Calibration of Soil Moisture Sensors (ECH 2 O-5TE) in Hot and Saline Soils with New Empirical Equation

: The use of soil moisture sensors is a practice applied to improve irrigation water management. ECH2O-5TE sensors are increasingly being used to estimate the volumetric water content (VWC). In view of the importance of the efﬁcient use of these devices, six main factors affecting the accuracy of sensor measurements were studied: soil moisture levels, soil salinity, temperature, organic matter, soil texture, and bulk density. The study showed that the electrical conductivity of the soil and the temperature independently affect the measurements, while the inﬂuence of other factors interferes with that of salinity. This study found that the sensor measurements of the VWC were closest to the actual VWC at the soil ECe and temperatures of 2.42 dS m − 1 and 25 ◦ C, with root-mean-square errors (RMSE) of 0.003 and 0.004 m 3 m − 3 . Otherwise, the measured VWC values of these sensor readouts signiﬁcantly overestimated the actual VWC, with an increasing soil ECe and/or producing temperatures higher than the stated values, and vice versa. Given the importance of these sensors for obtaining accurate measurements for water management, a simpliﬁed empirical equation was derived using the data collected from a wide range of measurements to correct the inﬂuences of electrical conductivity and temperature on the measurement accuracy of the sensors, while considering the inﬂuence of the soil’s texture. Thus, the following equation was proposed: θ va = θ vs (cid:0)(cid:0) aECe 2 + bECe + c (cid:1) + (cid:0) dT 2 + eT + f (cid:1)(cid:1) − 1 . The results concerning the measurement of different VWC levels via these sensors and the proposed L&O correction equation were compared with the corresponding actual VWC values determined by gravimetric methods. It was found that this empirical equation reduced the differences in the RMSE between the sensor readings for the VWC and the actual VWC from 0.072 and 0.252 to 0.030 and 0.030 m 3 m − 3 for 1 and 5 dS m − 1 , respectively, with respect to the EC’s inﬂuence at 25 ◦ C and reduced the RMSE from 0.053 and 0.098 to 0.007 and 0.011 at 3 and 50 ◦ C, respectively, regarding the effect of the temperature at EC 2.42 dS m − 1 at different levels of the actual VWC values.


Introduction
The key to irrigation water conservation, irrigation management, irrigation scheduling, and precision agriculture is the determination of the soil's moisture content.However, it is not practical to estimate the volumetric water content (VWC) via gravimetric methods for daily irrigation.Therefore, sensors must be installed to consistently measure the VWC level around the roots in a precise manner so that losses of water by the plant can be compensated in a timely manner.ECH2O-5TE sensors (METER Environment, formerly Decagon Devices, Inc., Pullman, WA, USA) which are increasingly used around the world, simplify the process because they are economical, smaller in size, they ensure fast and easy installation, and provide three measurements in one, namely, the bulk EC, (1) 5TE: A total of 12 ECH2O-5TE sensors were used with 3 Em50 data loggers (ME-TER Group, Inc., USA, formerly Decagon) as shown in Figure 1.(2) Em50 data logger: A 5-channel, self-contained data recorder designed for use with any ECH2O sensor.Two types of output data can be obtained by the device: raw count (unprocessed data) and processed data, which are converted to volumetric water content (m 3 m −3 ) that is ready to use directly.

Sensor head
Data logger box Data logger box

Soil
Three groups of soils were used in this study: A. In general, to test the influence of the factors, sandy loam soil was used as shown in Tables 1 and 2. B. For specific experiments, to test the influence of soil texture on sensor measurement accuracy, two types of soils were used, as shown in Table 3.These soils were used alone or were mixed, according to the required percentages for the specific experiment.

Soil
Three groups of soils were used in this study: A. In general, to test the influence of the factors, sandy loam soil was used as shown in Tables 1 and 2.
B. For specific experiments, to test the influence of soil texture on sensor measurement accuracy, two types of soils were used, as shown in Table 3.These soils were used alone or were mixed, according to the required percentages for the specific experiment.

Water
Two types of water were used in this experiment: A. Distilled water was used to test the influences of all mentioned factors except the decreasing salinity (EC) from bovine compost by leaching.B. Available irrigation water was used to remove the salinity from bovine compost by leaching.A water analysis is presented in Table 4.

Sporadic Materials and Devices Used
An electric oven, electronic balance, large normal scale, laptop, gas cylinder and stove for heating samples, refrigerator for sample freezing, 20 L pots, cans for drying samples, density tube, heating pots, other tools, and sodium chloride salt.

