Search Results (3)

NiTi shape memory alloys (SMAs) are widely studied for their potential applications, and atomic layer deposition (ALD) is an effective technique for coating them due to its precise control over coating thickness. This study investigates the impact of Al₂O₃ coating on the fatigue behavior of cold-drawn NiTi wires with a 0.125 mm diameter. The wires were coated using atomic layer deposition (ALD) with 100 ALD cycles. Fatigue tests were conducted in tensile mode at room temperature, applying cyclic loading between 0–50, and 700 MPa (700 MPa is almost 40% of ultimate tensile strength). The results show that the cold-drawn NiTi wires failed after an average of 7500 tensile loading cycles, while the lifetime of the coated and stretched NiTi wires with a preload of 1.7–2.8 kg significantly improved, with an average of 293,000 cycles before failure. Full article

The present study was carried out using a cold-drawn wire of Ni_50.8Ti at.% subjected to post-deformation solution treatment at 700 °C for 1 h to obtain a fine-grained recrystallized structure. Subsequent aging was carried out at a temperature range of 300, 430, and 500 °C for 1, 10, and 20 h. The time–temperature aging mode strongly affects the aging-induced microstructure. Variation of the aging-induced microstructure (using various aging modes) permits precise tuning of the characteristic temperature of the martensitic transformations and their specific temperature ranges upon cooling and heating. The latent heat and hysteresis exhibit different evolution vs. aging durations; this finding remains fair when using different aging temperatures. The aging mode strongly affects the stress–temperature behavior: (i) a dramatical expansion of the temperature range of realization of the transformation yield stress (σ_tr); and (ii) the magnitude of σ_tr at a chosen test temperature is generally determined by the position of the M_s temperature. An additional contribution of competing factors is discussed. The efficiency of the aging temperature under isochronous aging is significantly higher than the efficiency of the aging time under isothermal aging. Aging at 430 °C for 10–20 h provides the highest resource for the recovery strain. The strain–temperature behavior strongly depends on the relative position of the R_s and M_s temperatures (onset of B2→R and R→B19′ transformations, respectively). The regularities obtained can be used to predict the set of functional and mechanical properties of titanium nickelide. Full article

The specific damping capacity variation of heat-treated NiTi was observed during a pseudoelasticity test. The detailed B2 → R-phase transformation process in cold-drawn NiTi wires undergoing middle-temperature aging was studied via X-ray diffraction, transmission electron microscope, and internal friction technique. Results show that, as aging time increased at 450 °C, the dynamic phase transition splitting from B2 → R to B2 → R₁ and B2 → R₂ became evident. However, such a splitting process was not observed for the sample after aging at 400 °C. The reason for R-phase generation is attributed to non-uniformly distributed stress fields. The splitting of the internal friction peak, in conjunction with high-resolution transmission electron microscope and mechanic results, suggests a substantial occurrence of short-range segregation of Ni atoms in the B2-NiTi matrix. Furthermore, the specific damping capacity (SDC) exhibits a gradual increase with prolonged annealing time. Specifically, the sample with significant dynamic phase transition splitting reaches an SDC value of 0.60. Full article