Validation of a Textile Material’s Electrostatic Characterization Device for Different Parameters and Their Effect on the Electrostatic Charge Generation

This research aims to validate an electrostatics characterization device to better understand the process of static charge generation in textile materials and to see how different factors affect it. This electrostatic device offers a variety of settings for controlling sample electrostatic activation and has a sample size range of up to one square meter. It can move in both horizontal and vertical directions in a controlled manner, providing a variety of possibilities for testing the effect of various movement features on electrostatic charge formation. Not only the textile polymer but also the motion characterizations influence the generation of electrostatic charges in textiles. The influence of frequency, pressure, dwell time between moves, test duration, effect of different sample sizes, and amplitude of movement on electrostatic charge generation was studied in greater detail. Two different parameters of the electrostatic waveform (peak voltage and peak-to-peak voltage) were investigated. The generation of electrostatic charges is proportional to the peak voltage and peak-to-peak voltage of the electrostatic waveform. Overall electrostatic charge generation increases with increasing frequency, stepping height, applied pressure at the same frequency, and sample size, but decreases with increasing dwell time between moves at the same frequency. The charge also increases with test duration until a saturation point is reached.


Introduction
The measurement of electrostatic charge generation in textile materials can be done for two reasons. The first is to determine its generation to create better textile cloths [1] and floorcoverings with less static buildup [2], while the second is to optimize it to capture the Nano energy and utilize it to charge low-power sensors and electronic devices [3,4]. Concerning the last reason, it is vital to characterize them in order to maximize the charge generation for energy harvesting [5][6][7] and see the various parameters that control it. A device for determining the electrostatic behavior of textiles and floorcovering has been validated [8].
Electrical charges are the fundamental component of all static electricity. These come in both positive and negative. Atoms, which make up all materials, contain these electrical charges. Atoms have a positively charged nucleus and negative electrons around the nucleus. When these charges are present in about equal amounts, which they typically are, their electrical effects are neutralized. A substance may occasionally have a slight excess of positive or negative charges; in this instance, we refer to the material as being charged, and static electrical phenomena may be observed [9][10][11]. Triboelectrification, a method of contact and frictional charging, can be used to separate these charges, which are present in all materials [12][13][14]. A small number of electrons transfer from one substance to the other when any two materials come into contact. The imbalance of charge is carried by testing of floorcoverings and energy harvesting from electrostatic charges. This research is especially to validate a device that can walk on floorcovering to check its electrostatic behavior, but also the vertical movement could be precisely controlled. Additionally, this device is unique for the use of a sample size up to 1 m 2 with the movement of the second sample with specific controlled movement above it. This movement could be controlled with not only contact time but also dwell time (time between moves) and XY (horizontal) direction. The combination of all the possible parameters (frequency, pressure, testing time, stepping height, dwell time, and sample sizes) is controlled within one setup.

Materials and Methods
The material's electrostatic characterization device consists of different parts as seen in Figure 1 and illustrated in the schematic diagram in Figure 2. In the middle is the X-Carve, where the movement on the samples takes place. On the shelf is an aluminum plate, which is connected to the ground. This plate, therefore, serves as a reference for the measurements. A plastic mat is placed on the metal plate, which ensures insulation of the carpet in relation to the reference plane. These two layers remain permanently in the system. The piece of textile to be tested can then be placed on the plastic mat. On the left side of the X-Carve are all the electronics, controls, and pneumatics. At the bottom of the figure are the power supply and control of the X-Carve. Above that are both electronic boxes and the analogto-digital converter (ADC) used to record the waveform. The pneumatic circuit is located behind the electronics. A standard compressed air connector is provided to connect the compressed air to the pressure regulator. The regulated pressure then flows to the valve, which is actuated by the control of the X-Carve. The compressed air lines are directed upwards to prevent the lines from sinking down. The pneumatic cylinder, which acts as an actuator for up and down motion, was fixed to the Z-axis of the X-Carve via an adapter plate. In this way, the step height can be set from the GUI (Graphical User Interface). especially useful in optimization of electrostatic characterization parameters for electrostatic testing of floorcoverings and energy harvesting from electrostatic charges. This research is especially to validate a device that can walk on floorcovering to check its electrostatic behavior, but also the vertical movement could be precisely controlled. Additionally, this device is unique for the use of a sample size up to 1 m 2 with the movement of the second sample with specific controlled movement above it. This movement could be controlled with not only contact time but also dwell time (time between moves) and XY (horizontal) direction. The combination of all the possible parameters (frequency, pressure, testing time, stepping height, dwell time, and sample sizes) is controlled within one setup.