Bovine Compost
Bovine compost named Asas-Almazraa from the Al-Safi Organic Fertilizer Factory at Riyadh, Saudi Arabia, was used and analyzed according to the method described by [44].The organic matter content was determined by the Walkley and Black procedure [45].The average chemical properties of the compost used in this study are presented in Table 5.

Measuring VWC by Gravimetric Method and Sensors
The soil volumetric water content was determined by a gravimetric method as described by [46] and was measured by sensors.The sensor output of the processed data were converted from the raw data internally into values of volumetric water content as (m 3 m −3 ), electric conductivity (dS m −1 ), and temperature ( • C).The factory calibration was used in this study to investigate the results and obtain a correction equation.Sensors were inserted vertically into a 20 L plastic pot containing 17 kg of a soil sample at 15 cm in depth for a period of 15 min.An ECH2O-5TE sensor was connected to a continuous data logger (model EM50) and programmed to collect readings at 1 min intervals in order to determine the soil water content for soil moisture and EC tests.

Soil Moisture Level Impact on Sensor's Measurement
Three groups of soil with different EC (1, 2.42, and 5 dS m −1 ) were prepared as described in the soil EC influencing section.Eight levels of water were added to each group (4,12,16,19,20,23,25, and 28% w/w).The sensors were inserted vertically into the soil samples and readings of the volumetric water content were taken at approximately 25 • C, while the actual VWC was measured by the gravimetric method by inserting a known-volume cylinder into the soil until the top edge of the cylinder was flush with the soil.Then, the cylinder was placed in a metal tin.The metal tins were immediately weighed and oven dried at 105 • C for 24 h; the metal tins were subsequently reweighed [46].The water mass in the sample was converted to volumetric water content using both soil bulk density and the water density.The influences of soil moisture levels on the sensor's measurement accuracy at temperatures of 3, 25, and 50 • C were measured for comparison.The measurements of soil moisture content were carried out at seven levels of water on the soil experiment (2, 5, 10, 14, 17, 22, and  The soil salinity concentration was expressed as the electrical conductivity (EC) in saturated soil paste as a reference regardless of the soil moisture content.Total of 100 quantities of sodium chloride ranging from 0.54 g to 54 g were weighed.Each quantity was dissolved in water and added to 17 kg of soil in a plastic pot and mixed well.The mixing was done on a plastic sheet and then air-dried.The ECe of the saturated soil paste for each mixed soil sample was determined and recorded as a reference.These mixed soils were used as an empirical soil sample for testing soil salinity factor.

Testing and Sampling Method
To study the salinity influence on these sensors, the prepared soil with NaCl was used in five levels of VWC.Each 17 kg of soil was placed in a 20 L plastic pot and mixed with 750 mL of distilled water at temperature close to 25 • C (by mixing heated and cold water), and the sensor was inserted vertically at 15 cm in depth for a period of 15 min.The ECH2O-5TE sensor was connected to a continuous data logger (model EM50, Decagon Devices, Inc., Pullman, WA, USA).The EM50 data logger was programmed to collect readings at 1 min intervals.Two gravimetric method soil samples were taken by a cylinder of known-volume inserted beside the sensor and placed in a metal tin.The metal tins were immediately weighed and oven dried at 105 • C for 24 h; the cylinders were subsequently reweighed [46].The soil gravimetric water content was converted to volumetric water content by using both soil density and water density.The second, third, and fourth tests were added cumulatively at every testing time using 750 mL of distilled water at 25 • C in the same pot and examined in the same manner as the first test.For the final test, enough water was added to saturate the testing soil and was then tested.

ECe & ECa Testing
The electrical conductivity of the saturated soil paste (ECe) measured by the sensors was used as a steadier reference to investigate the influence of EC on the sensor's measurement accuracy, instead of the apparent electrical conductivity (ECa) by the sensor readings at different levels of VWC.Thus, in this study, the EC indicates the soil electrical conductivity in saturated soil paste regardless of the soil moisture content.

Comparison of the VWC Measured by Sensors and by Gravimetric Method
The actual VWCs of 1000 samples (20 samples daily) were determined by the gravimetric method.The sensor reading of VWC at 25 • C at each EC concentration point vs. the actual VWC values were determined.The VWC values measured by sensors were compared with the actual VWC at each EC level.

