Feasibility for the Recovery of Excavated Soils in Compressed Earth Blocks as a Sustainable Building Material

: Soil is continuously excavated for development activities in urban and rural areas and treated as waste. This study investigates the characteristics of urban soils excavated from earthworks of buildings in the Brittany region of France for their perspective reuse in earthen construction materials to valorize soil waste and provide a sustainable building material locally. Excavated soil from earthwork activities was taken from the Brittany region of France from three different locations. Soil suitability for compressed earth blocks was investigated based on their granulometry, consistency limits, and mineralogy. Finally, compressed earth blocks with dimensions of 4 × 4 × 16 cm 3 were manufactured with different formulations and compacted dynamically. Flexural and compressive strength tests were performed on bricks to observe their mechanical behavior. Grain size analysis of soil samples shows that the percentage of clay in the landﬁll stockpile of excavated soils varies between 13% and 16%, while at some local sites, the percentage of clay goes up to 57%. The grain size of soils varies from the recommended zone. The plasticity of soil samples ranges from 17.3% to 20.4%. The plasticity index and clay content of the soil show that these soils are inactive clays with a lesser possibility of swelling and shrinkage. Mineralogical analysis of soil shows the absence of water-sensitive clay minerals, while quartz, kaolinite, and illite are major minerals present in soils. Linear shrinkage in bricks ranges from 0.6% to 2.2% and is considerably higher for clayey soils. Mechanical testing of earth bricks shows that the compressive strength of earth blocks ranges from 0.92 MPa to 2.22 MPa while the ﬂexural strength ranges from 0.25 to 0.74 MPa. A mixture of sandy and clayey soils shows good strength due to improved granulometry. Earth bricks with soils from some stockpiles, excavation sites, and soil mixture show compressive strength higher than 1 MPa, which is recommended strength by international standards, and offer the opportunity to produce sustainable building materials locally.


Introduction
Infrastructure and development work generate a considerable amount of excavated soil from different operations, such as the installation of pipelines, excavations of trenches and tunnels, roads, and infrastructure projects. Excavated soil is treated as waste and dumped into land sites. Nearly half of the landfill sites are occupied by excavated soil [1]. The construction and public work sector in France produce nearly 231 million tons of waste every year, mainly in the form of excavated soils and demolition material [2]. Nearly 45 million tons of are to be excavated from the Grand Paris Express project (Paris, France) alone [3] Excavated soil storage in stockpiles on land sites is costly. Furthermore, increasing earth blocks, are manufactured based on the characteristics of excavated material and local climatic conditions [22].
Earth bricks can be stabilized with the addition of binders (lime, cement, gypsum, geopolymers) to increase the strength of bricks and water resistance as earth bricks have low strength and are sensitive to water and weathering actions, such as rain, snow, etc. [20,23,24]. However, binders have a higher economic and environmental cost. Furthermore, stabilized earth blocks reversibility in the form of natural soil is not possible [25]. The addition of natural fibers is also helpful to increase the strength of bricks as fibers act as reinforcement, and their distribution parallel the axis of bricks significantly increases the tensile strength and transforms ductile behavior into brittle one by increasing the toughness of bricks [26]. Soil with suitable granulometry for bricks also minimizes the need for binders as natural binders, such as clay, are helpful to bind the soil particles and increase the strength of bricks [27]. Therefore, a certain amount of clay is essential to increase the strength of bricks. In the case of earth wall construction, the presence of sand, silt, clay, and gravel in soil samples is also important. Coarse soil particles having a diameter above 5 mm to 10 mm are not suitable for earth bricks as the compressive strength of earthen bricks decreases with the increasing size of coarse particles [28,29]. Furthermore, the compaction of earth blocks is helpful to increase the strength and durability of bricks. The compaction of earth blocks increases density and decreases their water absorption capacity by eliminating pores. Compaction of earth bricks can be achieved with static compaction, dynamic compaction, and vibrations [30]. The manufacturing and labor cost of small-scale blocks is considerably higher. The manufacturing cost further increases with the addition of a binder. However, the manufacturing and labor cost decreases with increasing block size and automation. Large-size compressed earth blocks stabilized with compaction can have a similar cost to concrete with a much lower carbon footprint. In addition, excavated soil dumping involves transportation and land costs. A substantial amount of soil is excavated every year in the Brittany region of France from earthworks in construction activities. Gendrot (public work company) excavates 200,000 m 3 of soil and inert spoil in the Brittany region of France. France has planned an extended producer responsibility tax, which encourages the producer to look for recovery solutions to avoid this tax.
