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Article

Normalization of Relative-Permeability Curves of Cores in High-Water-Content Tight Sandstone Gas Reservoir

1
Sinopec North China Petroleum Bureau, Zhengzhou 450006, China
2
School of Petroleum and Natural Gas Engineering, Chongqing University of Science and Technology, Shapingba, Chongqing 401331, China
3
School of Petroleum Engineering, China University of Petroleum (East China), Qingdao 266580, China
*
Author to whom correspondence should be addressed.
Energies 2025, 18(9), 2335; https://doi.org/10.3390/en18092335
Submission received: 26 March 2025 / Revised: 24 April 2025 / Accepted: 29 April 2025 / Published: 3 May 2025

Abstract

:
The gas–water relative-permeability relationship in tight gas is complex due to interactions between the gas and water phases within the porous media in the reservoir. To clarify the fluid occurrence and the gas–water relative-permeability behavior in such reservoirs, the Dongsheng tight water-bearing reservoir from the Ordos Basin of China is taken as the research object. A non-steady state method is employed to explore the co-permeability of gas and water phases under dynamic conditions. The irreducible water saturation of different core samples is analyzed using nuclear magnetic resonance (NMR) centrifugation. The Simplified Stone equation is applied for phase permeability normalization. The results indicate that with the decrease in core permeability, the irreducible water saturation increases, and the gas and water permeability decreases. When the displacement pressure difference increases, the gas phase permeability decreases, and the water phase permeability increases. The centrifugal method is effective in reducing the saturation of bound water in rock cores. The displacement method forms channels using gas, which effectively removes free water, particularly in larger or smaller pores. In contrast, centrifugation further displaces water from smaller or capillary pores, where flow is more restricted. Based on these experimental findings, a relationship between displacement pressure difference, critical irreducible water saturation, and residual gas saturation is established. The Stone equation is further refined, and a phase permeability normalization curve is proposed, accounting for the true irreducible water saturation of rock. This provides a more accurate theoretical framework for understanding and managing the gas–water interaction in tight gas reservoirs with a high water content, ultimately aiding in the optimization of reservoir development strategies.