Soil Temperature Impact on Sensor's Measurement
A quantity of soil in an oven and a quantity of distilled water were heated to 60 • C. One of 7 quantities of heated water (0.4, 0.9, 1.6, 2.3, 2.9, 3.7, and 4.5 kg) was added to each 17 kg of the heated soil, then mixed well and placed in a 20 L pot.Then, the sensors were immediately inserted vertically into the soil sample, and two samples for VWC measurement were determined by the gravimetric method.Then, the pot was rapidly covered by nylon and a plastic sheet and was tightened with adhesive tape to keep the moisture inside the pot fixed by preventing the exchange of air currents with the outside.The sensors were adjusted at 2 min intervals.The temperature of the soil sample for each pot in the final measurement was close to 50-55 • C. The soil samples were placed in a freezer to cool for 24 h.Then, soil samples were brought out and left to return to the ambient temperature.The soil samples were opened, and two soil samples were taken immediately for drying in the oven.The actual VWC for each soil sample was determined.

Bovine Compost Impact on Sensor's Measurement
Two types of compost were used: high-EC compost (18 dS m −1 ) before leaching, and low-EC compost (1.8 dS m −1 ) that reduced its EC by leaching.The compost EC was reduced using tap water (EC = 0.98 dS m −1 ), filtering with a cloth bag from 18 dS m −1 until it reached 1.8 dS m −1 , and then the compost was air dried.The empirical soil EC (Table 1) was adjusted to the same compost EC by NaCl.The soil samples were then sequentially subjected to 10 different compost rates of 10, 20, 30, 40, 50, 60, 70, 80, 90, and 100 g compost per kg of soil using both high-and low-EC compost, with 10 pots for each experiment.A total of 4 water rates of 60, 120, 180, and 240 mL kg −1 were used by adding 60 mL water per kg of soil cumulatively.After the compost and the soil with the appropriate water rate were well mixed and put into a 20 L pot, the sensor was vertically inserted in each pot at a depth of 15 cm for 15 min and measured at 2 min intervals at each testing point.Two soil samples were taken for actual VWC measurement by a gravimetric method at each testing point.Finally, the average of the sensor readings of the VWC before and after removing EC from the compost was compared to the actual VWC in both cases.

Soil Texture Impact on Sensor's Measurement
Two types of soil were mixed to form soil sample: sand from dunes and clay sediment from a dam at 11 rates, to test the textures impact on sensor's measurement accuracy.The clay soil was added to the sand soil gradually, by 10% of the total sample at each time, cumulatively until the testing sample had a 100% clay texture.Each sample was mixed and placed in a 20 L pot.The mixture soil was tested by two sensors at a depth of 15 cm for 15 min, and at 2 min intervals for the sensor readings at four levels of moisture.The VWC by sensors and the actual VWC by the gravimetric method at different clay content points were compared.

Soil Bulk Density (ρ b ) Impact on Sensor's Measurement
Three prepared soils at different concentrations of EC (1.4,2.5, and 6.0 dS m −1 ) at four levels of VWC (60, 120, 180, and 240 mL per kg of soil) were used to test the influence of the soil bulk density.Two procedures for determining soil volume were conducted: (1) using a soil volume cylinder for the common gravimetric measurement method, and (2) changing the entire soil volume in a gradual cylindrical known-volumetric container by a mechanical pressing-down plate with two holes for the sensors.The total weight and total volume at every testing point were determined, and then the average ρ b was taken.After adding the appropriate amount of water to the soil, this was mixed thoroughly, to confirm that the moisture was uniformly distributed throughout the container.Then, two sensors were installed in the container, and measuring started, by sampling via the gravimetric method as mentioned after every pressing.The desired ρ b levels were achieved by pressing and changing the soil sample volume with a constant weight.The output of the sensors was then taken at different ρ b levels.The VWC determined by the sensors and gravimetric methods at different points of the bulk density were compared.This experiment, which used three EC concentrations at four moisture levels, was then repeated twice.

Statistical Analysis
Four statistical indicators were used to evaluate the sensor measurements of VWC values: the coefficient of determination (r 2 ), root-mean-square error (RMSE), relative rootmean-square error (RRMSE), and coefficient of residual mass (CRM).These measurements were determined by the sensor-based manufacturer and by proposed calibration equations against the actual VWC values determined by the gravimetric method.The root-meansquare error was calculated as: where M si is the soil water content determined by the sensor based on the factory numbers or calculated by proposed calibration equation, M gi is the real soil water content determined by the gravimetric method, and n is the number of measurement points.The relative rootmean-square error, proposed by Loague and Green (1991) [47] is calculated as: where M g is the corresponding mean of the gravimetric measurement, calculated as: The coefficient of residual mass (Loague and Green, 1991) [47] is calculated by Positive values of CRM indicate that the sensor underestimates, and negative values indicate that the sensor overestimates of VWC.For a perfect fit between gravimetric method and sensor values or obtained values by proposed L&O equation, the values of RMSE and CRM should approach or equal zero.In addition, a statistical analysis using a statistical package for social sciences (IBM SPSS Statistics for Windows, Version 19.0, Armonk, NY, USA: IBM Corp., 2010) [48] was carried out.

