliability of the research results. Full article

Ti(C, N)-based cermets are problematic in practical production applications due to their brittleness. To improve this defect, Ti(C, N)-based cermets were prepared under different sintering environments using a spark plasma sintering (SPS) device with different contents of Mo₂C and 25 wt.% of nano tungsten carbide as additives. By means of microstructural analysis and comprehensive performance tests, the Ti(C, N) cermet with 6 wt.% Mo₂C content showed the best comprehensive performance when sintered at 1450 °C under a pressure of 25 MPa with a holding time of 16 min. The density of this metal-ceramic was 6.27 g/cm³, the Vickers hardness was HV 2731, and the fracture toughness was 10.1 MPa·m^1/2, which increased the density by 15%, the hardness by 63%, and the fracture toughness by 84% compared with the ceramic without added Mo₂C. Densification of cermets can be promoted using SPS. The moderate addition of Mo₂C can improve the wettability between the bonded phase and the hard phase, and its joint action with tungsten carbide can promote the formation of a ring structure and inhibit the growth of core-structure grains to enhance the toughness of the ceramic. Full article

In modern tunnel construction, complex environments with high geothermal gradients and abundant groundwater are frequently encountered. To investigate the damage and failure mechanisms of sandstone under the combined effects of temperature and water, uniaxial compression tests were conducted on sandstone at different temperatures (25 °C, 55 °C, 85 °C, and 95 °C) and soaking durations (0.5 h, 1 h, and 3 h). The acoustic emission (AE) signals and energy evolution during the damage and failure processes were analyzed, revealing the damage characteristics and failure mechanisms of sandstone. The results indicate the following: (1) As the temperature increases, under the 3 h condition, the water content of sandstone is highest at 55 °C, reaching 3.01%, and the thermal expansion effect of sandstone is not obvious. Under the conditions of 85 °C and 95 °C, the thermal expansion effect leads to a decrease in the water content, enhances the water absorption softening effect, increases the plastic deformation capacity of sandstone, and weakens its brittle failure capacity. (2) When soaked for 0.5 h and 1 h, the maximum acoustic emission ring count and maximum acoustic emission energy of sandstone increase initially, then decrease, and subsequently increase again as the temperature rises, while the cumulative acoustic emission ring count gradually increases with temperature. Under the 3 h soaking condition, the maximum ring count, maximum energy, and cumulative ring count of sandstone at all temperatures show a consistent increasing trend with temperature. (3) The increase in soaking time reduced the damage variable of sandstone, with the largest reduction of 54.17% under the 3 h condition. At different temperatures, the damage variable of sandstone was smallest at 55 °C, only 0.33. (4) Sandstone primarily experiences tensile failure under different temperatures and soaking times. The extension of soaking time promotes the development of shear cracks, while the increase in temperature can effectively promote the expansion of tensile cracks. The research results provide certain theoretical references for the damage and failure of surrounding rock in modern tunnel construction. Full article

Crack generation and propagation are critical aspects of grinding processes for hard and brittle materials. Despite extensive research, the impact of residual cracks from coarse grinding on the cracks generated during fine grinding remains unexplored. This study aims to bridge this gap by examining the propagation law of existing cracks under indentation using the extended finite element method. The results reveal that prefabricated cracks with depths less than the crack depth produced on an undamaged surface tend to extend further without surpassing the latter. Conversely, deeper prefabricated cracks do not exhibit significant expansion. A novel method combining indentation and prefabricated cracks with fracture strength tests is proposed to determine crack propagation. Silicon wafers with varying damaged surfaces are analyzed, and changes in fracture strength, measured by the ball-on-ring method, are utilized to determine crack propagation. The experimental results confirm the proposed crack evolution law, validated by damage assessments across different grinding processes, which is suitable for crack damage. The findings demonstrate that residual cracks from coarse grinding are negligible in predicting the maximum crack depth during fine grinding. This research provides a crucial foundation for optimizing the wafer thinning process in 3D stacked chip manufacturing, establishing that changes in fracture strength are a reliable indicator of crack propagation feasibility. Full article