Materials and Methods
The material's electrostatic characterization device consists of different parts as seen in Figure 1 and illustrated in the schematic diagram in Figure 2. In the middle is the X-Carve, where the movement on the samples takes place. On the shelf is an aluminum plate, which is connected to the ground. This plate, therefore, serves as a reference for the measurements. A plastic mat is placed on the metal plate, which ensures insulation of the carpet in relation to the reference plane. These two layers remain permanently in the system. The piece of textile to be tested can then be placed on the plastic mat. On the left side of the X-Carve are all the electronics, controls, and pneumatics. At the bottom of the figure are the power supply and control of the X-Carve. Above that are both electronic boxes and the analog-to-digital converter (ADC) used to record the waveform. The pneumatic circuit is located behind the electronics. A standard compressed air connector is provided to connect the compressed air to the pressure regulator. The regulated pressure then flows to the valve, which is actuated by the control of the X-Carve. The compressed air lines are directed upwards to prevent the lines from sinking down. The pneumatic cylinder, which acts as an actuator for up and down motion, was fixed to the Z-axis of the X-Carve via an adapter plate. In this way, the step height can be set from the GUI (Graphical User Interface).  The GUI (Graphical User Interface) is shown in Figure 3 and is used to precisely control the total test time, dwell time, foot up, and foot down time. The effect of electrostatic charge generation has been studied at three different frequencies. In order to obtain the 1, 1.5, and 2-hertz frequency, the following settings have been used for the different time parameters.   The GUI (Graphical User Interface) is shown in Figure 3 and is used to precisely control the total test time, dwell time, foot up, and foot down time. The effect of electrostatic charge generation has been studied at three different frequencies. In order to obtain the 1, 1.5, and 2-hertz frequency, the following settings have been used for the different time parameters. The GUI (Graphical User Interface) is shown in Figure 3 and is used to precisely contro the total test time, dwell time, foot up, and foot down time. The effect of electrostatic charg generation has been studied at three different frequencies. In order to obtain the 1, 1.5, an 2-hertz frequency, the following settings have been used for the different time parameters    Three different pressure-applied settings of 0.5, 1, and 1.5 bar were selected with the help of a pressure valve unit to study the effect of pressure applied on the electrostatic charge generation. The effect of testing time was studied at six different test duration times: 10, 20, 30, 40, 50, and 60 s selected with the option given in GUI (test duration). Three different distances (10 mm, 30 mm, and 50 mm) between the up and down movement were selected at the same frequency, applied pressure, and total test duration. For dwell time between moves, three different times-100 ms, 200 ms, and 300 ms-were selected at 2 Hz frequency. Three different sample sizes were selected to study the effect of electrostatic charge generation for the same material and the same setting of applied pressure, frequency, stepping height, and test duration. The maximum peak voltage and peak-to-peak voltage were calculated and given in tables to see the effect of different parameters on electrostatic charge generation. The floorcovering pile fiber composition was 100% PA6, with bitumen backing, loop pile, nominal mass of 4128.4 g/m 2 , and total thickness of 6.9 mm.
The tests were carried out using the new device and with a one-square-meter sample size, with BAM as the sole material for the testing related to effect of sample size and conductive copper fabric (Shieldex ® , Bremen, Germany) for the rest of the parameters (frequency, dwell time, pressure, testing time, stepping height). The sample was cut to three different sizes to examine the influence of sample size. Three repetitions were performed for each parameter (frequency, dwell time, pressure, testing time, stepping height, and sample size). The average highest peak voltage was calculated for each repeat by averaging five peaks and valleys as described in standard ISO 6356. The difference between the highest peaks and highest valleys on an electrostatic voltage graph was used to compute the peak-to-peak voltage.

Effect of Frequency
The effect of three different frequencies-1 hertz, 1.5 hertz, and 2 hertz-on the electrostatic charge generation are summarized in Table 1. In Figure 4, the output voltage (peak voltage, peak-to-peak voltage) was increased with increase in frequency from 1 Hz to 2 Hz. The increase in voltage is due to more contact and separation motions that generate more electrostatic charges, and hence more output voltage. There is an increase in the electrostatic charge generation if we increase the frequency of tapping between the samples by taking the contact time constant indicated by the increase in peak voltage and peak-to peak-voltage, as shown in Figures 5 and 6. In addition, with the increase in frequency, there is an increase in the speed of movement and contact time that generates more electrostatic charges at the same pressure, stepping height, and testing time. The coefficient of variation (CV %) is the ratio of the standard deviation to the mean expressed as percentage.             Figure 6. Effect of different frequency on the electrostatic waveform, peak voltage, and amplitude (peak-to-peak voltage).