Combining the Analysis Results with the True Values Measured by the Gravimetric Method under Different Constraints
Figure 2 shows five factors influencing the sensor's measurement under different conditions.It is clear from the figure the influence of salinity and temperature on the measurements, with an increasing or decreasing VWC.

Influence of Soil Moisture Content on 5TE Sensor Measurement Accuracy
Figures 3 and 4 show that the influence of different factors on the sensor reading accuracy depends on the soil moisture level, the EC level, and the temperature.There was no significant impact on the measurement's accuracy when the EC and temperature of the soil were 2.42 dS m −1 and 25 • C, respectively.However, the differences between the sensor readings and the real soil moisture content increased with increasing soil moisture levels, just as much as the differences in the soil EC and its temperature increased away from the indicated limits.This result agreed with the studies of Heidi et al. (2012) [1], that the accuracy of soil moisture sensor measurements is inversely proportional to the soil moisture content.

Influence of Soil Moisture Content on 5TE Sensor Measurement Accuracy
Figures 3 and 4 show that the influence of different factors on the sensor reading accuracy depends on the soil moisture level, the EC level, and the temperature.There was no significant impact on the measurement's accuracy when the EC and temperature of the soil were 2.42 dS m −1 and 25 °C, respectively.However, the differences between the sensor readings and the real soil moisture content increased with increasing soil moisture levels, just as much as the differences in the soil EC and its temperature increased away from the indicated limits.This result agreed with the studies of Heidi et al. ( 2012) [1], that the accuracy of soil moisture sensor measurements is inversely proportional to the soil moisture content.

Influence of Soil Temperature on Sensor Measurement Accuracy
The sensor measurement accuracy of the VWC under different soil temperatures (from 0 to 50 °C) at a fixed EC of 2.42 dS m −1 was tested.Figure 5 shows that the measured VWC-value line intercepts the real-value line when the soil temperature was about 25 °C.However, the sensor readings were under-or overestimated when the soil temperature was lower or higher than 25 °C, respectively.This result agreed with many reported studies [10, 11,14,[41][42][43].

Influence of Soil Temperature on Sensor Measurement Accuracy
The sensor measurement accuracy of the VWC under different soil temperatures (from 0 to 50 • C) at a fixed EC of 2.42 dS m −1 was tested.Figure 5 shows that the measured VWC-value line intercepts the real-value line when the soil temperature was about 25 • C.However, the sensor readings were under-or overestimated when the soil temperature was lower or higher than 25 • C, respectively.This result agreed with many reported studies [10, 11,14,[41][42][43].

Influence of Soil Temperature on Sensor Measurement Accuracy
The sensor measurement accuracy of the VWC under different soil temperatures (from 0 to 50 °C) at a fixed EC of 2.42 dS m −1 was tested.Figure 5 shows that the measured VWC-value line intercepts the real-value line when the soil temperature was about 25 °C.However, the sensor readings were under-or overestimated when the soil temperature was lower or higher than 25 °C, respectively.This result agreed with many reported studies [10, 11,14,[41][42][43].

Influence of Organic Matter Content on Sensor Measurement Accuracy
Figure 6 shows that the sensor measurement accuracy, by the continuous addition of bovine compost containing its primary EC (18 dS m −1 ) to the testing soil at about 25 • C, was affected.With decreasing the compost salinity by leaching (EC = 1.8 dS m −1 ), there was no significant influence of compost addition (until 10% w/w) on the sensor measurement accuracy [6].Some studies reported an independent influence of organic matter on sensor readings [10].

Influence of Organic Matter Content on Sensor Measurement Accuracy
Figure 6 shows that the sensor measurement accuracy, by the continuous addition of bovine compost containing its primary EC (18 dS m −1 ) to the testing soil at about 25 °C, was affected.With decreasing the compost salinity by leaching (EC = 1.8 dS m −1 ), there was no significant influence of compost addition (until 10% w/w) on the sensor measurement accuracy [6].Some studies reported an independent influence of organic matter on sensor readings [10].

