Nondestructive Evaluation of Thermal Barrier Coatings Interface Delamination Using Terahertz Technique Combined with SWT-PCA-GA-BP Algorithm

Thermal barrier coatings (TBCs) are usually subjected to the combined action of compressive stress, tensile stress, and bending shear stress, resulting in the interfacial delamination of TBCs, and finally causing the ceramic top coat to peel off. Hence, it is vital to detect the early-stage subcritical delamination cracks. In this study, a novel hybrid artificial neural network combined with the terahertz nondestructive technology was presented to predict the thickness of interface delamination in the early stage. The finite difference time domain (FDTD) algorithm was used to obtain the raw terahertz time-domain signals of 32 TBCs samples with various thicknesses of interface delamination, not only that, the influence of roughness and the thickness of the ceramic top layer were considered comprehensively when modeling. The stationary wavelet transform (SWT) and principal component analysis (PCA) methods were employed to extract the signal features and reduce the data dimensions before modeling, to make the cumulative contribution rate reach 100%, the first 31 components of the SWT detail data was used as the input data during modeling. Finally, a back propagation (BP) neural network method optimized by the genetic algorithm (GA-BP) was proposed to set up the interface delamination thickness prediction model. As a result, the root correlation coefficient R2 reached over 0.95, the various errors—including the mean square error, mean squared percentage error, and mean absolute percentage error—were less than or equal to 0.53. All these indicators proved that the trained hybrid SWT-PCA-GA-BP model had excellent prediction performance and high accuracy. Finally, this work proposed a novel and convenient interface delamination evaluation method that could also be potentially utilized to evaluate the structural integrity of TBCs.


Introduction
Aero-engine technology is known as the jewel in the industrial crown and is also the focus technology that countries all over the world are pursuing. The continuous improvement of the thrust-to-weight ratio puts forward higher challenges for the refractoriness and corrosion resistance of the hot-end components of aero-engines. Even though the most effective cooling structure technology is used, the extreme temperature of advanced superalloy material is still far from meeting the surface temperature of the turbine blade. Thermal barrier coatings (TBCs) have been widely used as a protective material for hot-end components of aero-engines, owing to their excellent high-temperature resistance, low thermal conductivity, and anti-wear and anti-corrosion properties, which can effectively improve In this work, FDTD numerical simulation method was applied to obtain the terahertz time-domain signals of the TBCs samples with different interface delamination thickness. Nevertheless, the delamination signal was still very weak in terahertz time-frequency waveforms and the conventional Coatings 2020, 10, 859 3 of 12 signal filtering and deconvolution approaches could not distinguish the slight interface delamination. The SWT method was employed to preprocess the raw terahertz time-domain signals and the PCA approach was used to reduce the data dimension of these terahertz time-domain signals processed by SWT. By using the hybrid artificial neural network algorithm, the optimization regression model was set up to predict the thickness of the interface delamination.

Terahertz Simulation Signal Obtained by FDTD Algorithm
As shown in Figure 1, the terahertz waves are incident on the surface of the TBCs, part of the terahertz waves will reflect back to the air in advance, part of the terahertz waves penetrate into the top coat, to reflect and transmit at the interface of delamination repeatedly. The interface delamination could be simplified as the ultrathin air layer inside the TBCs; in theory, the thickness information of the interface delamination could be extracted by analyzing the time difference between the multiple echoes. However, in practice, previous studies (including ours) [15,21] showed that it is very hard to extract the time difference (peak finding) to estimate the interface delamination thickness for the thicknesses in the range of~100 microns; not only that, the peak finding method is difficult for field engineer.
Coatings 2020, 10, x FOR PEER REVIEW 3 of 12 the delamination signal was still very weak in terahertz time-frequency waveforms and the conventional signal filtering and deconvolution approaches could not distinguish the slight interface delamination. The SWT method was employed to preprocess the raw terahertz time-domain signals and the PCA approach was used to reduce the data dimension of these terahertz time-domain signals processed by SWT. By using the hybrid artificial neural network algorithm, the optimization regression model was set up to predict the thickness of the interface delamination.