1. Introduction

As a crucial unconventional natural gas resource, tight sandstone gas reservoirs contribute to 75% of the total unconventional natural gas production, which is of great significance for development. China is rich in tight gas resources, predominantly located in regions such as Ordos, Sichuan, Tarim, and Songliao. However, a common issue during the development process is water production, which leads to wellbore fluid accumulation, reduced production, and even shutdowns. This, in turn, negatively impacts the overall development efficiency of tight gas reservoirs [1]. Specifically, the tight reservoir of the Dongsheng gas field in Ordos faces the challenges of poor physical properties, strong heterogeneity, and a complex pore-throat structure, which lead to intricate gas–water permeability characteristics that directly impact the gas reservoir’s recovery rate [2,3]. Therefore, studying the gas–water permeability characteristics and occurrence patterns of tight sandstone reservoirs is crucial for improving the development efficiency of tight gas reservoirs [4,5,6].
During the formation of tight water-bearing reservoirs, hydrocarbon gases displace the primary formation water as they migrate. However, due to the varying sizes of reservoir pore throats, some small pore throats tend to trap residual formation water. At the same time, pore water is more likely to accumulate in reservoirs with low local structures and favorable physical properties. Additionally, the change in geological structure and water content distribution, as well as the change in pressure difference in the development process, may lead to the formation of aquifers, which makes the tight water gas reservoir show the characteristic of a high water content [7]. A high water content increases gas flow resistance, which hinders gas production, leads to a rapid decline in gas well pressure and output, and shortens the production life cycle of gas wells [8].
The two-phase flow behavior of gas and water in tight sandstone is complex. Laboratory experiments have been conducted to determine the gas–water two-phase permeability curves of rock cores using both steady-state and non-steady state methods. The steady relative-permeability test method is used to measure the relative permeability according to the gas and water flow rate under the stable state of inlet and outlet pressure by simultaneously injecting gas and water phases at a constant flow rate. There is a logarithmic function relationship between relative permeability and water saturation. With the increase in core permeability, the isotonic point moves towards a higher water saturation, the irreducible water saturation increases, and the residual gas saturation decreases accordingly [9]. In the saturated core, gas migration needs to overcome capillary displacement pressure, and its process undergoes two characteristic stages: capillary force and diffusion control [10]. The experimental results show that the relative-permeability curve of fixed water saturation measured by the steady-state method can effectively characterize the multiphase flow characteristics in the fractured and porous dual media [11]. The fracture geometry and temperature and pressure conditions will significantly affect the relative permeability of gas and water [12], and the change in the properties of the two-phase fluid under a high-temperature and high-pressure environment will lead to significant changes in the relative-permeability curve [13].
The unsteady gas–water-phase permeability experiment is simple, and closer to the actual reservoir conditions, and it is widely used. In the unsteady displacement method, the saturated water core is driven by gas. The gas–water production and the pressure difference between the two ends of the sample are recorded with time at the outlet of the sample, and the relation curve between gas–water relative permeability and water saturation is plotted. The gas–water two-phase seepage behavior in the reservoir is affected by many complicated factors. In terms of the theoretical model, the traditional relative-permeability model is improved based on the fractal capillary bundle hypothesis by introducing parameters such as the effective porosity coefficient and critical pore diameter, so as to describe the gas–water seepage characteristics in coal more accurately [14]. The experimental results show that the capillary end effect and the end water film result in the low relative permeability of gas under low injection pressure [15]. Pore structure characteristics, wettability, confining pressure conditions, and pressure gradients all significantly affect the variation in gas–water relative permeability. It is worth noting that due to the high heterogeneity of the rock itself, the relative-permeability curves of different coal samples show significant differences [16,17].
The relative-permeability curve is a key indicator for exploring the flow characteristics of multiphase fluids in reservoirs. It provides essential data for dynamic analysis, development strategy planning, and reservoir numerical simulation during oil and gas field development. To accurately depict the permeability characteristics of reservoir fluids, indoor experiments are necessary to measure the phase permeability curves of multiple representative rock samples. These curves are then normalized to obtain a single phase permeability curve that represents the entire reservoir’s permeability characteristics while preserving the overall features of each individual curve. Currently, the main normalization methods include the averaging method, empirical formula method, and polynomial fitting method. Many scholars have proposed normalization models, as shown in Table 1. Lu et al. [18] improved the average method using Lagrange interpolation, which provides better normalization effects on oil–water permeability curves. Pan et al. [19] valuated the applicability of normalization methods for relative-permeability curves across different reservoir types and flow units, considering variations in reservoir properties and the morphological characteristics of relative-permeability curves. Gong et al. [20] proposed the semi-normalization method for relative-permeability curves, which normalizes only the water phase’s relative permeability, while the oil phase’s relative permeability is obtained by multiplying the water phase’s relative permeability with the ratio of the oil to water relative permeability. This method avoids the problem of low fitting accuracy in the logarithmic relationship between the oil phase’s relative permeability and oil saturation. For tight gas reservoirs with a high water content, the irreducible water saturation obtained from non-steady-state displacement experiment is high, but the actual irreducible water content of the reservoir is low, which makes it difficult for the existing normalization methods to accurately characterize the gas–water relative permeability of such gas reservoirs.
This study aims to address the gap in the literature by focusing on the gas–water permeability characteristics and normalization methods specifically for high-water-content tight gas reservoirs. Through laboratory experiments and refined normalization techniques, this research seeks to provide a more accurate and reliable framework for modeling gas–water two-phase flow and improving the development efficiency of such reservoirs. Additionally, the study will explore the impact of high water content on gas flow resistance and propose optimized methods for reservoir management that account for these unique challenges.

2. Materials and Methods

2.1. The Experimental Materials

Six core samples were collected from the Permian B1 layer of the Dongsheng gas field in the Ordos Basin (Figure 1), and their porosity and permeability were measured. The basic physical properties of the core samples are shown in Table 2. The synthetic formation water was prepared to replicate the groundwater properties of the Dongsheng gas field, with a composition designed to closely match the typical ionic profile and salinity found in the region’s formation water (Table 3). The salinity of 48,126 mg/L is typical for the water found in the Permian B1 layer, providing a realistic simulation for the experimental conditions. Methane was used as the gas in the experiment. The core samples collected from the Permian B1 layer of the Dongsheng gas field exhibit a wide range of porosity (2.14% to 11.58%) and permeability (0.027 to 1.149 mD), indicative of the heterogeneity typical of tight gas reservoirs. The nuclear magnetic pore size distribution and mineral content of 6 core samples are shown in Figure 2 and Figure 3, respectively. It can be seen from Figure 2 that the mineral contents of the six cores are not much different, with quartz content accounting for 70%, indicating that the six cores are hydrophilic. It can be seen from Figure 3 that as the permeability of the core increases, the peak value of the nuclear magnetic resonance curve shifts to the right and the proportion of macropores in the core increases.