Influence of Soil Texture on Sensor Measurement Accuracy
This study focused on the addition of clay deposits to sand from dunes in order to form the required soil texture to investigate the influence of soil texture on the sensor measurement accuracy.Figure 7 shows that when the soil salinity level was fixed in both soils (at 2.45 dS m −1 ) and the temperature was at 25 °C, the influence of the gradual sand clay addition on the sensor accuracy was unsignificant but could be considered.However, its influence was clearly observed when the soil EC values deviated from the indicated limits.Nevertheless, these results do not contradict those of other studies that reported on the influence of clay on sensor readings.For example, Fernando et al. (2014a) [12] reported that sensor measurements in clay soil in an open field were overestimated, and Schwartz et al. (2013) [16] noted that soil permittivity is high in clay soils because of the increased concentration of soluble minerals compared to sandy soil in the same conditions, as well as the influences of saturation capacity and cation exchange capacity.

Influence of Soil Texture on Sensor Measurement Accuracy
This study focused on the addition of clay deposits to sand from dunes in order to form the required soil texture to investigate the influence of soil texture on the sensor measurement accuracy.Figure 7 shows that when the soil salinity level was fixed in both soils (at 2.45 dS m −1 ) and the temperature was at 25 • C, the influence of the gradual sand clay addition on the sensor accuracy was unsignificant but could be considered.However, its influence was clearly observed when the soil EC values deviated from the indicated limits.Nevertheless, these results do not contradict those of other studies that reported on the influence of clay on sensor readings.For example, Fernando et al. (2014a) [12] reported that sensor measurements in clay soil in an open field were overestimated, and Schwartz et al. (2013) [16] noted that soil permittivity is high in clay soils because of the increased concentration of soluble minerals compared to sandy soil in the same conditions, as well as the influences of saturation capacity and cation exchange capacity.

Influence of Soil Bulk Density on Sensor Measurement Accuracy
As illustrated in Figure 8, there was no significant influence of soil density on the sensor's accuracy when the measurements were made at the soil EC of 2.42 dS m −1 , while its influence was clearly observed when the values of the soil ECe deviated from the indicated limits.An increased or decreased EC level from the mentioned limit resulted that the sensor was over-or -underestimating the VWC values with the bulk density.

Influence of Soil Bulk Density on Sensor Measurement Accuracy
As illustrated in Figure 8, there was no significant influence of soil density on the sensor's accuracy when the measurements were made at the soil EC of 2.42 dS m −1 , while its influence was clearly observed when the values of the soil ECe deviated from the indicated limits.An increased or decreased EC level from the mentioned limit resulted that the sensor was over-or -underestimating the VWC values with the bulk density.

Influence of Soil Bulk Density on Sensor Measurement Accuracy
As illustrated in Figure 8, there was no significant influence of soil density on the sensor's accuracy when the measurements were made at the soil EC of 2.42 dS m −1 , while its influence was clearly observed when the values of the soil ECe deviated from the indicated limits.An increased or decreased EC level from the mentioned limit resulted that the sensor was over-or -underestimating the VWC values with the bulk density.

An Empirical Equation to the Influence of EC and Temperature
Since there is a systematic relationship between the more affected factors (EC and temperature) and the sensor measurements, a multivariate polynomial empirical equation [Equation ( 5)] was developed to correct the sensor measurements of VWC values to the real VWC values immediately in situ.The concept of this equation is based on the direct use of the sensor's output, which is internally processed data by the factory (instead of a raw count), because it is easily corrected by using the following equation: Whereas: ϴvɑ: Actual VWC (m 3 m −3 ).ϴvs: Sensor's measurement of VWC (m 3 m −3 ).ECe: Electrical conductivity of the saturated soil paste (dS m −1 ) by sensors.T: Soil temperature (°C) as measured by sensors.

An Empirical Equation to Correct the Influence of EC and Temperature
Since there is a systematic relationship between the more affected factors (EC and temperature) and the sensor measurements, a multivariate polynomial empirical equation [Equation ( 5)] was developed to correct the sensor measurements of VWC values to the real VWC values immediately in situ.The concept of this equation is based on the direct use of the sensor's output, which is internally processed data by the factory (instead of a raw count), because it is easily corrected by using the following equation:  6 show the average values of the proposed L&O correction equation parameters for different soil textures.