Terahertz Simulation Signal Obtained by FDTD Algorithm
As shown in Figure 1, the terahertz waves are incident on the surface of the TBCs, part of the terahertz waves will reflect back to the air in advance, part of the terahertz waves penetrate into the top coat, to reflect and transmit at the interface of delamination repeatedly. The interface delamination could be simplified as the ultrathin air layer inside the TBCs; in theory, the thickness information of the interface delamination could be extracted by analyzing the time difference between the multiple echoes. However, in practice, previous studies (including ours) [15,21] showed that it is very hard to extract the time difference (peak finding) to estimate the interface delamination thickness for the thicknesses in the range of ~100 microns; not only that, the peak finding method is difficult for field engineer. The ZrO2 8 wt % Y2O3 (8YSZ) powder (15~45 μm, Beijing Sunspraying Technology Co., Ltd., Beijing, China) was employed to prepare the top coat (spray power: 36 kW, spray distance: 90 mm, power feed rate: 10 L/min, spray gun speed: 15 cm/s), as shown in Figure 2, the complex refractive index of the ceramic coat was tested using a TAS7400TS transmission terahertz time-domain spectroscopy system (Advantest Corporation, Tokyo, Japan). The wavelength was 1560 nm, the pulse width was 300 fs, and the frequency resolution was 1.9 GHz.  The ZrO 2 8 wt % Y 2 O 3 (8YSZ) powder (15~45 µm, Beijing Sunspraying Technology Co., Ltd., Beijing, China) was employed to prepare the top coat (spray power: 36 kW, spray distance: 90 mm, power feed rate: 10 L/min, spray gun speed: 15 cm/s), as shown in Figure 2, the complex refractive index of the ceramic coat was tested using a TAS7400TS transmission terahertz time-domain spectroscopy system (Advantest Corporation, Tokyo, Japan). The wavelength was 1560 nm, the pulse width was 300 fs, and the frequency resolution was 1.9 GHz.
Coatings 2020, 10, x FOR PEER REVIEW 3 of 12 the delamination signal was still very weak in terahertz time-frequency waveforms and the conventional signal filtering and deconvolution approaches could not distinguish the slight interface delamination. The SWT method was employed to preprocess the raw terahertz time-domain signals and the PCA approach was used to reduce the data dimension of these terahertz time-domain signals processed by SWT. By using the hybrid artificial neural network algorithm, the optimization regression model was set up to predict the thickness of the interface delamination.

Terahertz Simulation Signal Obtained by FDTD Algorithm
As shown in Figure 1, the terahertz waves are incident on the surface of the TBCs, part of the terahertz waves will reflect back to the air in advance, part of the terahertz waves penetrate into the top coat, to reflect and transmit at the interface of delamination repeatedly. The interface delamination could be simplified as the ultrathin air layer inside the TBCs; in theory, the thickness information of the interface delamination could be extracted by analyzing the time difference between the multiple echoes. However, in practice, previous studies (including ours) [15,21] showed that it is very hard to extract the time difference (peak finding) to estimate the interface delamination thickness for the thicknesses in the range of ~100 microns; not only that, the peak finding method is difficult for field engineer. The ZrO2 8 wt % Y2O3 (8YSZ) powder (15~45 μm, Beijing Sunspraying Technology Co., Ltd., Beijing, China) was employed to prepare the top coat (spray power: 36 kW, spray distance: 90 mm, power feed rate: 10 L/min, spray gun speed: 15 cm/s), as shown in Figure 2, the complex refractive index of the ceramic coat was tested using a TAS7400TS transmission terahertz time-domain spectroscopy system (Advantest Corporation, Tokyo, Japan). The wavelength was 1560 nm, the pulse width was 300 fs, and the frequency resolution was 1.9 GHz.   In this study, the FDTD Solutions software (Lumerical Solutions Inc., Vancouver, Canada) was applied to set up the simulation model and simulate the propagation process of terahertz waves in the TBCs with various thicknesses of top coat and interface delamination. The incident broadband terahertz Gaussian waves in the range of 0.3-1.5 THz were set vertical to the TBCs surface, the reflection echoes were recorded and analyzed for the TBCs interface delamination evaluation [22,23]. Perfectly matched layer (PML) boundary condition was set in the terahertz incidence Z direction, periodic boundary conditions were set in the X and Y directions, and the complex refractive index shown in Figure 2 was imported into the FDTD model as the terahertz property of ceramic top coat to mimic the actual detection process. As shown in Table 2, the influences of the top coat thickness, the interface delamination thickness, and the roughness are considered comprehensively for modeling and analysis. When setting up the FDTD model, the thickness of YSZ top coat ranges from 100~410 µm (interval: 10 µm) during modeling; the thickness of interface delamination ranges from 1~20 µm (eight kinds of thickness, each thickness occurs four times during modeling); the surface roughness of YSZ top coat ranges from 2~8 µm (four kinds of thickness, each thickness occurs eight times during modeling); the surface and bottom roughness of interface delamination also ranges from 2~8 µm (four kinds of thickness, each thickness occurs eight times during modeling). Hence, a total of 32 FDTD models is obtained and calculated.