The objective of this study is to investigate the characteristics of excavated soils and examine the feasibility of the recovery of this material in compressed earth blocks for nonstructural building applications. Laboratory-scale earth blocks will be manufactured without the addition of a binder for the reversibility of soil.

Materials and Method
Inert soil samples are taken from the Brittany region around Rennes city. The soil samples selected are the most representative surface soils of the region. In terms of geology, the Rennes basin and the surrounding area are part of a vast plateau in central Brittany. Most of it is made up of schists. There are virtually no rock outcrops. These schists are more or less weathered to provide a clayey subsoil and are sometimes covered by aeolian silts or loess (west of Rennes). The overlying soils can be described as silty-clayey [31].
The soil was excavated after removing vegetative soil. Typically, the excavated soil comes from suburban areas and covers soils to an average depth of 1 m. The soil samples were taken from excavated soil deposits belonging to the Gendrot public works company but are representative of regularly stored soil from various regional construction projects. Sampling sites are Bourg de Compte (BDC) and Cesson Redwood (Cesson) storage site and the Calma earthwork site. Excavated soil from the BDC and Cesson sites is crushed and sieved into a fraction of 0/4 mm with a crush/sieve system. Soil excavation from a site is shown in Figure 1a. Figure 1b shows the crushing/sieving of soil, and Figure 1c shows the extracted soil stockpile.
Physicochemical and mineralogical characteristics of excavated soils were determined to observe their suitability for earth bricks. These characteristics include granulometry, moisture content, particle density, Atterberg limits, methylene blue value, organic matter, Environments 2023, 10, 131 4 of 17 carbonate content, and minerals such as quartz, kaolinite, calcite, etc. The grain size of soil samples is important for their reuse in earthen materials. Soil samples were passed through sieves of 2 mm, and the granulometry of soil samples was determined with laser granulometry by following French standards [32] to observe the percentage of clay, silt, and sand. Atterberg limits of soil are important for their reuse in building materials and road applications for molding and compaction of the soil. Liquidity limits of soils were determined with the Casagrande test, while plasticity of soil was observed by the failure of soil roll in accordance with the French standard [33]. Methylene blue value (MBV) was determined by the French standard [34] to observe the presence of clay and the behavior of soil. Organic matter in soil significantly influences its strength and approach to the treatment of soil. The organic matter of studied soils was determined by burning the soil at 550 • C in accordance with the French standard [35]. The particle density of soil samples was determined with a helium pycnometer, model AccuPyc 1330 [36]. The test was repeated 3 times on each soil sample to obtain an average value.
Environments 2023, 10, x FOR PEER REVIEW 4 of 18 is shown in Figure 1a. Figure 1b shows the crushing/sieving of soil, and Figure 1c shows the extracted soil stockpile. Physicochemical and mineralogical characteristics of excavated soils were determined to observe their suitability for earth bricks. These characteristics include granulometry, moisture content, particle density, Atterberg limits, methylene blue value, organic matter, carbonate content, and minerals such as quartz, kaolinite, calcite, etc. The grain size of soil samples is important for their reuse in earthen materials. Soil samples were passed through sieves of 2 mm, and the granulometry of soil samples was determined with laser granulometry by following French standards [32] to observe the percentage of clay, silt, and sand. Atterberg limits of soil are important for their reuse in building materials and road applications for molding and compaction of the soil. Liquidity limits of soils were determined with the Casagrande test, while plasticity of soil was observed by the failure of soil roll in accordance with the French standard [33]. Methylene blue value (MBV) was determined by the French standard [34] to observe the presence of clay and the behavior of soil. Organic matter in soil significantly influences its strength and approach to the treatment of soil. The organic matter of studied soils was determined by burning the soil at 550 °C in accordance with the French standard [35]. The particle density of soil samples was determined with a helium pycnometer, model AccuPyc 1330 [36]. The test was repeated 3 times on each soil sample to obtain an average value.