Testing the Empirical Correction Equation
The influence of salinity and temperature with the correction equation on the sensor measurement accuracy of VWC values was tested at different statuses.Table 7 showed a correction test of the proposed L&O correction equation with the sensor measurements under different salinity concentrations and temperatures at different levels of moisture.Figure 9 shows a comparison between the actual VWC values measured by the gravimetric method and the VWC calculated by the proposed L&O correction equation in graded soil with increasing moisture at three levels of EC and temperature.Using Table 8, the RRMSE decreased with the proposed L&O correction equation from 31.2 and 109.4% to 4.3 and 11.5% at 1.0 and 5.0 dS m −1 soil salinity, respectively, and from 26.8 and 49.1% to 3.3 and 5.7% at 3 and 50 • C soil temperature, respectively.

Testing Equation to Correct Influence of Electric Conductivity (EC) at 25 • C
Figure 10 shows that the VWC values calculated by the proposed L&O correction equation were closest to the actual VWC as the EC gradually changed.According to Table 9, it appeared that the RRMSE decreased when using the proposed L&O correction equation from 49.2 and 53% to 6.6 and 5.3%, at the field capacity and saturated point, respectively.Figure 11 shows a comparison between the sensor measurements of VWC values by the gravimetric method and those calculated using the L&O equation.In Table 9, it seems that the RRMSE was reduced from 27.8 and 17.2% to 6.1 and 3%, respectively.9, it appeared that the RRMSE decreased when using the proposed L&O correction equation from 49.2 and 53% to 6.6 and 5.3%, at the field capacity and saturated point, respectively.10 shows that the VWC values calculated by the proposed L&O correction equation were closest to the actual VWC as the EC gradually changed.According to Table 9, it appeared that the RRMSE decreased when using the proposed L&O correction equation from 49.2 and 53% to 6.6 and 5.3%, at the field capacity and saturated point, respectively.9 illustrates that the RMSE was decreased from 35.6 and 90.1% to 2.5 and 3% when using the proposed L&O equation.Figure 11 shows a comparison between the sensor measurements of VWC values by the gravimetric method and those calculated using the L&O equation.In Table 9, it seems that the RRMSE was reduced from 27.8 and 17.2% to 6.1 and 3%, respectively.9 illustrates that the RMSE was decreased from 35.6 and 90.1% to 2.5 and 3% when using the proposed L&O equation.9 indicates that the RMSE was  9 indicates that the RMSE was decreased from 24.3 and 96.7% to 5.4 and 11.2%, respectively, when using the proposed L&O equation.

Multiple Comparisons
An analysis of variance (ANOVA) was performed using SPSS Statistics [48] in order to make multiple comparisons between the sensor readings of the VWC as measured by the gravimetric method and the results calculated by the proposed L&O correction equation using multiple comparisons: least significant difference (LSD) and a Dunnett t-test.The results presented in (Table 10) indicate significant differences between the average of the sensor readings and the actual VWC, at a salinity and temperature of 4.48 dS m −1 and 36.7 • C, respectively.There were no significant differences between the actual VWC values and the calculated values of the VWC by the proposed L&O correction equation using the same sensor readings.9 illustrates that the RMSE was decreased from 35.6 and 90.1% to 2.5 and 3% when using the proposed L&O equation.9 indicates that the RMSE was decreased from 24.3 and 96.7% to 5.4 and 11.2%, respectively, when using the proposed L&O equation.An analysis of variance (ANOVA) was performed using SPSS Statistics [48] in order to make multiple comparisons between the sensor readings of the VWC as measured by the gravimetric method and the results calculated by the proposed L&O correction equation using multiple comparisons: least significant difference (LSD) and a Dunnett t-test.The results presented in (Table 10) indicate significant differences between the average of

Correlations
The correlation test results using the Pearson correlation are listed in Table 11.A strong significant correlation between the sensor readings of VWC values and the soil EC levels is indicated, while no statistically significant correlation is shown between the soil EC levels and the actual VWC, or the calculated values of VWC by proposed L&O equation.

Figure 2 .
Figure 2. The influence of various factors on sensor measurements.

Figure 2 .
Figure 2. The influence of various factors on sensor measurements.Agronomy 2022, 12, x FOR PEER REVIEW 9 of 20

Figure 3 .
Figure 3. Correlation between actual VWC by gravimetric method and the sensor at three levels of (a) salinity concentration and (b) temperature.Figure 3. Correlation between actual VWC by gravimetric method and the sensor at three levels of (a) salinity concentration and (b) temperature.