Data Processing and Feature Extraction
Wavelet transform technique was used to process the raw terahertz signals obtained by these FDTD models to extract the features. The scaling function ϕ(x) and mother wavelets function f (x) used in the wavelet transform can be expressed as [24,25] here h(n) and g(n) are the impulse responses of low-pass filter and high-pass filter, respectively. Compared with the traditional discrete wavelet transform (DWT) algorithm, SWT is an up-sampling process by inserting zeros between each of the other filter coefficients, rather than down-sampling the signal. The decimation coefficient sequence is not performed at every stage, thus avoiding the translation variance and preserving the more detail signal. SWT decomposes the original signal x(n) into the approximation coefficient vector A j (n) and the detail coefficient vector D j (n), and the data length is equal to the original signal length, the decomposition process is shown in Figure 3.
Compared with the traditional discrete wavelet transform (DWT) algorithm, SWT is an up-sampling process by inserting zeros between each of the other filter coefficients, rather than down-sampling the signal. The decimation coefficient sequence is not performed at every stage, thus avoiding the translation variance and preserving the more detail signal. SWT decomposes the original signal x(n) into the approximation coefficient vector Aj(n) and the detail coefficient vector Dj(n), and the data length is equal to the original signal length, the decomposition process is shown in Figure 3.  The approximation coefficients mainly preserve the low-frequency information of the original signal, and the detail coefficients mainly preserve the high-frequency information of the original signal [26]. The approximation and detail coefficients at the jth layer can be computed by Equations (3) and (4) below, and the decomposition signal at the (j + 1)th layer can be estimated as here f (t) is the original signal, k is a non-zero integer, ϕ(·) is the scale function, f (·) is the wavelet function,ã j,k andd j,k are the approximation coefficients and detail coefficients at the jth layer, respectively.
In this work, based on the SWT, the original raw terahertz time-domain signals were decomposed into the approximation coefficients and detail coefficients. Previous studies showed that the detail coefficients were more suitable to be used to characterize the microscale features during modeling. In this work, the original terahertz data was decomposed at level 2 with the db1 mother wavelet, and the SWT detail data was applied to train the GA-BP network [27].
Principal component analysis (PCA) is an important statistical analysis approach to evaluate the correlation between multiple variables. Through linear transformation, the original data is transformed into a set of linearly independent representations of each dimension, and the main features of the data can be extracted as much as possible while retaining the original variable information as much as possible, and the weights can be calculated [17,28].
Suppose there are s samples, and each sample has b observation indicators. Original data could be expressed as here, b indicators form a b-dimensional random vector, X = (X 1 , X 2 . . . X b ).
Coatings 2020, 10, 859 6 of 12 Standardize the data of each variable to eliminate the influence of dimension, the standardized data matrix is used to calculate the correlation coefficient matrix of the variables according to The standardized correlation coefficient matrix is expressed as On the basis of the equation R ij − λ j E = 0, the b characteristic roots λ j of R ij can be obtained. Then find the corresponding feature vector as The principal component could be expressed as The contribution rate of each principal component (PC) is estimated as The cumulative contribution rate of PCs is estimated as To determine the number of principal components, generally take the first l(l ≤ b) PCs corresponding to the eigenvalues whose cumulative contribution rate reaches 85%.
In this study, the SWT and PCA function were implemented through MATLAB programming. The 32 sets of terahertz time-domain data were processed by SWT. After PCA processing, the contribution rate and the cumulative contribution rate were obtained. These PCs were used as the input features during modeling.