Poly-3-hydroxybutyrate (P3HB) is a biodegradable polyester produced mainly by bacterial fermentation in an isotactic configuration. Its high crystallinity (about 70%) and brittle behavior have limited the process window and the application of this polymer in different sectors. Atactic poly-3-hydroxybutyrate (a-P3HB) is an amorphous polymer that can be synthesized chemically and blended with the isotactic P3HB to reduce its crystallinity and improve its processability Ring-opening polymerization (ROP) is the most cited synthesis route for this polymer in the literature. In this work, a new synthesis route of a-P3HB by self-polycondensation of racemic ethyl 3-hydroxybutyrate will be demonstrated. Different catalysts were tested regarding their effectiveness, and the reaction parameters were optimized using titanium isopropoxide as the catalyst. The resulting polymers were compared by self-polycondensation for their properties with those of a-P3HB obtained by the ROP and characterized by Fourier transform infrared spectroscopy (FTIR) and gel permeation chromatography (GPC), and the double bond content (DBC) was determined by UV–VIS spectroscopy by using 3-butenoic acid as a standard. Additionally, a life cycle analysis (LCA) of the new method of synthesizing has been carried out to assess the environmental impact of a-P3HB. Full article

To study the mechanical performance of bolted connections with different structural forms of reinforced rings, based on the results of monotonic loading tests on two bolted connections between a concrete-filled steel tubular column and a steel beam with an outer reinforcing ring, this article uses ABAQUS v.2020 software to establish a three-dimensional refined finite element analysis model of such connections using appropriate constitutive models for concrete and steel. Subsequently, the effect of the dimensions of the steel beam, reinforcing ring, and cover plate on the load-bearing properties and the failure mechanism of the connections is investigated, and the numerical model is consistent with the verification test results. Then, the numerical simulations comparing bolted exterior reinforced rings under seven different construction measures (i.e., number of bolts, stiffeners) based on a conventional welded exterior reinforced rings with rigid connections (i.e., CGJ) are standardized. The research results indicate that when four rows of bolts are introduced on exterior reinforced rings, the web of steel beam is welded with stiffeners, and the top and bottom reinforced rings are also added with stiffeners; this bolted connection with an external reinforcing ring (i.e., GZ-7) can achieve the rigidity and load-bearing capacity of a fully welded external reinforcing ring rigid connection. At the same time, the reinforcing ring plate is bolted to the flange of the steel beam, and the force transmission path at the connection is changed to avoid the brittle fracture easily caused by the welded flange joints. It is also in line with the development trend of sustainable construction of “assembly” and “disassembly”. Full article

In the realm of engineering rotary excavation, the rigid and brittle nature of the Polycrystal Diamond Compact (PDC) layer poses challenges to the impact resistance of conical teeth. This hinders their widespread adoption and utilization. In this paper, the Abaqus simulation is used. By optimizing the parameters of the radius of the cone top arc, we analyzed the changing law of the parameters of large-diameter D30 series conical PDC teeth, such as the equivalent force, impact force, and energy absorption of the conical teeth during the impact process, and optimized the best structure of the conical PDC teeth. After being subjected to a high temperature and high pressure, we synthesized the specimen for impact testing and analyzed the PDC layer crack extension and fracture failure. The findings reveal the emergence of a stress ring below the compacted area of the conical tooth. As the radius of the cone top arc increases, so does the area of the stress ring. When R ≥ 10 mm, the maximum stress change is minimal, and at R = 10 mm, the stress change in its top unit is relatively smooth. Optimal impact resistance is achieved, withstanding a total impact work value of 7500 J. Extrusion cracks appear in the combined layer part of PDC layers I and II, but the crack source is easy to produce in the combined layer of PDC layer II and the alloy matrix and extends to both sides, and the right side extends to the surface of the conical tooth in a “dragon-claw”. The failure morphology of the conical teeth includes ring shedding at the top of the PDC layer, the lateral spalling of the PDC layer, and the overall cracking of the conical teeth. Through this study, we aim to promote the popularization and application of large-diameter conical PDC teeth in the field of engineering rotary excavation. Full article