Proctor test was performed to observe the optimum moisture content and maximum dry density of soil as optimum moisture content of the soil is essential to achieve maximum densification of soil and increase its load-bearing capacity. Compaction of soil in building materials increases the compressive and tensile strength of building composites. The optimum moisture content of soil samples was determined with a modified Proctor test [37] by applying compaction energy of 600 kN.m/m 3 to achieve the maximum dry density. XRD analyses were carried out to identify and determine the mineral phases. The analyses were performed by using a D8-Advance Bruker-AXS diffractometer with a Nifiltered CuKα radiation at 40 kV and 40 mA. Quantitative phase analysis based on reference intensity ratio values was performed on randomly oriented soil powders with a step length of 0.5° and a scan speed of 0.014°/s over the range 3°-70°2θ for the whole soil composition. The uncertainty was estimated to be ±5%. The interpretations of the data obtained were performed using the DIFFRAC EVA v4.2 (©Bruker AXS) software. Proctor test was performed to observe the optimum moisture content and maximum dry density of soil as optimum moisture content of the soil is essential to achieve maximum densification of soil and increase its load-bearing capacity. Compaction of soil in building materials increases the compressive and tensile strength of building composites. The optimum moisture content of soil samples was determined with a modified Proctor test [37] by applying compaction energy of 600 kN.m/m 3 to achieve the maximum dry density. XRD analyses were carried out to identify and determine the mineral phases. The analyses were performed by using a D8-Advance Bruker-AXS diffractometer with a Ni-filtered CuKα radiation at 40 kV and 40 mA. Quantitative phase analysis based on reference intensity ratio values was performed on randomly oriented soil powders with a step length of 0.5 • and a scan speed of 0.014 • /s over the range 3 • -70 • 2θ for the whole soil composition. The uncertainty was estimated to be ±5%. The interpretations of the data obtained were performed using the DIFFRAC EVA v4.2 (©Bruker AXS) software.

Sample Preparation
Manufacturing of earth blocks includes mixing of soil, molding, compaction, and drying. Soil samples were dried in an oven at 50 • C for 24 h. Dried soil samples were crushed, ground, and passed through a 2 mm sieve for their reuse in compressed earth blocks. Earth blocks were manufactured with 5 different soil compositions to optimize the strength of bricks. The soil compositions studied are shown in Table 1. The soil mixture was prepared with the addition of optimum moisture content and molded into prismatic specimens of 4 × 4 × 16 cm 3 for flexural and compressive strength tests based on French standards for mortars [38]. A total of 450 g of soil was mixed with optimum moisture content, which is commonly used to mix soils to achieve maximum densification through compaction [39,40]. Prismatic molds were oiled to decrease the adhesion of soil to molds. The soil mixture was filled into molds in two layers [41] and compacted with dynamic loading by applying Proctor normal energy of 600 kN.m/m 3 with repeated strokes of falling mass. With dynamic compaction of bricks, it is easier to control compaction energy-it is one of the efficient techniques to remove the voids and increase the strength of bricks [42,43]. After compaction of the first layer of soil, groves were made on the first layer of soil to make it rough and increase bonding between the two layers. Strong bonding between layers increases the strength of earth bricks. The bonding of layers in the case of mortar specified in the standards is different from the cement paste which when poured in the mold is homogenized and has no problem with adhesion. Compaction tools and groves on the soil layer can be seen in Figure 2a. Excessive soil on the brick surface after compaction was trimmed to maintain a height of 4 cm. Compacted bricks were unmolded and dried at a low temperature in the oven at 40 • C to rest near the natural drying temperature. Demolded compressed earth blocks can be seen in Figure 2b.

Testing of Earth Bricks
The mechanical behavior of earth blocks was investigated with flexural and compressive strength tests. The flexural strength of earth bricks (indirect tensile strength) was determined with a three-point bending test [44] using a Shimadzu AGS-X model machine with a 50 kN sensor at a displacement rate of 0.5 mm/min. Figure 3 shows the flexural strength testing of compressed earth blocks with the BDC soil sample along with the flexural load-deflection curve. The flexural load was applied perpendicular to the layer interface of earth bricks. During the flexural loading in Figure 3a, cracks started from the bottom of the brick and propagated slowly upward before failure. Figure 3b shows that unreinforced bricks do not support the load after failure as they have very little toughness.

Testing of Earth Bricks
The mechanical behavior of earth blocks was investigated with flexural and compressive strength tests. The flexural strength of earth bricks (indirect tensile strength) was determined with a three-point bending test [44] using a Shimadzu AGS-X model machine with a 50 kN sensor at a displacement rate of 0.5 mm/min. Figure 3 shows the flexural strength testing of compressed earth blocks with the BDC soil sample along with the flexural load-deflection curve. The flexural load was applied perpendicular to the layer interface of earth bricks. During the flexural loading in Figure 3a, cracks started from the bottom of the brick and propagated slowly upward before failure. Figure 3b shows that unreinforced bricks do not support the load after failure as they have very little toughness.