2.2. Non-Steady State Infiltration Experiment

To investigate the variation in the relative permeability of rock core gas and water under different displacement pressures, a self-made experimental device was developed for this study, as shown in Figure 4. The device includes a high-precision plunger pump, an intermediate container, a high-precision pressure-regulating valve, a nitrogen cylinder, a core seat, a hand pump, and a back pressure valve. The detailed experimental steps are as follows:
Step 1: Place the core sample in the intermediate container and vacuum for 48 h to remove any residual fluids.
Step 2: Introduce the formation water into the container, pressurize it to 5 MPa, and allow the core to equilibrate for 48 h before proceeding to the next phase.
Step 3: Weigh the water-saturated rock core and place it in the core holder. Simulate the sandstone’s state under pressure by applying a confining pressure of 10 MPa. Open the gas cylinder, adjust the pressure valve, and inject CH4 into the core through the injection end at a pressure of 2 MPa to simulate the gas flooding process. Record the volume of liquid in the measuring cylinder and the reading of the gas flowmeter every 3 min, and calculate the cumulative water and gas production until there is no water production at the outlet end.
Step 4: The inlet pressures of 3 MPa, 4 MPa, and 5 MPa were selected to simulate a range of typical formation pressures in tight gas reservoirs. These pressures represent conditions where gas displacement is likely to occur in the initial, intermediate, and late stages of reservoir depletion.
Calculate the relative permeability of gas and water based on the experimental results, where the formula for calculating the non-steady state relative permeability of gas and water is as follows [25]:
f w S g = d V w ¯ t d V ¯ t
f w S g = d V w ¯ t d V ¯ t
K r g = K r w μ g μ w × 1 f w S g f w S g
I = Q t Q 0 Δ p 0 Δ p t
S g = V w ¯ t V ¯ t f w S g
In the formula, fw (Sg) is the moisture content; V w ¯ (t) is the dimensionless cumulative water production, expressed as a multiple of pore volume; V ¯ (t) is the dimensionless cumulative liquid production, expressed as a multiple of pore volume; Krw is the relative permeability of the aqueous phase; Krg is the relative permeability of the gas phase; I is the relative injection capacity, also known as the flow capacity ratio, dimensionless; Q(t) is the liquid production and flow rate at the outlet face of the rock sample at time t, cm3/s; Q0 is the initial oil production flow rate at the outlet section of the rock sample, cm3/s; Δp0 is the initial driving pressure difference, MPa; Δp(t) is the displacement pressure difference at time t, MPa; Sg is the gas saturation at the outlet face of the rock sample; μg is the gas viscosity, mPa·s; under experimental conditions; μw is the viscosity of the formation water under experimental conditions, mPa·s.

2.3. Determination of Irreducible Water Saturation Based on NMR

NMR (nuclear magnetic resonance) measurements, specifically the T2 relaxation time, provide additional insights into the water distribution in pores, allowing for a more accurate determination of irreducible water saturation when used in conjunction with the centrifugal method. The centrifuge and nuclear magnetic device were shown in Figure 5. The centrifugal force was gradually increased to remove water from the rock core. At each centrifugal stage, nuclear magnetic resonance (NMR) was used to monitor changes in water content over time. When the water content stabilized and showed no further change under a given centrifugal force, it was considered that the minimum water saturation corresponding to that centrifugal force had been reached. As the centrifugal force continued to increase and the water content in the core remained effectively unchanged, it was determined that the bound water saturation had been reached. At this point, the experiment was concluded. This range of centrifugal forces ensures that water is removed from both macro-pores and micro-pores, allowing for the determination of irreducible water saturation across the full spectrum of pore structures. T₂ spectra of the core samples were obtained at different levels of centrifugal pressure. The shorter T2 values correspond to water in smaller pores, while longer T2 values are associated with water in larger pores. By correlating the T2 values with known saturation values, the irreducible water saturation can be calculated, providing insight into the pore structure and water retention characteristics of the core sample.