Figure 3 .
Figure 3. Correlation between actual VWC by gravimetric method and the sensor at three levels of (a) salinity concentration and (b) temperature.Figure 3. Correlation between actual VWC by gravimetric method and the sensor at three levels of (a) salinity concentration and (b) temperature.

Figure 3 .
Figure 3. Correlation between actual VWC by gravimetric method and the sensor at three levels of (a) salinity concentration and (b) temperature.

Figure 4 .
Figure 4. Influence of EC on sensor measurements at (a) field capacity and (b) saturated points.

Figure 4 .
Figure 4. Influence of EC on sensor measurements at (a) field capacity and (b) saturated points.

Figure 3 .
Figure 3. Correlation between actual VWC by gravimetric method and the sensor at three levels of (a) salinity concentration and (b) temperature.

Figure 4 .
Figure 4. Influence of EC on sensor measurements at (a) field capacity and (b) saturated points.

Figure 5 .
Figure 5. Influence of soil temperature on sensor measurements at (a) field capacity and (b) saturated points.

Figure 6 .
Figure 6.Influence of organic matter on sensor measurements before and after desalination.

Figure 6 .
Figure 6.Influence of organic matter on sensor measurements before and after desalination.

Figure 7 .
Figure 7. Influence of soil texture on sensor measurements.

Figure 7 .
Figure 7. Influence of soil texture on sensor measurements.
Actual VWC (m 3 m −3 ).θvs: Sensor's measurement of VWC (m 3 m −3 ).ECe: Electrical conductivity of the saturated soil paste (dS m −1 ) by sensors.T: Soil temperature ( • C) as measured by sensors.a, b, c, d, e, and f are the equation constants depending on the soil texture.Table

3. 8 . 3 .
Testing L&O Equation to Correct Influence of Temperature at ECe of 2.42 dS m −1

Figure 10 .
Figure 10.Comparison between VWC values measured by sensor, by gravimetric method, and by proposed L&O correction equation with a gradual increase in soil EC at 25 °C, tested at (a) soil moisture at field capacity and (b) soil moisture at saturated point.

Figure 9 .
Figure 9.Comparison between actual VWC values measured by gravimetric method and calculated by L&O equation in graded increasing soil moisture at three levels of (a) EC and (b) temperature.

Figure 9 .
Figure 9.Comparison between actual VWC values measured by gravimetric method and calculated by L&O equation in graded increasing soil moisture at three levels of (a) EC and (b) temperature.

Figure 10 .
Figure 10.Comparison between VWC values measured by sensor, by gravimetric method, and by proposed L&O correction equation with a gradual increase in soil EC at 25 °C, tested at (a) soil moisture at field capacity and (b) soil moisture at saturated point.

Figure 10 .
Figure 10.Comparison between VWC values measured by sensor, by gravimetric method, and by proposed L&O correction equation with a gradual increase in soil EC at 25 • C, tested at (a) soil moisture at field capacity and (b) soil moisture at saturated point.

3. 8 . 4 .
Figure 12 shows a comparison between the VWC values measured by the sensor, the actual VWCs, and the VWC values calculated by the proposed L&O correction equation with a gradual change in the soil EC at (a) 5 • C and (b) 38 • C. A statistical analysis in Table9illustrates that the RMSE was decreased from 35.6 and 90.1% to 2.5 and 3% when using the proposed L&O equation.

Figure 11 .
Figure 11.Comparison between VWC values measured by sensor, by gravimetric method, and by proposed L&O correction equation with gradual increase in soil temperature at 2.42 dS m −1 at (a) field capacity moisture and (b) saturated points.3.8.4.Testing Equation with Graded EC at Low and High Temperatures Figure 12 shows a comparison between the VWC values measured by the sensor, the actual VWCs, and the VWC values calculated by the proposed L&O correction equation with a gradual change in the soil EC at (a) 5 °C and (b) 38 °C.A statistical analysis in Table9illustrates that the RMSE was decreased from 35.6 and 90.1% to 2.5 and 3% when using the proposed L&O equation.