After the flexural strength test, two halves of BDC brick were cut into cubes of 4 × 4 × 4 cm 3 with an electric cutter with a fine blade. Brick sections were cut into cubes contrary to the norm's specifications due to compressive machine adaptability with cubic blocks. Cutting of bricks introduces the microcracks and readjustment of particles, which decreases the strength of bricks. However, compressive load-deflection graphs show no oscillation indicating that there was no significant cracking. The compressive strength of earth bricks was observed by applying compressive load at the top of cubic specimens. Compressive strength testing of the BDC brick cube can be seen in Figure 4a. Figure 4b shows the compressive load-deflection behavior of unreinforced compressed earth blocks. termined with a three-point bending test [44] using a Shimadzu AGS-X model machine with a 50 kN sensor at a displacement rate of 0.5 mm/min. Figure 3 shows the flexural strength testing of compressed earth blocks with the BDC soil sample along with the flexural load-deflection curve. The flexural load was applied perpendicular to the layer interface of earth bricks. During the flexural loading in Figure 3a, cracks started from the bottom of the brick and propagated slowly upward before failure. Figure 3b shows that unreinforced bricks do not support the load after failure as they have very little toughness. After the flexural strength test, two halves of BDC brick were cut into cubes of 4 × 4 × 4 cm 3 with an electric cutter with a fine blade. Brick sections were cut into cubes contrary to the norm's specifications due to compressive machine adaptability with cubic blocks. Cutting of bricks introduces the microcracks and readjustment of particles, which decreases the strength of bricks. However, compressive load-deflection graphs show no oscillation indicating that there was no significant cracking. The compressive strength of earth bricks was observed by applying compressive load at the top of cubic specimens. Compressive strength testing of the BDC brick cube can be seen in Figure 4a. Figure 4b shows the compressive load-deflection behavior of unreinforced compressed earth blocks.

Characteristics of Excavated Soils
The physicochemical and mineralogical characteristics of soil samples were determined by different tests. The results are summarized in Table 2. Note: Wopt = optimum moisture content; ρopt = optimum moisture density; PL = plasticity limit; LL = liquidity limit; Wi = initial moisture content; MBV = methylene blue value; ρs = particles density; OM = organic matter.
The grain size distribution of soils is shown in Table 3. Table 3. Grain size distribution of soil.

Characteristics of Excavated Soils
The physicochemical and mineralogical characteristics of soil samples were determined by different tests. The results are summarized in Table 2. Note: Wopt = optimum moisture content; ρ opt = optimum moisture density; PL = plasticity limit; LL = liquidity limit; Wi = initial moisture content; MBV = methylene blue value; ρ s = particles density; OM = organic matter.
The grain size distribution of soils is shown in Table 3.  Granulometry of soil shows that BDC and Cesson soils have higher sand content while Calma soil has higher clay content. According to the USDA soil classification system [45], BDC and Cesson soils are sandy loam while Calma is clayey soil. The grading coefficient of Calma soils is between 1 and 3, which means that this soil is well graded while the other soils are poorly graded [46]. Soils with a higher percentage of fine particles usually have higher plasticity. Significant clay quantity is essential in bricks to ensure the plasticity and bonding of soil particles. However, excessive clay leads to shrinkage, cracks, and expansion of earth blocks in their interaction with water. The suitability of the Brittany region soils for earth bricks with granulometry in accordance with the French standard [47] and recommendations of Houben and Guillaud [48] is shown in Figure 5. plasticity and bonding of soil particles. However, excessive clay leads to shrinkage, cracks, and expansion of earth blocks in their interaction with water. The suitability of the Brittany region soils for earth bricks with granulometry in accordance with the French standard [47] and recommendations of Houben and Guillaud [48] is shown in Figure 5. It can be observed from Figure 5 that Cesson soils are close to the zones recommended for adobe bricks. Clay and silt content in Cesson soils is slightly lower than the recommended zone. BDC soils have significantly lower clay and silt content and higher sand content. A sufficient quantity of fine particles is necessary for the plasticity of soils for their reuse in earth bricks. On the other hand, Calma soils have a higher percentage of fine particles and tend to move away from the zones recommended for earthen construction. A higher percentage of fine particles leads to excessive shrinkage and cracking during the drying of bricks. Therefore, for balanced granulometry, a mixture of BDC and Cesson soil with Calma soils can be interesting and push the soil samples inside the zones recommended for earth bricks in Figure 5.
Liquidity and plasticity limits of soil are also helpful in the analysis of the soil suitability for earth bricks. Clayey soils have usually higher plasticity. The liquidity and plasticity s of soils in Table 2 are the highest for Calma soils, which are clayey. The plasticity of sandy soil (Cesson) is the lowest. For molding of bricks, such as adobe and cob, molding moisture content of soil used varies between the liquidity and plasticity limit of soil. Figure 6 defines the zones suitable for earth bricks based on their Atterberg limits. It can be observed from Figure 5 that Cesson soils are close to the zones recommended for adobe bricks. Clay and silt content in Cesson soils is slightly lower than the recommended zone. BDC soils have significantly lower clay and silt content and higher sand content. A sufficient quantity of fine particles is necessary for the plasticity of soils for their reuse in earth bricks. On the other hand, Calma soils have a higher percentage of fine particles and tend to move away from the zones recommended for earthen construction. A higher percentage of fine particles leads to excessive shrinkage and cracking during the drying of bricks. Therefore, for balanced granulometry, a mixture of BDC and Cesson soil with Calma soils can be interesting and push the soil samples inside the zones recommended for earth bricks in Figure 5.