3. Results

3.1. Analysis of Experimental Results of Non-Steady State Permeation Curve

As shown in Figure 6, the variation in fluid permeability within the core of tight sandstone was revealed. It can be seen that, with the increase in water saturation, the relative permeability of the water phase gradually increases, while the relative permeability of the gas phase shows an exponential upward trend. This phenomenon may be due to the fact that, under high-water-saturation conditions, most of the pore space is filled with water, which restricts gas flow. As the water saturation decreases, the connectivity between pore spaces improves, resulting in more open channels for gas to flow. This is due to the reduced capillary forces holding the water within the pore throats, which allows gas to flow more freely through previously constricted pathways. This increase in gas flow capacity is directly related to the rapid increase in the relative permeability of gas.
As shown in Figure 6, under the same water saturation conditions, an increase in displacement pressure led to a decrease in the relative permeability of gas, while the relative permeability of liquid increased. Taking Core 1 as an example, at a water saturation of 80%, the relative permeability of gas decreased by 70.98%, while the relative permeability of liquid increased by 251.51%. This phenomenon can be attributed to the fact that the higher displacement pressure allowed the gas to more effectively overcome the obstruction of capillary forces, thereby occupying a larger portion of the flow channel and altering the shape of the gas–liquid interface. At the same time, the flow channels for the liquid became narrower and more complex, leading to increased flow resistance. The combined effect of these factors ultimately resulted in a decrease in the gas relative permeability and an increase in the liquid relative permeability.
As the displacement pressure gradually increased, the irreducible water saturation tended to decrease. During the process of increasing from 2 MPa to 5 MPa, the irreducible water saturation of the six samples decreased by 7.21%, 7.39%, 12.06%, 13.05%, 19.69%, and 22.52%, respectively. This was because, as the displacement pressure increased, it was able to overcome the binding effect of capillary forces, thereby breaking the bound state of water and leading to a decrease in the saturation of bound water. However, when the displacement pressure increases, it tends to flow preferentially along the “dominant path” with the least resistance. Once these dominant channels are established and connected, the gas will mainly migrate within these channels rather than continue to penetrate into the water in the non-dominant paths. A large amount of water is left behind, forming residual water, which leads to the residual water remaining high even when the displacement pressure difference is increased.
Under the same displacement pressure, the higher the permeability of the core, the lower the saturation of bound water. Taking a displacement pressure of 5 MPa as an example, the irreducible water saturation of the six samples decreased to 72.63%, 71.04%, 65.08%, 64.03%, 56.71%, and 53.09%, respectively. This is because rocks with high permeability have larger and more connected pore networks, making it easier for gas to form continuous phases and occupy more space, while water becomes more confined to smaller pores. As permeability further increased, the distribution of water tended to become more uneven, gathering more in areas with lower permeability, thereby reducing the saturation of bound water.

3.2. Determination of Irreducible Water Saturation Endpoint Based on NMR Centrifugation Method

Figure 7 shows a comparison of the nuclear magnetic resonance (NMR) curves of six cores under saturated water and a centrifugal force of 3 MPa. It can be seen from the figure that the curves show a downward trend under centrifugal force, indicating that the water in the cores has been displaced. The curves of Cores 5 and 6 show a significant decrease after 10 ms, suggesting a high degree of water displacement in the macropores. The water saturation after centrifugation was calculated by the nuclear magnetic resonance curves before and after centrifugation, as shown in Figure 8. As seen in Figure 8, the water saturation of the cores gradually decreases with an increase in centrifugal force. At low centrifugal forces, the decrease in water saturation is slower because the initial displacement pressure is insufficient to overcome capillary forces, causing water to remain trapped in the pores. At higher centrifugal forces, water saturation decreases rapidly, indicating that the displacement pressure is sufficient to overcome capillary forces, leading to the expulsion of more water.
Under the same centrifugal force, as the permeability of the core increased, the water saturation decreased. For example, when the centrifugal force was 3 MPa, the water saturation of the six core samples was 60.58%, 58.56%, 52.21%, 48.83%, 43.28%, and 41.93%, respectively. Core samples with higher permeability were more sensitive to changes in water saturation due to their well-developed pore structures, which offered less resistance to fluid flow. As a result, water was more easily expelled under the same centrifugal force. In contrast, rock cores with lower permeability were less sensitive to changes in water saturation because their complex pore structures significantly hindered fluid flow.

