Measurement Uncertainty Estimation for Laser Doppler Anemometer

: Twenty percent of global electricity supplied to the buildings is used for preventing air temperature increase; its consumption for this prevention will triple by 2050 up to China’s present needs. Heat removed from the thermal power plants may drive cold generation in the absorption devices where mass and heat transfer are two-phase phenomena; hence liquid ﬁlm break-up into the rivulets is extensively investigated, which needs knowledge of the velocity proﬁles. Laminar ﬂow in a pipe is used in the preliminary study, velocity proﬁle of developed ﬂow is used as a benchmark. The study account writes the applied apparatus with their calibration procedure, and the uncertainty estimation algorithm. The calibration regression line with the slope close to one and a high Pearson’s coefﬁcient value is the ﬁnal outcome. Therefore, the apparatus may be applied in the principal research.


Introduction
Crisis in cold generation approaches the world's economy, for the air conditioners and electric fans working against air temperature increase need nearly 20% of the total electrical energy used in buildings in the world. Electricity demands for these purposes is forecasted to triple by 2050, which would equal China's present usage [1]. These demands reach the winter and summer peaks. Figure 1 shows the former in December and January and the latter in July and August; these seasonal peaks concern total energy production and its part generated in thermal power plants, from fossil fuels combustion, or radioactive decay [2].
Thermal power plants, in accordance with the second law of thermodynamics, need to remove heat to a heat sink which can be either surface water or a district heating system. However, in summer time, these systems supply heat only for generating domestic hot water, which may be insufficient; this insufficiency might be overcome with cold production, in the absorption refrigeration systems, from the removed heat temperatures of at least 80 • C [3]. In other words, the absorption refrigeration system might utilize heat that is removed from the thermal power plant during electricity generation. Absorption refrigeration systems might alternate from the traditional ones if they are equipped with compact and high-performance heat and mass exchangers [4]. A low usage of the absorption refrigeration systems stems from high ratio between the volume and the cooling capacity [5]. For this reason, they are also experimentally studied [6,7]. An absorption refrigerator uses two fluids, which change phases, and concentration flowing through the absorber, generator, evaporator, and condenser [8,9]. The change of phase or concentration occurs due to heat and mass transfer in thin liquid layers, which flow down a solid surface (cf. Figure 3 in [4]). Firstly, these layers were investigated because of the burnout in the steam boilers or distillatory equipment. Hartley and Murgatroyd [10] investigated liquid film break away into the rivulets using two approaches: the first one is mechanical equilibrium in the highest point of the dry patch, which results in the force balance in this point named stagnation point; the other method employs energy minimization, assuming the sum of kinetic energy across a plane and the surface energy approaches minimum. Bankoff [11] balanced flow rates and energies of the film and rivulets at the critical film thickness; it was assumed that a segment of circle as a cross-section of the rivulet, and the velocity profiles in film, and in each slice of the rivulet, are the same. Mikielewicz and Moszynski [12,13] applied minimization of energy extended by surface energy of the solid-gas interface. A common feature of the investigations presented above, in this paragraph, is assumed laminar velocity profile derived by Nusselt (1916) (cf. Madejski [14]); additionally, Hartley and Murgatroyd [10] assumed a linear laminar profile for film, motivated by surface shear only or a von Karman universal velocity profile for turbulent flow.
El-Genk and Saber [15] continued research into film breakdown, applying the energetic approach; their analysis includes a two-dimensional velocity profile solved using Ritz method. Perazzo and Gratton [16] derived another two-dimensional velocity profile, which is solved in closed form, for both the rivulet and film, flowing along a vertical plate; the contact angle was assumed to be either perpendicular to the plate for the rivulet or parallel for the film. While Tanasijczuk et al. [17] derived a two-dimensional velocity profile for a rivulet pending from a horizontal plate. The change of phase or concentration occurs due to heat and mass transfer in thin liquid layers, which flow down a solid surface (cf. Figure 3 in [4]). Firstly, these layers were investigated because of the burnout in the steam boilers or distillatory equipment. Hartley and Murgatroyd [10] investigated liquid film break away into the rivulets using two approaches: the first one is mechanical equilibrium in the highest point of the dry patch, which results in the force balance in this point named stagnation point; the other method employs energy minimization, assuming the sum of kinetic energy across a plane and the surface energy approaches minimum. Bankoff [11] balanced flow rates and energies of the film and rivulets at the critical film thickness; it was assumed that a segment of circle as a cross-section of the rivulet, and the velocity profiles in film, and in each slice of the rivulet, are the same. Mikielewicz and Moszynski [12,13] applied minimization of energy extended by surface energy of the solid-gas interface. A common feature of the investigations presented above, in this paragraph, is assumed laminar velocity profile derived by Nusselt (1916) (cf. Madejski [14]); additionally, Hartley and Murgatroyd [10] assumed a linear laminar profile for film, motivated by surface shear only or a von Karman universal velocity profile for turbulent flow.
El-Genk and Saber [15] continued research into film breakdown, applying the energetic approach; their analysis includes a two-dimensional velocity profile solved using Ritz method. Perazzo and Gratton [16] derived another two-dimensional velocity profile, which is solved in closed form, for both the rivulet and film, flowing along a vertical plate; the contact angle was assumed to be either perpendicular to the plate for the rivulet or parallel for the film. While Tanasijczuk et al. [17] derived a two-dimensional velocity profile for a rivulet pending from a horizontal plate.
Ataki and Bart [18] applied a velocity profile for a gravity driven rivulet along an inclined plate in the analysis of their experiments. Another assumption was the static contact angle value 56 • . Charogiannis et al. [19] experimentally determined laminar velocity profile for a gravity driven rivulet along an inclined plate for a Reynolds number less than 5.9 and Kapitza number equal to 1.4 following its definition: where σ is surface tension, g is gravitational acceleration, α is an inclination of film to the horizon, and ν is kinematic viscosity; they also obtain a profile for wavy flow forced with frequencies 2 and 6 Hz, when the Reynolds number was about 5.2. The very familiar configurations of the absorbers, applied in the absorption cooling systems, consists of the horizontal tubes, which are covered with falling liquid film; this film is an absorbent solution that, flowing across the tubes, absorbs the vapor of a refrigerant [4]. The flow divides into three regimes: falling-film flowing around the tubes, droplet-formation flow that occurs on, and in, the vicinity of the lowest tube generatrix, and the droplet-fall flow that appears between two tubes; these regimes exist for LiBr/water [20] and aqueous alkaline nitrate solution [4].
When the absorbent solution is overflowing the tubes, two phenomena are occurring simultaneously: heat and mass exchange, which are mathematically modeled using two different algorithms; modelling heat exchange needs a knowledge of film thickness, which is computed from a velocity profile. Despite different geometry, both Alvarez and Bourouis [4] and Jeong and Garimella [20] apply, in their models, a laminar velocity profile derived by Nusselt, mentioned above, derived for a flow along the vertical plate. Accordingly, the film thickness δ is obtained from formula where µ is dynamic viscosity, Γ is mass flowrate per unit of wetted tube, ρ is solution density.