Liquidity and plasticity limits of soil are also helpful in the analysis of the soil suitability for earth bricks. Clayey soils have usually higher plasticity. The liquidity and plasticity  Table 2 are the highest for Calma soils, which are clayey. The plasticity of sandy soil (Cesson) is the lowest. For molding of bricks, such as adobe and cob, molding moisture content of soil used varies between the liquidity and plasticity limit of soil. Figure 6 defines the zones suitable for earth bricks based on their Atterberg limits. It can be seen in Figure 6 that BDC, Cesson, and Calma soils are within the zone recommended for compressed earth blocks and rammed earth. The plasticity index of BDC, Cesson, and Calma soil is lower than 12, which means that these soils are less plastic silts [49]. Table 3 shows that activity of clay is below 0.75, which means the soils are inactive clays with less swelling and shrinkage potential. XRD analysis of soils in Table 4 also confirms the absence of swelling clays in soil samples.
BDC, Cesson, and Calma have organic matter, which is below 10, and according to French standards [50] these soils are classified as low organic soils. Cesson and Calma soils have a higher percentage of organic matter than BDC soil. Higher organic matter in the soil makes soil unsuitable for building applications, such as earth bricks, as higher organic matter influences the cohesion and molding of soil, decreases the strength of bricks, and leads to higher shrinkage and biodeterioration in bricks [27]. Higher organic soils require treatment with a binder, such as lime, cement, or geopolymers, to improve their mechanical properties [42]. Table 2 shows that the solid particle density of soil samples ranges from 2.6 to 2.7 g/cm 3 , which is within the common range of density of soils from 2.55 to 2.7 g/cm 3 . The density of soil is influenced by the presence of minerals in soils as the density of quartz is 2.65 g/cm 3 , feldspar 2.65 to 2.8, and micas 2.7 to 3.3 g/cm 3 [51]. The optimum molding moisture content of Calma soils is the highest as this soil has a higher percentage of clay particles. The optimum moisture content of the soil is helpful to achieve maximum densification of soil samples through compaction. MBV value of Cesson and BDC soil samples shows that these soils are sandy silts and water-sensitive soils as their MBV value is below 1.5. Calma soil has an MBV value of 1.6, which is sandy-clayey soil with low plasticity [49]. Based on granulometry, plasticity index, and methylene blue value, soil samples were classified by the French standard [52]. Soil classification shows that BDC and Cesson soils are category B5 soils, which are silty sand soils while Calma soils are within the category of A1 soils, which are low plasticity soils [49].
The mineralogy of soil samples was investigated with X-ray diffraction (XRD) analysis. The diffractogram of soil samples shows that silicate minerals are dominant in all soil samples, which include clay (illite, kaolinite), feldspar (albite), mica (biotite), quartz, and It can be seen in Figure 6 that BDC, Cesson, and Calma soils are within the zone recommended for compressed earth blocks and rammed earth. The plasticity index of BDC, Cesson, and Calma soil is lower than 12, which means that these soils are less plastic silts [49]. Table 3 shows that activity of clay is below 0.75, which means the soils are inactive clays with less swelling and shrinkage potential. XRD analysis of soils in Table 4 also confirms the absence of swelling clays in soil samples. BDC, Cesson, and Calma have organic matter, which is below 10, and according to French standards [50] these soils are classified as low organic soils. Cesson and Calma soils have a higher percentage of organic matter than BDC soil. Higher organic matter in the soil makes soil unsuitable for building applications, such as earth bricks, as higher organic matter influences the cohesion and molding of soil, decreases the strength of bricks, and leads to higher shrinkage and biodeterioration in bricks [27]. Higher organic soils require treatment with a binder, such as lime, cement, or geopolymers, to improve their mechanical properties [42]. Table 2 shows that the solid particle density of soil samples ranges from 2.6 to 2.7 g/cm 3 , which is within the common range of density of soils from 2.55 to 2.7 g/cm 3 . The density of soil is influenced by the presence of minerals in soils as the density of quartz is 2.65 g/cm 3 , feldspar 2.65 to 2.8, and micas 2.7 to 3.3 g/cm 3 [51]. The optimum molding moisture content of Calma soils is the highest as this soil has a higher percentage of clay particles. The optimum moisture content of the soil is helpful to achieve maximum densification of soil samples through compaction. MBV value of Cesson and BDC soil samples shows that these soils are sandy silts and water-sensitive soils as their MBV value is below 1.5. Calma soil has an MBV value of 1.6, which is sandy-clayey soil with low plasticity [49]. Based on granulometry, plasticity index, and methylene blue value, soil samples were classified by the French standard [52]. Soil classification shows that BDC and Cesson soils are category B5 soils, which are silty sand soils while Calma soils are within the category of A1 soils, which are low plasticity soils [49].