3.3. Differential Analysis of Irreducible Water Saturation Using Different Methods

A comparison of the non-reducible water saturation of Sample 1 under centrifugation and displacement conditions is shown in Figure 9. As seen in Figure 9, centrifugation effectively reduces the irreducible water saturation of rock cores, with reductions of 16.56%, 17.56%, 19.77%, 23.74%, 23.69%, and 21.01%, respectively, across the six rock cores. Figure 10 illustrates the distribution of pore water using both the non-steady-state displacement method and the centrifugal method. In tight sandstone reservoirs, formation water can be categorized into immobile bound water, mobile bound water, and mobile free water. Under displacement conditions, gas can form displacement channels, effectively displacing free water, which flows more easily through larger or smaller pores. However, water that is not easily displaced, such as that trapped in the reservoir rock surface, pore fissure corners, and microcapillary pores, remains difficult to remove. While the centrifugal method efficiently expels water from tight pores, the non-steady-state displacement method struggles to remove water from smaller pores and pore corners, where water remains trapped due to strong capillary forces. Furthermore, centrifugal action overcomes the adhesion forces between the rock surface and water, allowing the water to be expelled more quickly; the results are in agreement with the findings of Wang [26]. Despite this, some water remains trapped on the rock surface, in the corners of the pores, and in microcapillary channels, where strong adhesion forces between the water and rock prevent its expulsion. Taking Core #1 as an example, the actual irreducible water saturation (Swc) obtained using the 3 MPa centrifugation method shows a significant shift to the left on the phase permeability curve, compared to the critical water saturation (Swcrit) measured by the unsteady state method under a displacement pressure difference of 5 MPa.