Effect of Different Pressure
The effect of applied pressure is more significant for compressible textiles or floorcoverings, as shown in Figure 7, and hence have a different area of contact at different pressure. A floorcovering sample with bulky piling has been selected to see the charge generation at different pressure as shown in Figure 4. Three different pressures (0.5, 1, and 2 bar) have been applied to see the effect of changing pressure on electrostatic charge generation (see Table 2). There is an increase in peak voltage and peak-to-peak voltage with the successive increase in applied pressure. The output voltage increases more when the pressure applied is changed from 0.5 to 1 bar as compared to 1 bar to 1.5 bar. The increase in static charges with increasing pressure is due to the increased compressing of the textile structure, which causes more inter-fiber friction. Over one bar, the change in static charges is not so large anymore, so over a threshold pressure, the influence of pressure will not be large anymore.

Effect of Different Pressure
The effect of applied pressure is more significant for compressible textiles or floorcoverings, as shown in Figure 7, and hence have a different area of contact at different pressure. A floorcovering sample with bulky piling has been selected to see the charge generation at different pressure as shown in Figure 4. Three different pressures (0.5, 1, and 2 bar) have been applied to see the effect of changing pressure on electrostatic charge generation (see Table 2). There is an increase in peak voltage and peak-to-peak voltage with the successive increase in applied pressure. The output voltage increases more when the pressure applied is changed from 0.5 to 1 bar as compared to 1 bar to 1.5 bar. The increase in static charges with increasing pressure is due to the increased compressing of the textile structure, which causes more inter-fiber friction. Over one bar, the change in static charges is not so large anymore, so over a threshold pressure, the influence of pressure will not be large anymore.

Effect of Test Duration Time
The test duration is essential to see a saturation point in the electrostatic charge generation waveform. Table 3 summarized the effect of different test durations (10 s, 20 s, 30 s, 40 s, 50 s, 60 s) on the electrostatic charge generation. There is a successive increase in peak voltage and peak-to-peak voltage with the increase in total test time, as shown in Figures 8 and 9. At 60 s, the saturation is almost reached, and a balance must be found to allow sufficiently fast testing. While the time increased from 40 s to 50 s, the increase in output voltage was 10%, and it was just 5% from 50 s to 60 s.

Effect of Test Duration Time
The test duration is essential to see a saturation point in the electrostatic charge generation waveform. Table 3 summarized the effect of different test durations (10 s, 20 s, 30 s, 40 s, 50 s, 60 s) on the electrostatic charge generation. There is a successive increase in peak voltage and peak-to-peak voltage with the increase in total test time, as shown in Figures 8 and 9. At 60 s, the saturation is almost reached, and a balance must be found to allow sufficiently fast testing. While the time increased from 40 s to 50 s, the increase in output voltage was 10%, and it was just 5% from 50 s to 60 s.

Effect of Stepping Height
The effect of different stepping heights of 10, 30, and 50 mm on the electrostatic charge generation is summarized in Table 4. There is an increase in peak voltage and peakto-peak voltage with the increase in stepping height from 10 mm to 50 mm, as shown in Figure 10. As the frequency is the same for each stepping height, there is an increase in speed of movement, which corresponds to the higher generation of electrostatic charges. Compared to human testing, this might explain some of the differences between human testing and device testing, as humans will take steps that typically lift the foot more than 50 mm. The increase with height is also significant with a rise of 32% when going from 30 to 50 mm, so large differences can arise if humans step on the same carpet.

Effect of Stepping Height
The effect of different stepping heights of 10, 30, and 50 mm on the electrostatic charge generation is summarized in Table 4. There is an increase in peak voltage and peakto-peak voltage with the increase in stepping height from 10 mm to 50 mm, as shown in Figure 10. As the frequency is the same for each stepping height, there is an increase in speed of movement, which corresponds to the higher generation of electrostatic charges. Compared to human testing, this might explain some of the differences between human testing and device testing, as humans will take steps that typically lift the foot more than 50 mm. The increase with height is also significant with a rise of 32% when going from 30 to 50 mm, so large differences can arise if humans step on the same carpet.