The mineralogy of soil samples was investigated with X-ray diffraction (XRD) analysis. The diffractogram of soil samples shows that silicate minerals are dominant in all soil samples, which include clay (illite, kaolinite), feldspar (albite), mica (biotite), quartz, and chlorites (chamosite, clinochlore). The presence of carbonates is low, as only BDC soils show the presence of calcite. XRD diffractogram of soil samples is shown in Figure 7.
XRD analysis helps to see the presence of different minerals in the soil. Different types of clay minerals help to assess the swelling and shrinkage potential of earth bricks. Furthermore, the presence of minerals, such as carbonates, is helpful to determine a suitable binder to stabilize the soil. The percentage of different minerals in soil samples is given in Table 4.
Calma soils have a high percentage of clay minerals. The clay and sand content of soils determined with laser granulometry and XRD are consistent. However, for BDC soils, sand content was overestimated by laser granulometry. Quantitative analysis with the XRD test provides a more comprehensive picture of soil mineralogy and the percentage of clay minerals. An important clay mineral identified in soil samples is illite along with chlorites (chamosite and clinochlore). Illite clay is good for shaping and drying bricks. Illite and chlorite clays demonstrate small volumetric changes in their interaction with water contrary to montmorillonite and smectite clays, which have very good cohesion and a tendency to swell during their interaction with water. Swelling and shrinkage of bricks on wetting and drying lead to crack growth, which is undesirable for construction materials [39,53]. Quartz (SiO 2 ) and feldspar minerals are other major minerals in soil samples, and these are the most common mineral in the earth's crust. The presence of calcite is negligible in Calma and Cesson soils while its percentage is 4.1% in BDC soils. Calcium carbonate acts as a cementing agent in soils by increasing their compressive and shear strength [54].

Physical Characteristics of Earth Bricks
Earth bricks were manufactured with dynamic compaction and dried in an oven at 40 • C. The drying of bricks lasted for 3 to 4 days. The dry density of earth bricks was measured with the ratio of mass and volume of bricks [55] and the linear shrinkage of earth bricks was measured by observing the shrinkage in bricks specimens during drying before mechanical testing. These characteristics of bricks are important for their reuse as construction material for earthen structures. The physical characteristics of compressed earth blocks are shown in Table 5. Table 5 shows that the density of earth bricks ranges from 1661 kg/m 3 to 1718 kg/m 3 . Calma soils have the lowest density as they are clayey soil. Small pores in clayey particles contribute to the low density of clayey soil. Densification of soil by dynamic or energycontrolled compaction helps to obtain better material homogeneity. The procedure needs to be formalized and implemented in a production cycle. This procedure could be adapted to larger brick sizes or even metric-sized walls. The dry density of compressed earth blocks in the literature varies from 1500 to 2000 kg/m 3 and is lower that than of concrete. The density of bricks is influenced by compaction, the addition of binder, and reinforcement of bricks with natural fibers as the addition of natural fibers decreases the density of bricks [56][57][58].    Linear shrinkage in Calma bricks is around 2.2%, which is considerably high. Sandy soils, such as Cesson, have low shrinkage. Higher clay content and molding moisture content of Calma soils are the reason behind higher shrinkage. Similar behavior was observed in the literature studies [59].

Flexural Strength of Earth Bricks
The flexural strength of earth bricks was determined with a 3-point bending test. The results relating to deflection under a vertical load (4 × 4 × 16 cm 3 test) could be used to define the load-bearing capacity limitation as compressive testing. However, other tests, such as pushover tests, could be carried out on walls built with this type of bricks [60]. Flexural load-deflection curves of soil samples are shown in Figure 8.  Table 5 shows that the density of earth bricks ranges from 1661 kg/m 3 to 1718 kg/m 3 . Calma soils have the lowest density as they are clayey soil. Small pores in clayey particles contribute to the low density of clayey soil. Densification of soil by dynamic or energycontrolled compaction helps to obtain better material homogeneity. The procedure needs to be formalized and implemented in a production cycle. This procedure could be adapted to larger brick sizes or even metric-sized walls. The dry density of compressed earth blocks in the literature varies from 1500 to 2000 kg/m 3 and is lower that than of concrete. The density of bricks is influenced by compaction, the addition of binder, and reinforcement of bricks with natural fibers as the addition of natural fibers decreases the density of bricks [56][57][58].