Figure 12 .
Figure 12.Comparison between VWC values measured by sensors using gravimetric method and proposed L&O correction equation with gradual increase in soil salinity at (a) 5 °C and (b) 38 °C.3.8.5.Testing Equation to Correct for Influence of Both Temperature and Low or High EC Figure 13 shows a comparison between the VWC values measured by the sensor, the actual VWC, and the VMC values resulted from the proposed correction equation as the temperature gradually changed at (a) 1.55 dS m −1 at low moisture and (b) 4.62 dS m −1 at the field capacity moisture.A statistical analysis in Table9indicates that the RMSE was

Figure 11 .
Figure 11.Comparison between VWC values measured by sensor, by gravimetric method, and by proposed L&O correction equation with gradual increase in soil temperature at 2.42 dS m −1 at (a) field capacity moisture and (b) saturated points.3.8.5.Testing Equation to Correct for Influence of Both Temperature and Low or High EC Figure 13 shows a comparison between the VWC values measured by the sensor, the actual VWC, and the VMC values resulted from the proposed correction equation as the temperature gradually changed at (a) 1.55 dS m −1 at low moisture and (b) 4.62 dS m −1 at the field capacity moisture.A statistical analysis in Table9indicates that the RMSE was decreased from 24.3 and 96.7% to 5.4 and 11.2%, respectively, when using the proposed L&O equation.

3. 8 . 4 .
Figure 12 shows a comparison between the VWC values measured by the sensor, the actual VWCs, and the VWC values calculated by the proposed L&O correction equation with a gradual change in the soil EC at (a) 5 °C and (b) 38 °C.A statistical analysis in Table9illustrates that the RMSE was decreased from 35.6 and 90.1% to 2.5 and 3% when using the proposed L&O equation.

Figure 12 .
Figure 12.Comparison between VWC values measured by sensors using gravimetric method and proposed L&O correction equation with gradual increase in soil salinity at (a) 5 °C and 38 °C.

3. 8 . 5 .
Figure 13 shows a comparison between the VWC values measured by the sensor, the actual VWC, and the VMC values resulted from the proposed correction equation as the temperature gradually changed at (a) 1.55 dS m −1 at low moisture and (b) 4.62 dS m −1 at the field capacity moisture.A statistical analysis in Table9indicates that the RMSE was decreased from 24.3 and 96.7% to 5.4 and 11.2%, respectively, when using the proposed L&O equation.

Figure 12 .
Figure 12.Comparison between VWC values measured by sensors using gravimetric method and proposed L&O correction equation with gradual increase in soil salinity at (a) 5 • C and (b) 38 • C. Agronomy 2022, 12, x FOR PEER REVIEW 16 of 20

Figure 13 .
Figure 13.Comparison between VWC values measured by the sensors using gravimetric method and calculated by proposed L&O correction equation with gradually increasing soil temperature at (a) 1.55 dS m −1 in low moisture and (b) 4.62 dS m −1 in field-capacity moisture.

Figure 13 .
Figure 13.Comparison between VWC values measured by the sensors using gravimetric method and calculated by proposed L&O correction equation with gradually increasing soil temperature at (a) 1.55 dS m −1 in low moisture and (b) 4.62 dS m −1 in field-capacity moisture.

Table 1 .
Mechanical analysis of general empirical soil.

Table 2 .
Routine analysis of general empirical soil.

Table 1 .
Mechanical analysis of general empirical soil.

Table 2 .
Routine analysis of general empirical soil.

Table 3 .
Mechanical analysis of specific test soils.
* Soil EC was adjusted with sodium chloride (NaCl).

Table 4 .
Irrigation water analysis used for leaching to remove salinity from bovine compost.

Table 5 .
Chemical properties of bovine compost.

Table 6 .
Constant values of correction equation for measuring soil moisture sensors by soil texture.

Table 7 .
Sensor measurement corrections using the proposed L&O correction equation under different soil salinity and temperatures (in loam soil samples).

Table 8 .
Statistics results of testing proposed L&O correction equation vs. actual VWC values at three salinity levels, and temperature impact on sensor readings of VWC (m 3 m −3 ) in gradually increasing soil moisture as determined by R 2 , RMSE, RRMSE, and CRM.

Table 9 .
Statistical analysis of performance comparison of sensor and proposed L&O correction equation for correcting gradual increase in salinity and temperature on sensor readings as determined by RMSE, RMSE, and CRM in field capacity and saturated point moisture.Testing L&O Equation to Correct Influence of Temperature at ECe of 2.42 dS m −1

Table 9 .
Statistical analysis of performance comparison of sensor and proposed L&O correction equation for correcting gradual increase in salinity and temperature on sensor readings as determined by RMSE, RMSE, and CRM in field capacity and saturated point moisture.

Table 10 .
Variance analysis of sensor readings of VWC as a function of salinity level and temperature, compared with actual VWC values by gravimetric method and calculated VWC by proposed L&O equation.Dependent variable: values of VWC.