Effect of Stepping Height
The effect of different stepping heights of 10, 30, and 50 mm on the electrostatic charge generation is summarized in Table 4. There is an increase in peak voltage and peak-to-peak voltage with the increase in stepping height from 10 mm to 50 mm, as shown in Figure 10. As the frequency is the same for each stepping height, there is an increase in speed of movement, which corresponds to the higher generation of electrostatic charges. Compared to human testing, this might explain some of the differences between human testing and device testing, as humans will take steps that typically lift the foot more than 50 mm. The increase with height is also significant with a rise of 32% when going from 30 to 50 mm, so large differences can arise if humans step on the same carpet.

Effect of Different Dwell Time between Moves at Fixed Frequency
The dwell time is the time between the up and down maximum point. Table 5 shows the effect of dwell time on the electrostatic charge generation at a stepping frequency of 2 Hz. It was found that there was a decrease in electrostatic charge generation with the increase in dwell time. As the movement frequency is the same, the increase in dwell time corresponds to a decrease in movement time (higher speed), generating fewer electrostatic charges at higher dwell time, as shown in Figure 11.

Effect of Sample Size
The study of electrostatic charge generation was tested for the different sample sizes to see the effect of exposed surface area on the generation of electrostatic charges. For this, three samples size of the same materials were selected, as summarized in Table 6. The increase in sample size increases peak voltage and peak-to-peak voltage. The reason is bigger surface area means more exposure to material that has not yet been stepped on. So, the material where stepping occurs is not charged yet and can further charge the foot. Figure 12 shows the increase in electrostatic charge generation with the increase in sample size. It is clear that over a specific size, there is sufficient material to step on, leading to a cut off of how much charge is possible as the sample size increases.

Effect of Different Dwell Time between Moves at Fixed Frequency
The dwell time is the time between the up and down maximum point. Table 5 shows the effect of dwell time on the electrostatic charge generation at a stepping frequency of 2 Hz. It was found that there was a decrease in electrostatic charge generation with the increase in dwell time. As the movement frequency is the same, the increase in dwell time corresponds to a decrease in movement time (higher speed), generating fewer electrostatic charges at higher dwell time, as shown in Figure 11.

Effect of Different Dwell Time between Moves at Fixed Frequency
The dwell time is the time between the up and down maximum point. Table 5 shows the effect of dwell time on the electrostatic charge generation at a stepping frequency of 2 Hz. It was found that there was a decrease in electrostatic charge generation with the increase in dwell time. As the movement frequency is the same, the increase in dwell time corresponds to a decrease in movement time (higher speed), generating fewer electrostatic charges at higher dwell time, as shown in Figure 11.

Effect of Sample Size
The study of electrostatic charge generation was tested for the different sample sizes to see the effect of exposed surface area on the generation of electrostatic charges. For this, three samples size of the same materials were selected, as summarized in Table 6. The increase in sample size increases peak voltage and peak-to-peak voltage. The reason is bigger surface area means more exposure to material that has not yet been stepped on. So, the material where stepping occurs is not charged yet and can further charge the foot. Figure 12 shows the increase in electrostatic charge generation with the increase in sample size. It is clear that over a specific size, there is sufficient material to step on, leading to a cut off of how much charge is possible as the sample size increases.

Effect of Sample Size
The study of electrostatic charge generation was tested for the different sample sizes to see the effect of exposed surface area on the generation of electrostatic charges. For this, three samples size of the same materials were selected, as summarized in Table 6. The increase in sample size increases peak voltage and peak-to-peak voltage. The reason is bigger surface area means more exposure to material that has not yet been stepped on. So, the material where stepping occurs is not charged yet and can further charge the foot. Figure 12 shows the increase in electrostatic charge generation with the increase in sample size. It is clear that over a specific size, there is sufficient material to step on, leading to a cut off of how much charge is possible as the sample size increases.