Hybrid Artificial Neural Network Model
The back propagation (BP) neural network is a multilayer feedforward neural network with complex pattern classification capability and excellent multi-dimensional function mapping capability. The BP neural network iterates on the weights and thresholds of neurons by the principle of back propagation, each iteration of weight and threshold will be adjusted toward the direction of the output error reduction [29][30][31]. The BP neural network formula could be expressed as Coatings 2020, 10, 859

of 12
Here, X is the input matrix, W is the weighting matrix, and c is the threshold. The BP neural network mainly contains an input layer, several hidden layers and an output layer. Generally, the triple-layer BP neural network has been able to solve complex nonlinear mapping problems [29,30]. In this work, as shown in Figure 4, the triple-layer BP neural network is applied to set up the prediction model. The minimum error of the training target is set to 0.01, the number of trainings is 1000, and the two transfer functions are respectively set to "tansig" and "logsig". The genetic algorithm (GA) is an approach designed to seek for the optimal solution by simulating the natural evolutionary process. When solving more complicated assorted optimization problems, it is usually applied to acquire better results faster than other algorithms [32,33].
Although the BP neural network can solve complex nonlinear mappings, its prediction performance will be affected by the initial weight and threshold, resulting in a large gap in the prediction performance of multiple training. Therefore, as shown in Figure 5, GA is applied to optimize the initial values and the detailed execution steps are as follows [34][35][36]: • Determine the basic structure of BP neural network, including the number of the input neurons, the hidden neurons, the output neurons, and the hidden layers.
where S is the code length, input S , hidden S and output S are the input neuron number, hidden neuron number and output neuron number, respectively.
• Design the degree of fitness function. The fitness function is employed to measure the merit degree. In this work, the degree of fitness function was designed based on the prediction index mean squared error. • Define the genetic algorithm parameters and initialize the population. The optimization algorithm parameters include the population size, the iteration number, the variation probability, and the crossover probability. • Estimate the fitness value of the population according to the fitness function designed in Step (3).
• Use the fitness value as the basis for selection, crossing, and variation of the population. If the termination condition is met, the calculation is terminated; if not, return back to Step (5) until the termination condition is achieved. • Decode the optimal individuals in the population as initial weights and thresholds and train the BP model. • Test the BP model performance after training completion. The genetic algorithm (GA) is an approach designed to seek for the optimal solution by simulating the natural evolutionary process. When solving more complicated assorted optimization problems, it is usually applied to acquire better results faster than other algorithms [32,33].
Although the BP neural network can solve complex nonlinear mappings, its prediction performance will be affected by the initial weight and threshold, resulting in a large gap in the prediction performance of multiple training. Therefore, as shown in Figure 5, GA is applied to optimize the initial values and the detailed execution steps are as follows [34][35][36]: • Determine the basic structure of BP neural network, including the number of the input neurons, the hidden neurons, the output neurons, and the hidden layers.

•
Encoding. The formula for calculating the length of the code can be expressed as S = S input × S hidden + S hidden × S output + S hidden + S output (15) where S is the code length, S input , S hidden and S output are the input neuron number, hidden neuron number and output neuron number, respectively. • Design the degree of fitness function. The fitness function is employed to measure the merit degree. In this work, the degree of fitness function was designed based on the prediction index mean squared error.

•
Define the genetic algorithm parameters and initialize the population. The optimization algorithm parameters include the population size, the iteration number, the variation probability, and the crossover probability.

•
Estimate the fitness value of the population according to the fitness function designed in Step (3).

•
Use the fitness value as the basis for selection, crossing, and variation of the population. If the termination condition is met, the calculation is terminated; if not, return back to Step (5) until the termination condition is achieved.

•
Decode the optimal individuals in the population as initial weights and thresholds and train the BP model.

•
Test the BP model performance after training completion. In this work, the prediction accuracy and reliability of the GA-BP algorithm were estimated via four parameters: root correlation coefficient (R 2 ), mean squared error (MSE), mean squared percentage error (MSPE), and mean absolute percentage error (MAPE). Their definitions can be expressed as here m is the number of samples, i Y is the actual value of interface delamination thickness, ˆi Y is the predicted value of interface delamination thickness obtained by GA-BP model.