4. Discussion

The non-steady state displacement experiment is effective in measuring the critical irreducible water saturation under different displacement pressure differentials. However, it does not fully capture the actual irreducible water saturation of the core, as laboratory conditions may not entirely replicate reservoir conditions. To ensure a phase permeability curve that accurately represents the permeability characteristics of the entire reservoir, it is essential to apply endpoint corrections to relative-permeability curves. This study employs the Stone equation for gas–water systems within tight sandstone reservoirs, building on the empirical model proposed by Baker et al. [24] for sandstone and mudstone. The Stone equation is particularly suitable for modeling relative permeability in tight sandstone reservoirs as it accounts for gas–water phase interactions while eliminating the influence of oil. In the gas–water system, the oil phase does not exist, that is, So = 0, the residual oil saturation is 0, and the terminal permeability symbols of the water phase and the gas phase are adjusted to the standard representation forms of the gas–water system, Krwirg and Krgcl. And the total saturation satisfies Sw + Sg = 1. Bound water saturation (Swc) and residual gas saturation (Sgcrit) have become the dominant parameters. Based on experimental observations and numerical fitting, the following parameters were determined (water phase index Nw = 1.5 and gas phase index Ng = 2.5). These values reflect the pore structure and fluid distribution within the cores and are crucial for normalizing the relative-permeability curves. The relationship between the water and gas phases was analyzed, leading to the following equation:
K r w = K r w i r g S w S w c 1 S w c N w
K r g = K r g c l S g S g c r i t 1 S g c r i t S w c N g
where Krwirg and Krgcl are the water phase permeability under residual gas and gas phase permeability under bound water, and Nw and Ng are the water phase index and gas phase index, respectively. These two parameters are determined by the pore structure of the rock. By using the interpolation method to continuously fit the normalized curve, the curvature of the experimental gas–water two-phase permeability curve is made to be the same as that of the normalized curve, and the fitting value in the experiment was Nw = 1.5, Ng = 2.5.
The relative-permeability curves of gas and water for different samples exhibit variations in terms of irreducible water saturation, residual gas saturation, the number of experimental data points, and the corresponding water saturation. Consequently, it is not feasible to directly use the curve of any single sample type as a comprehensive permeability curve that represents all samples. To address this issue, the normalization of these curves is required.
The relationship between irreducible water saturation and residual gas saturation was derived by fitting data from different permeability cores and displacement pressure differentials, as shown in Figure 11 and Figure 12. The corresponding expressions for displacement pressure difference, irreducible water saturation, and residual gas saturation are presented in Formulas (8) and (9).
S wcrit = a Δ P b
S gcrit = c Δ P d
The fitting coefficients (a, b, c, and d) were determined through regression analysis of experimental data, ensuring that the derived models accurately represent the irreducible water saturation and residual gas saturation for each core sample, as shown in Table 4.
In order to study the influence of different permeability cores on irreducible water saturation and residual gas saturation, the relationship between coefficients a, b, c, and d in Equations (8) and (9) and permeability was fitted as shown in Figure 13. The mathematical models of irreducible water saturation and residual gas saturation with permeability and displacement pressure difference were obtained, as shown in Equations (10) and (11).
S wcrit = 82.42 K 0.009 Δ P 0.23 K 0.16
S gcrit = 4.57 K 0.17 Δ P 0.72 K 0.04
The irreducible water saturation and residual gas saturation at different pressure differentials under reservoir permeability can be calculated using Equations (4) and (5). The resulting phase permeability curves are then normalized using Equations (6) and (7), with the normalized phase permeability curves shown in Figure 14.
To validate the accuracy of the proposed normalization method, a comparison was conducted with existing normalization models, including the Jone Park J model and Corey model. The result is shown in Figure 15. The Krg values in the Jone Park J model exceed 1, and the Krw values in the Jone Park J and Corey models fall below 0, both of which introduce significant errors. These discrepancies indicate that these models are not suitable for characterizing the gas–water relative permeability of high-water-content tight sandstone reservoirs. In contrast, the proposed normalization approach effectively eliminates inconsistencies across different samples and ensures a standardized representation of the reservoir’s permeability characteristics. This study established a robust normalization method for the gas–water relative-permeability curve of high-water-content tight sandstone gas reservoirs, which improved the accuracy of reservoir characterization and development planning. The normalized relative-permeability curve can be integrated into reservoir simulation models to more accurately predict fluid flow behavior and reservoir performance. This is crucial for optimizing development strategies such as well spacing, production rate, and injection schemes, which can help to improve gas recovery and reduce operating costs.

5. Conclusions

This study conducted experimental research on the gas–water phase permeability variations in high-water-content tight sandstone gas reservoirs of the Ordos Basin. The study analyzed the differences in irreducible water saturation obtained using different methods and constructed a normalized relative-permeability curve for gas–water flow in tight gas reservoirs. The key conclusions are as follows:
(1)
As the core permeability decreases from 0.027 mD to 1.149 mD, the irreducible water saturation significantly increases. Under a displacement pressure of 5 MPa, the immobile water saturation of the lowest permeability core reaches 72.63%, while the immobile water saturation of the highest permeability core decreases to 53.09%. When the displacement pressure difference increased from 2 MPa to 5 MPa, the average immobile water saturation of all cores decreased by about 15%, and the relative permeability of gas and water phases increased. The increase in displacement pressure helps to improve the overall permeability of the reservoir.
(2)
The centrifugal method effectively reduces irreducible water saturation in rock cores, and the irreducible water saturation of the core decreased by approximately 19% on average. While the gas displacement method forms displacement pathways that remove free water, particularly from larger pores, the centrifugal method can remove water from smaller capillary pores where water retention is stronger. This highlights the importance of selecting appropriate experimental techniques when evaluating water distribution in tight sandstone reservoirs.
(3)
A quantitative relationship between displacement pressure difference, critical irreducible water saturation, and residual gas saturation was established. Based on the Stone equation, this study proposes a normalized curve of gas–water relative permeability considering the true immovable water saturation condition. This model not only eliminates inconsistencies between different samples, but also provides a theoretical basis for predicting gas reservoir production performance and optimizing development strategies. The experimental verification results show that compared with the existing Jones Park J model and Corey model, the normalization method proposed in this study can more accurately characterize the gas–water relative-permeability characteristics of high-water-content tight sandstone gas reservoirs.
(4)
This study has made significant progress in revealing the gas–water relative-permeability characteristics of high-water-content tight sandstone gas reservoirs, but there are still some limitations. Firstly, there is a certain difference between the displacement pressure and the actual reservoir conditions, which may affect the universality of the experimental results. In addition, future research should also consider the impact of more influencing factors (such as stress sensitivity, capillary pressure hysteresis effect, etc.) on the relative permeability of gas and water.