In this paper, 5083 aluminum alloy and T2 copper were selected for the friction stir lap welding test. The effect of intermetallic compounds on the microstructure and properties of Al/Cu dissimilar metal lap joints was studied. The results showed that the circulating Al/Cu composite structure was formed on the advancing side of the lap joint, and the Al/Cu staggered hook-like structure and copper-rich region were generated on the retreating side. There was no typical ‘onion ring’ structure in the joint. Element diffusion occurred at the interface of the joint, forming a thin and uniform interfacial layer of Al/Cu intermetallic compounds, thus achieving a well-metallurgical bond at the Al/Cu interface. There were the intermetallic compounds Al₂Cu and Al₄Cu₉, without AlCu, in the lap joint. In addition, dynamic recrystallization occurred in the nugget zone, and higher dislocation density and dislocation entanglement were generated, which enhanced the deformation resistance in the nugget zone and increased the joint strength. The tensile test showed that the ductile–brittle mixed fracture occurred in the heat-affected zone on the advancing side of the aluminum plate, and the fracture had necking. The failure load of the lap joint was 4350 ± 30 N, about 80% of the aluminum base metal. The elongation of the Al/Cu dissimilar lap joint tensile specimen was 2.5%. Full article

This study investigates the sealing performance of a combined sealing structure under extremely high and low temperature conditions, considering potential issues like high-temperature aging and low-temperature brittle fracture, which can lead to sealing failure. EPDM rubber underwent uniaxial compression tests at high, low, and normal temperatures, then the sealing performance under extreme working conditions was compared with that under normal temperature conditions. Additionally, the influences of gasket parameters and gas pressure on the sealing performance were analyzed. The result shows that compared with the normal temperature conditions, the maximum von Mises stress is reduced by 65% and the effective sealing length and the maximum contact pressure is reduced by 40% under the high temperature conditions, while the maximum von Mises stress is increased by 7 times and the maximum contact pressure is increased by a remarkable 7 times under the low temperature conditions. In the range of 10–100 MPa, the increase in gas pressure aggravates the O-ring stress concentration and improves the sealing performance relatively. When the thickness of gasket is 0.85–1.05 mm, the stress concentration of the O-ring is lighter and the sealing performance is better. Full article

In order to study the physical and mechanical properties of sandstone under high-temperature water-cooling cycling conditions, an RMT-150B electrohydraulic servo rock testing system and a DS-5 acoustic emission detection and analysis system were used to conduct uniaxial compression acoustic emission tests on sandstone after high-temperature water-cooling cycles. The deformation, strength, and acoustic emission characteristics of sandstone were analyzed under different temperatures and cycle times. The results show that the high-temperature water-cooling effect caused changes in the physical properties of sandstone. The volumetric expansion rate of the rock samples first decreased, then increased in temperature, and the strength first increased, then decreased, whereas the number of cycles had less of an impact on the physical properties. At 200 °C, with increased cycle number, the elastic modulus increased by 20.1%, and the compressive strength increased from 63.9 MPa to 71.46 MPa. At 300–600 °C, the elastic modulus and compressive strength of sandstone gradually decreased with increases in the temperature and cycle number, with reductions of 6.04%, 7.24%, 28.7%, 35.57%, 17.6%, 18.2%, 20.4%, and 60.5%, respectively. With increased temperature and cycle times, the acoustic emission ringing counts increased, ringing counts and cumulative energy appeared earlier, the rock samples entered elastic deformation earlier, the yield stage length increased, and the samples showed a tendency to transition from brittle to ductile damage. Full article