Results and Discussion
As shown in Figure 6, for instance, the terahertz time-domain signals of sample 1 and sample 16 obtained by FDTD calculation and SWT processing are compared with each other. Comparison results show that both the variations of the thickness and the roughness will lead to the change of the time-domain wave on the amplitude and the optical delay, owing to the existence of interface delamination, the ideal time differences for the delamination thickness 1 and 20 μm depicted in Figure 6 should be 0.0067 and 0.1333 ps, respectively. If the peak finding method is applied to estimate the delamination thickness, it is nearly impossible. Nevertheless, SWT detail coefficients have kept the main characteristic peak position unchanged and also played the role of waveform baseline adjustment. Hence, the SWT approach has the potential to assist a machine learning model to distinguish the thin interface delamination layer and previous studies had proven its effectiveness [15,22]. In this work, the prediction accuracy and reliability of the GA-BP algorithm were estimated via four parameters: root correlation coefficient (R 2 ), mean squared error (MSE), mean squared percentage error (MSPE), and mean absolute percentage error (MAPE). Their definitions can be expressed as here m is the number of samples, Y i is the actual value of interface delamination thickness,Ŷ i is the predicted value of interface delamination thickness obtained by GA-BP model.

Results and Discussion
As shown in Figure 6, for instance, the terahertz time-domain signals of sample 1 and sample 16 obtained by FDTD calculation and SWT processing are compared with each other. Comparison results show that both the variations of the thickness and the roughness will lead to the change of the time-domain wave on the amplitude and the optical delay, owing to the existence of interface delamination, the ideal time differences for the delamination thickness 1 and 20 µm depicted in Figure 6 should be 0.0067 and 0.1333 ps, respectively. If the peak finding method is applied to estimate the delamination thickness, it is nearly impossible. Nevertheless, SWT detail coefficients have kept the main characteristic peak position unchanged and also played the role of waveform baseline adjustment. Hence, the SWT approach has the potential to assist a machine learning model to distinguish the thin interface delamination layer and previous studies had proven its effectiveness [15,22]. As shown in Figure 7, to make the cumulative contribution rate reach 100%, it is found that the cumulative contribution rate of the first 31 PCs of the SWT detail data. Finally, the data dimension is reduced from 32 × 3840 to 32 × 31, these dimension-reduced data are used as the input for the BP and GA-BP models to evaluate the interface delamination thickness. As shown in Figure 8, the GA-BP model is trained by selecting twenty-six random data sets, it could be seen from the fitness evolution curve that the training error of the parameter reached the minimum value and fulfilled the trained requirement when the training model evolved to the 433 generations, respectively.  As shown in Figure 7, to make the cumulative contribution rate reach 100%, it is found that the cumulative contribution rate of the first 31 PCs of the SWT detail data. Finally, the data dimension is reduced from 32 × 3840 to 32 × 31, these dimension-reduced data are used as the input for the BP and GA-BP models to evaluate the interface delamination thickness. As shown in Figure 7, to make the cumulative contribution rate reach 100%, it is found that the cumulative contribution rate of the first 31 PCs of the SWT detail data. Finally, the data dimension is reduced from 32 × 3840 to 32 × 31, these dimension-reduced data are used as the input for the BP and GA-BP models to evaluate the interface delamination thickness. As shown in Figure 8, the GA-BP model is trained by selecting twenty-six random data sets, it could be seen from the fitness evolution curve that the training error of the parameter reached the minimum value and fulfilled the trained requirement when the training model evolved to the 433 generations, respectively.  As shown in Figure 8, the GA-BP model is trained by selecting twenty-six random data sets, it could be seen from the fitness evolution curve that the training error of the parameter reached the minimum value and fulfilled the trained requirement when the training model evolved to the 433 generations, respectively. As shown in Figure 7, to make the cumulative contribution rate reach 100%, it is found that the cumulative contribution rate of the first 31 PCs of the SWT detail data. Finally, the data dimension is reduced from 32 × 3840 to 32 × 31, these dimension-reduced data are used as the input for the BP and GA-BP models to evaluate the interface delamination thickness. As shown in Figure 8, the GA-BP model is trained by selecting twenty-six random data sets, it could be seen from the fitness evolution curve that the training error of the parameter reached the minimum value and fulfilled the trained requirement when the training model evolved to the 433 generations, respectively.  To compare and test the prediction accuracies and reliabilities of the simple BP and the hybrid GA-BP models, their performances are verified via the remaining six random samples. As shown in Figure 9, the black, green, and red symbols represent the actual, BP predicted, and GA-BP predicted values of the thickness of interface delamination, and the results show that the variation trend of their prediction results is basically consistent with each other.
Coatings 2020, 10, x FOR PEER REVIEW 10 of 12 To compare and test the prediction accuracies and reliabilities of the simple BP and the hybrid GA-BP models, their performances are verified via the remaining six random samples. As shown in Figure 9, the black, green, and red symbols represent the actual, BP predicted, and GA-BP predicted values of the thickness of interface delamination, and the results show that the variation trend of their prediction results is basically consistent with each other. For the sake of further comparison between the BP and GA-BP models, as shown in Table 3, their accuracies and reliabilities could be seen clearly, the R 2 value of the GA-BP model has reached over 0.95, which is greater than the R 2 value of the BP model; the values of all these error performance indicators (MSE, MSPE, MAPE) of the GA-BP model are kept very low (≤0.5300), which are lower than the various errors of the BP model (≥1.8636). All these proved that the GA-BP model showed the higher accuracy and reliability in predicting the thickness of interface delamination; hence, the hybrid GA-BP algorithm model could satisfy the needs of in actual interface delamination evaluation.