Author Contributions

Conceptualization, B.H. and J.F.; methodology, K.C.; software, K.C.; validation, W.Y. and J.F.; formal analysis, J.D.; investigation, J.F.; resources, B.H.; data curation, W.Y. and K.C.; writing—original draft preparation, W.Y.; writing—review and editing, J.F.; visualization, J.D.; project administration, B.H.; funding acquisition, J.F. All authors have read and agreed to the published version of the manuscript.

Funding

This research was funded by the National Science Foundation Projects of China (52104022), the Science and Technology Research Project of Chongqing Municipal Education Commission (KJQN202401509), and the Natural Science Foundation of Chongqing (CSTB2024NSCQ-MSX0815).

Data Availability Statement

The data that support the findings of this study are available on request from the corresponding author, upon reasonable request.

Acknowledgments

The authors wish to thank the Sinopec North China Petroleum Bureau for providing samples and data access and for permission to publish this work. Additionally, the authors are thankful to the anonymous reviewers for reviewing this paper and their valuable comments and suggestions, which significantly improved the quality of this research. We are also grateful to the anonymous reviewers for their selfless contribution to the better publication and refinement of this paper.

Conflicts of Interest

The authors declare no conflicts of interest.

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Figure 1. Structure units and location of the study area in China.
Figure 1. Structure units and location of the study area in China.
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Figure 2. Distribution map of mineral content in tight sandstone.
Figure 2. Distribution map of mineral content in tight sandstone.
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Figure 3. Distribution of nuclear magnetic resonance curves in tight sandstone.
Figure 3. Distribution of nuclear magnetic resonance curves in tight sandstone.
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Figure 4. Schematic diagram of non-steady state infiltration test equipment.
Figure 4. Schematic diagram of non-steady state infiltration test equipment.
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Figure 5. MacroMR12-150H-VTHP NMR and centrifuge.
Figure 5. MacroMR12-150H-VTHP NMR and centrifuge.
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Figure 6. Gas–water relative-permeability curve. (a) Sample 1; (b) Sample 2; (c) Sample 3; (d) Sample 4; (e) Sample 5; (f) Sample 6.
Figure 6. Gas–water relative-permeability curve. (a) Sample 1; (b) Sample 2; (c) Sample 3; (d) Sample 4; (e) Sample 5; (f) Sample 6.
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Figure 7. Nuclear magnetic pore distribution curve before and after core centrifugation.
Figure 7. Nuclear magnetic pore distribution curve before and after core centrifugation.
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Figure 8. Relationship between water saturation and centrifugal force.
Figure 8. Relationship between water saturation and centrifugal force.
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Figure 9. Comparison of Bound Water in Permeation Curve.
Figure 9. Comparison of Bound Water in Permeation Curve.
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Figure 10. Non-steady state displacement method and centrifugal method pore water distribution. (a) Distribution of pore water in saturated rock cores. (b) The pore water distribution after gas flooding. (c) The pore water distribution after centrifugation. (Blue areas represent pore water; gray areas represent the rock matrix; white areas represent gas-filled pores.)
Figure 10. Non-steady state displacement method and centrifugal method pore water distribution. (a) Distribution of pore water in saturated rock cores. (b) The pore water distribution after gas flooding. (c) The pore water distribution after centrifugation. (Blue areas represent pore water; gray areas represent the rock matrix; white areas represent gas-filled pores.)
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Figure 11. The relationship between Swcrit and ΔP.