Conclusions
Six parameters (frequency, pressure, testing time, stepping height, dwell time, and different sample sizes) could be controlled with the automatic electrostatic characterization device. The effect of different parameters on electrostatic charge generation was studied with the help of peak voltage and peak-to-peak voltage. Peak voltage increases with the increase in frequency, stepping height, time duration of the test until a saturation point, applied pressure at the same frequency, and sample size, but decreases with an increase in dwell time at the same frequency. Additionally, the peak-to-peak voltage increases with the increase in frequency, stepping height, time duration of the test until a saturation point, and applied pressure at the same frequency, but decreases with an increase in dwell time at the same frequency. Therefore, various motion-related parameters controlled through this device were validated by the peak and peak-to-peak voltage to see their effect on the overall output voltage.
Higher frequency causes more electrostatic charges to be generated due to faster movement. The higher frequency is achieved by reducing the dwell time, so a shorter dwell time leads to more electrostatic charge. This corresponds to what is seen when the frequency is kept fixed, but the dwell time increases. This increase in dwell time leads to a decrease in electrostatic charges. We can conclude that contact and release generate static charges, which slowly disappear again as the materials remain in contact. So, the dwell time will have a high effect on the result and should be well-defined when doing automated static testing. As the stepping height increases, more electrostatic charges are generated due to increased exposure to air during movement. The change is large (33.5% when going from 1 to 5 cm), so automated systems clearly report it. The increase in static charges with increasing pressure is due to the increased compressing of the textile structure, which causes more inter-fiber friction. Over one bar, the change in static charges is not so large anymore, so over a threshold pressure, the influence of pressure will not be large anymore.
The rise in electrostatic charges with larger sample sizes is due to increased material exposure over a larger surface area, with the influence being largest when going to very small samples, so testing should always be done on a sufficiently large testing sample to be representative. The same applies in case of testing time; it should be sufficiently large to be able to reach the saturation point as 60 s in this research testing. The validation performed in this research gives clear guidelines on settings to use and what parameters are important to report on when using automated static testing devices. The devices must be used over a testing time of a minimum of 1 min, must step on samples being 1 m 2 or higher, must use pressure higher than 1 bar, and dwell time and stepping height must be clearly reported as these factors have an effect on the generation of static charges. Table 7

Conclusions
Six parameters (frequency, pressure, testing time, stepping height, dwell time, and different sample sizes) could be controlled with the automatic electrostatic characterization device. The effect of different parameters on electrostatic charge generation was studied with the help of peak voltage and peak-to-peak voltage. Peak voltage increases with the increase in frequency, stepping height, time duration of the test until a saturation point, applied pressure at the same frequency, and sample size, but decreases with an increase in dwell time at the same frequency. Additionally, the peak-to-peak voltage increases with the increase in frequency, stepping height, time duration of the test until a saturation point, and applied pressure at the same frequency, but decreases with an increase in dwell time at the same frequency. Therefore, various motion-related parameters controlled through this device were validated by the peak and peak-to-peak voltage to see their effect on the overall output voltage.
Higher frequency causes more electrostatic charges to be generated due to faster movement. The higher frequency is achieved by reducing the dwell time, so a shorter dwell time leads to more electrostatic charge. This corresponds to what is seen when the frequency is kept fixed, but the dwell time increases. This increase in dwell time leads to a decrease in electrostatic charges. We can conclude that contact and release generate static charges, which slowly disappear again as the materials remain in contact. So, the dwell time will have a high effect on the result and should be well-defined when doing automated static testing. As the stepping height increases, more electrostatic charges are generated due to increased exposure to air during movement. The change is large (33.5% when going from 1 to 5 cm), so automated systems clearly report it. The increase in static charges with increasing pressure is due to the increased compressing of the textile structure, which causes more inter-fiber friction. Over one bar, the change in static charges is not so large anymore, so over a threshold pressure, the influence of pressure will not be large anymore.
The rise in electrostatic charges with larger sample sizes is due to increased material exposure over a larger surface area, with the influence being largest when going to very small samples, so testing should always be done on a sufficiently large testing sample to be representative. The same applies in case of testing time; it should be sufficiently large to be able to reach the saturation point as 60 s in this research testing. The validation performed in this research gives clear guidelines on settings to use and what parameters are important to report on when using automated static testing devices. The devices must be used over a testing time of a minimum of 1 min, must step on samples being 1 m 2 or higher, must use pressure higher than 1 bar, and dwell time and stepping height must be clearly reported as these factors have an effect on the generation of static charges. Table 7 summarized the effect of different parameters on the overall electrostatic charge generation. Stepping height Increase with the increase in stepping height Informed Consent Statement: Not applicable.

Data Availability Statement:
Most of data is presented in this article. More detailed data presented in this study are available on request from the corresponding author.

Conflicts of Interest:
The authors declare no conflict of interest.