Conclusions
In this study, the terahertz nondestructive technology combined with the hybrid machine learning algorithm was applied to estimate the thickness of the interface delamination in the early stage. Major and useful conclusions are summarized as follows: • It was found that FDTD model could be used to simulate the propagation process of terahertz waves in the TBCs with various thicknesses of interface delamination. The simulated terahertz time-domain signals after SWT processing showed that the detail coefficient kept the main characteristic peak position of raw signals and also adjusted waveform baseline. • The PCA approach could be effectively used to reduce the SWT data dimension to improve the computational speed during modeling, the top 31 PCs were chosen instead of the original SWT signals as the input data during machine learning modeling, owing to their cumulative contribution rate (100%). • To get the prediction accuracy and reliability of the BP model improved, the GA algorithm was employed to optimize the BP model. Finally, the hybrid SWT-PCA-GA-BP regression model with high R 2 value (>0.95) and low error values (≤0.5300) were obtained, the hybrid SWT-PCA-GA-BP model showed its high accuracy and reliability in predicting the thickness of interface delamination, hence, it could be potentially used to monitor the TBCs delamination progression starting from the early stage of subcritical delamination crack propagation. For the sake of further comparison between the BP and GA-BP models, as shown in Table 3, their accuracies and reliabilities could be seen clearly, the R 2 value of the GA-BP model has reached over 0.95, which is greater than the R 2 value of the BP model; the values of all these error performance indicators (MSE, MSPE, MAPE) of the GA-BP model are kept very low (≤0.5300), which are lower than the various errors of the BP model (≥1.8636). All these proved that the GA-BP model showed the higher accuracy and reliability in predicting the thickness of interface delamination; hence, the hybrid GA-BP algorithm model could satisfy the needs of in actual interface delamination evaluation. Table 3. Prediction performance of the BP and GA-BP models tested by the six remaining random samples.

Conclusions
In this study, the terahertz nondestructive technology combined with the hybrid machine learning algorithm was applied to estimate the thickness of the interface delamination in the early stage. Major and useful conclusions are summarized as follows: • It was found that FDTD model could be used to simulate the propagation process of terahertz waves in the TBCs with various thicknesses of interface delamination. The simulated terahertz time-domain signals after SWT processing showed that the detail coefficient kept the main characteristic peak position of raw signals and also adjusted waveform baseline.

•
The PCA approach could be effectively used to reduce the SWT data dimension to improve the computational speed during modeling, the top 31 PCs were chosen instead of the original SWT signals as the input data during machine learning modeling, owing to their cumulative contribution rate (100%).

•
To get the prediction accuracy and reliability of the BP model improved, the GA algorithm was employed to optimize the BP model. Finally, the hybrid SWT-PCA-GA-BP regression model with high R 2 value (>0.95) and low error values (≤0.5300) were obtained, the hybrid SWT-PCA-GA-BP model showed its high accuracy and reliability in predicting the thickness of interface delamination, hence, it could be potentially used to monitor the TBCs delamination progression starting from the early stage of subcritical delamination crack propagation. • Additionally, this novel terahertz nondestructive technology combined hybrid artificial neural network would be potentially applied in the future to monitor and improve the service life of TBCs.