The sustained casing pressure (SCP) phenomenon of shale gas and oil wells occurs frequently after fracturing; therefore, in order to assess the cement sheath’s integrity in the vertical well portion, the cement stones were subjected to a compression test under different temperatures and confining pressures to obtain the mechanical parameters of the cement sheath at different well depths. The integrity of the cement ring between the production casing and the intermediate casing was then investigated using the Moore–Coulomb criterion. We also took into account other elements including pump pressure, production casing wall thickness, and cement ring mechanical properties. The results show that (1) the compressive strength, Poisson’s ratio, and Young’s modulus of cement stone vary obviously under different confining pressures and temperature conditions, and the cement stone shows elastic–brittle failure characteristics at 20 °C. The compressive strength, Poisson’s ratio, and Young’s modulus increase with the confining pressure, but the Young’s modulus and compressive strength gradually decrease with the increase in temperature, while the stress–strain curves show obvious plastic failure characteristics at 80 °C and 130 °C. (2) The tangential tensile stress decreases and depth increases from the wellhead to the intermediate casing shoe, while the radial compressive stress of the cement sheath increases. The stress state of the cement sheath changes abruptly at the position of the casing shoe due to the change in casing layers, and under the intermediate casing shoe, the tangential tensile stress changes from tension to compression. When a conventional cementing slurry system is used, the integrity of the cement sheath above the intermediate casing shoe will fail during fracturing. (3) Reducing the pump pressure and increasing casing wall thickness can reduce the tangential and radial stresses of the cement sheath, but the integrity of cement sheath cannot be fully guaranteed. For the cement sheath’s sealing integrity, it is advantageous to decrease the Young’s modulus and raise its strength. Full article

Primer is widely used to prepare bonding of chlorinated poly(vinyl chloride) (CPVC) pipe. The study examined the influences of primer and its major component, acetone, on CPVC’s mechanical properties. Two types of CPVC product, sheet and pipe, were used in the mechanical testing. Sheet specimens were immersed in acetone or primer for 40 and 10 min, respectively, i.e., the maximum allowable time without mass loss, and then dried in air before the mechanical testing. Pipe (ring) specimens were treated either through immersion in acetone or primer for 30 min or in contact with these solvents locally on the inner surface for 2.5 h, and then air dried for 10.5 days before the mechanical testing. Results showed that CPVC’s strength decreased after the absorption of these solvents, and air dry could remove acetone but not completely primer. The study also showed that pipe specimens by local contact with primer could generate brittle fracture. In view that sheet specimens always fractured in a ductile manner, brittle fracture of the pipe specimens could not be caused by CPVC degradation. Rather, strength decrease in the local region could provide a plausible explanation for the brittle fracture behavior, though further investigation is needed. Full article

The step from the testing of oxygen transport membranes on a lab scale to long-term operation on a large scale is a challenge. In a previous study, membrane failure was observed at defined positions of one end of the cooled tubular Ba_0.5Sr_0.5Co_0.8Fe_0.2O_3−δ membranes after an emergency shutdown. To understand the failure mechanisms, strength degradation and transient stress distribution were investigated by brittle-ring tests and finite element simulations, respectively. A 15% decrease in the characteristic strength of 162 MPa was proven after aging at 850 °C and was attributed to grain coarsening. The reduction in characteristic strength after thermal shock ranged from 5 to 90% depending on the cooling rates, and from 5 to 40% after the first and 20th soft thermal cycling. Simulations indicated the chemical strains induced by a 10-bar feed air and 50 mbar permeate pressure, which caused tensile stresses of up to 70 MPa at the outer surface. These stresses relaxed to 43 MPa by creep within a 1000 h operation. A remaining local stress maximum seemed to be responsible for the fracture. It evolved near the experimentally observed fracture position during a 1000 h permeation and exceeded the temperature and time-dependent strength. The maximum stress was formed by a chemical strain at temperatures above 500 °C but effective creep relaxation needed temperatures above 750 °C. Full article