Figure 11. The relationship between Swcrit and ΔP.
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Figure 12. The relationship between Sgcrit and ∆P.
Figure 12. The relationship between Sgcrit and ∆P.
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Figure 13. (a) Coefficient a and permeability fitting curve. (b) Coefficient b and permeability fitting curve. (c) Coefficient c and permeability fitting curve. (d) Coefficient d and permeability fitting curve.
Figure 13. (a) Coefficient a and permeability fitting curve. (b) Coefficient b and permeability fitting curve. (c) Coefficient c and permeability fitting curve. (d) Coefficient d and permeability fitting curve.
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Figure 14. The relative-permeability curve under different pressure drop based on tone II equation.
Figure 14. The relative-permeability curve under different pressure drop based on tone II equation.
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Figure 15. Verification of relative-permeability normalization curve.
Figure 15. Verification of relative-permeability normalization curve.
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Table 1. Empirical formula for relative permeability.
Table 1. Empirical formula for relative permeability.
ScholarFormulas
Jone Park J [21] K r w = S w S w i r r 1 S w i r r 2
K r o = ( 1 S w ) 2.1 ( 1 S w i r r ) 2
Corey [22] S = S o 1 S w i r r
K r o = ( S ) 4
K r g = ( 1 S o 1 S w i r r ) 2 ( 1 S 2 )
Honarpour [23] K r w = K r w 0 ( S w S w i r r 1 S o r S w i r r ) n 1
K r o = K r o 0 ( 1 S w S o r 1 S o r S w i r r ) n 2
Baker [24] k r w = k r w i r o S r S w c r i t 1 S w c r i t S o i r w N w k r o w = k r o c w S o S o r w 1 S w c o n S o r w N o w k r o g = k r o g c g S l S o r g S w c o n 1 S g c o n S o r g S w c o n N o g k r g = k r gcl S g S g c r i t 1 S g c r i t S o r i g S w c o n N g
Table 2. Parameters of natural core samples.
Table 2. Parameters of natural core samples.
SampleDepth, mDiameter, cmLength,
cm
Porosity,
%
Permeability,
mD
#13547.182.55.842.140.027
#23063.782.55.354.790.149
#33489.642.55.675.250.286
#43491.202.55.895.970.439
#53628.642.56.086.940.763
#63504.552.55.9211.581.149
Table 3. Composition of the synthesized formation water.
Table 3. Composition of the synthesized formation water.
Salinity, mg/LWater TypepHConcentration, mg/L
K+ + Na+Ca2+Mg2+Ba2+Sr2+Fe2+SO42−HCO3Cl
48,126CaCl26.2780509906195.1158.777110646.221428,679
Table 4. Fitting result of Swcrit and Sgcrit of cores with different permeabilities.
Table 4. Fitting result of Swcrit and Sgcrit of cores with different permeabilities.
SamplePermeabilitySwcrit FormulaSgcrit Formula
#10.016 S w c r i t = 85.81 Δ P 0.12 S g c r i t = 2.17 Δ P 0.87
#20.027 S w c r i t = 84.81 Δ P 0.14 S g c r i t = 2.65 Δ P 0.83
#30.149 S w c r i t = 83.54 Δ P 0.15 S g c r i t = 3.27 Δ P 0.77
#40.563 S w c r i t = 82.88 Δ P 0.19 S g c r i t = 3.83 Δ P 0.73
#51.249 S w c r i t = 82.42 Δ P 0.23 S g c r i t = 4.67 Δ P 0.72
#61.735 S w c r i t = 81.99 Δ P 0.25 S g c r i t = 5.28 Δ P 0.71
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Hu, B.; Fu, J.; Yan, W.; Chen, K.; Ding, J. Normalization of Relative-Permeability Curves of Cores in High-Water-Content Tight Sandstone Gas Reservoir. Energies 2025, 18, 2335. https://doi.org/10.3390/en18092335

AMA Style

Hu B, Fu J, Yan W, Chen K, Ding J. Normalization of Relative-Permeability Curves of Cores in High-Water-Content Tight Sandstone Gas Reservoir. Energies. 2025; 18(9):2335. https://doi.org/10.3390/en18092335

Chicago/Turabian Style

Hu, Bo, Jingang Fu, Wenxin Yan, Kui Chen, and Jingchen Ding. 2025. "Normalization of Relative-Permeability Curves of Cores in High-Water-Content Tight Sandstone Gas Reservoir" Energies 18, no. 9: 2335. https://doi.org/10.3390/en18092335

APA Style

Hu, B., Fu, J., Yan, W., Chen, K., & Ding, J. (2025). Normalization of Relative-Permeability Curves of Cores in High-Water-Content Tight Sandstone Gas Reservoir. Energies, 18(9), 2335. https://doi.org/10.3390/en18092335

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