Linear shrinkage in Calma bricks is around 2.2%, which is considerably high. Sandy soils, such as Cesson, have low shrinkage. Higher clay content and molding moisture content of Calma soils are the reason behind higher shrinkage. Similar behavior was observed in the literature studies [59].

Flexural Strength of Earth Bricks
The flexural strength of earth bricks was determined with a 3-point bending test. The results relating to deflection under a vertical load (4 × 4 × 16 cm 3 test) could be used to define the load-bearing capacity limitation as compressive testing. However, other tests, such as pushover tests, could be carried out on walls built with this type of bricks [60]. Flexural load-deflection curves of soil samples are shown in Figure 8.   Table 6 shows that BDC soils have the lowest flexural  2.26 MPa [61][62][63]. Table 6 shows that BDC soils have the lowest flexural strength while the mixture of BDC and Cesson soils and the Calma soils have the highest flexural strength. The flexural strength of BDC-CS soils is nearly 3 times higher than that of BDC soils. BDC soils have a higher percentage of clays, such as illite, which have low cohesion. A mixture of sandy soils (Cesson) with BDC and CL soils, which have a higher percentage of clay minerals, gives good compressive and flexural strength as the presence of both clay and sand is essential to increasing the strength of specimens. Higher sand content in bricks leads to brittleness while higher clay content results in higher plasticity and crack growth [64]. Furthermore, higher organic matter in Cesson soils is also reduced in the mixture as BDC soils have low organic matter. Higher strength of Calma soils is associated with a higher percentage of fine particles and clay minerals, which act as a binder. There is a lack of norms and standards for earth bricks and recommended tensile strength for unstabilized earth bricks varies from 0.12 MPa to 0.25 MPa in different norms [40,47,65]. BDC samples have considerably lower tensile strength, which is 0.25 MPa while Cesson and Calma soils have higher tensile strength that meets the strength requirement of earthen bricks. The bending stiffness of earth blocks was determined with flexural load-deflection curves. The results of bending stiffness are shown in Table 6. The rise in flexural load is similar for most of the bricks in Figure 8. Calma bricks have the highest bending stiffness as these bricks have higher flexural strength and bending stiffness usually increases with increasing flexural load.

Compressive Strength of Earth Bricks
The compressive strength of earth bricks was determined on cubes of earth bricks with dimensions of 4 × 4 × 4 cm 3 obtained after the flexural strength test. Compressive strength load-deflection curves are shown in Figure 9.
The compressive strength of earth blocks is shown in Table 6. The compressive strength of earth blocks ranges from 0.92 MPa to 2.22 MPa. The BDC-CS soil mixture has higher compressive and flexural strength as shown in Table 6. Mineralogy of BDC soils shows that BDC soil is mainly composed of clay mineral illite while CS is sandy soil. A mixture of BDC and CS soil improves soil granulometry, and bricks have good mechanical behavior with improved soil granulometry contrary to the soil mixture of BDC and CL soils, which are both rich in clay minerals and have low compressive strength. CS is sandy soil and exhibits good compressive and flexural strength. However, sandy soils have brittle behavior. Therefore, ideal soil should be a mixture of both fine and coarse particles [66]. Cesson and Calma soils have two times higher compressive strength than BDC soils. The compressive strength of compressed earth blocks recommended by the French standard is 1 MPa [47], while in some international standards, it ranges from 1 to 2 MPa [65,67,68]. Cesson, Calma, and a mixture of Cesson and BDC soils have a good compressive strength that satisfies the strength requirement according to French recommendations. In French specifications for nonstructural applications, 1 MPa strength is the minimum threshold for compressed earth blocks as the earthen walls are often protected with stabilized earth plaster to protect them from rain and to overcome the durability issue. Stabilization of the earth with hydraulic binders and geopolymers increases the strength and durability of earth bricks. However, the reversibility of stabilized soils is not possible after the life cycle of the earthen structure.
The ratio of compressive and tensile strength (σc/σt) of earth bricks varies from 1.9 to 4 in Table 6, which is significantly lower than that of concrete (σc/σt = 10), which has significantly higher compressive strength and whose tensile strength is usually 10% of its compressive strength. The compressive strength requirement for earthen construction materials varies with applications and the applied load. Table 7 shows the strength requirement prescribed in some international standards for stabilized and nonstabilized earthen construction materials.

Conclusions
In this study, physicochemical and mineralogical characteristics of excavated soils from the Brittany region of France were investigated for their reuse in raw earth blocks (CEB). The grain size distribution of studied soils differs from soil suitable for compressed earth blocks as laser granulometry of BDC and Cesson soils' grain size shows that they have higher sand content while Calma soils have a higher percentage of clay particles In French specifications for nonstructural applications, 1 MPa strength is the minimum threshold for compressed earth blocks as the earthen walls are often protected with stabilized earth plaster to protect them from rain and to overcome the durability issue. Stabilization of the earth with hydraulic binders and geopolymers increases the strength and durability of earth bricks. However, the reversibility of stabilized soils is not possible after the life cycle of the earthen structure.
The ratio of compressive and tensile strength (σc/σt) of earth bricks varies from 1.9 to 4 in Table 6, which is significantly lower than that of concrete (σc/σt = 10), which has significantly higher compressive strength and whose tensile strength is usually 10% of its compressive strength. The compressive strength requirement for earthen construction materials varies with applications and the applied load. Table 7 shows the strength requirement prescribed in some international standards for stabilized and nonstabilized earthen construction materials.

Conclusions
In this study, physicochemical and mineralogical characteristics of excavated soils from the Brittany region of France were investigated for their reuse in raw earth blocks (CEB). The grain size distribution of studied soils differs from soil suitable for compressed earth blocks as laser granulometry of BDC and Cesson soils' grain size shows that they have higher sand content while Calma soils have a higher percentage of clay particles (57%). Higher clay content causes shrinkage in bricks while higher sand content results in brittleness. Organic matter in soils ranges from 3% to 8.7%, which is low and suitable for earth bricks as high organic matter increases soil porosity and decreases the strength of bricks. Methylene blue values of soils range from 1.23 to 1.60 g/100 g, which are low values, and indicate that soils have low plasticity. Liquidity and plasticity limits of soil show that the soils are within the zone recommended for bricks. In addition, the activity of clay calculated with the plasticity index and clay content shows that the studied soils are inactive with less possibility of swelling and shrinkage, which is essential for earth bricks. Silicate minerals (quartz, feldspar) are major components of soil samples with illite and kaolinite as major clay minerals, which are dimensionally stable clays with low water sensitivity and suitable for earthen constructions.
Prismatic earth brick specimens were manufactured through dynamic compaction. Due to the lack of a definite standard for earth bricks, laboratory-scale prismatic specimens' surface layers were scratched to improve bonding between layers. The density of manufactured compressed earth blocks varies from 1661 to 1718 kg/m 3 . Earth bricks with clayey soils (CL) have the lowest density and higher optimum moisture content. Linear shrinkage in bricks ranges from 0.6 to 2.2% and is the highest for clay soil (CL) due to a higher percentage of fine particles and molding moisture content.
For the compressive strength test, bricks were cut into cubes with a fine blade electric saw, which induced the microcracks in bricks and undermined the compressive strength of bricks. Flexural and compressive strength testing of bricks shows that a mixture of Cesson and BDC soils, Cesson, Calma, and a mixture of Cesson and Calma soil-based bricks have good compressive (2.22, 1.74, 1.71, and 1.6 MPa) and flexural strength (0.74, 0.43, 0.47, and 0.69 MPa). A mixture of sandy soils with soils having a higher percentage of clay minerals, including BDC and CL soils, shows good compressive and flexural strength due to improved granulometry of soil mixture. Most of the soil samples have compressive strength higher than 1 MPa and meet the compressive strength requirement of compressed earth blocks, except for BDC soil samples, and can be used for manufacturing earth blocks for walls and nonstructural applications. The flexural strength of all the soil samples is higher than 0.25 MPa and meets the strength requirement of compressed earth bricks in different standards. The bending stiffness of Calma soils is higher as these soils have higher flexural strength. The strength requirement of compressed earth blocks varies with application. For structural applications, the required compressive strength is around 5 MPa by some standards. The compressive strength of most of the studied soil samples is below 2 MPa except for a mixture of BDC and CS soil. The low strength of earth blocks is one of the main barriers to using these blocks for load-bearing structural walls. The durability of earthen blocks is also a problem as these blocks are often sensitive to water and show swelling and shrinkage when they interact with water.
The feasibility study on the design of earth blocks without the addition of stabilizers showed that the compressive strengths reached the threshold recommended by the French standard. However, given the variability of excavated soil, there is a risk that the resistance value will be lower than that required. To address this risk, controls on the disposal of excavated soil must be put in place to ensure geotechnical quality. Geotechnical monitoring must be carried out when the soil is deposited on site. In addition, compaction can also be improved, by developing mechanized compaction and kneading of the material. Further research work is recommended to study the durability of bricks and the variation in brick behavior with different soils.  Data Availability Statement: Data will be made available on request.