Reynolds number for flowing film is defined by Equation [21]
Combining Equations (2) and (3) we obtain a formula for film thickness as a function of the Reynolds number: (4) Figure 2 shows a solution of Equation (4) for two Reynolds numbers: 100 and 1600; the latter is thought as the critical Reynolds number for films [21] which, under laminar flow, seems to be very thin, e.g., 0.5 mm or less under vertical flow; for the thicker films, a flow should not be laminar.
Therefore, an in-depth research into the velocity profiles of thin liquid layers would be helpful in modelling absorbers; it should indicate whether the velocity profile, beyond laminar flow, is two dimensional, turbulent, and whose formula models best model the flows. The experimental investigations of the velocity profiles in the rivulets and liquid films, for a Reynolds number in range from 400 to 3000 and Kapitza number 3000-6000, determined with laser Doppler anemometer (LDA) usage, is the main area of the investigation, which will be done for water flows along copper, aluminum, brass, and stainless steel plates. The particular goal of the published preliminary studies is measurement uncertainty estimation and calibration of an applied LDA system. Therefore, an in-depth research into the velocity profiles of thin liquid layers would be helpful in modelling absorbers; it should indicate whether the velocity profile, beyond laminar flow, is two dimensional, turbulent, and whose formula models best model the flows. The experimental investigations of the velocity profiles in the rivulets and liquid films, for a Reynolds number in range from 400 to 3000 and Kapitza number 3000-6000, determined with laser Doppler anemometer (LDA) usage, is the main area of the investigation, which will be done for water flows along copper, aluminum, brass, and stainless steel plates. The particular goal of the published preliminary studies is measurement uncertainty estimation and calibration of an applied LDA system.

Materials and Methods
The presented experimental investigations are carried out with an existing pipeline [22] that is shown as an internal loop in Figure 3. A researcher plugs in a pump (10) supplying water, through a discharge pipe (11), an upper tank (12), and an inlet pipe (13), to a transparent pipe (15). When the upper tank (12) is full and water is overflowing the brim of a pipe (22), and returning to a bottom tank (21), a valve (16) is opening. Then the assumed flow is fixed using the needle valve (19) and the flow meter (20). Afterwards the researcher runs a computer program, which sends out the proper signals to the Burst Spectrum Analyzer (BSA) (5) and the stepper motor controller (6). BSA (5) sends, through an optical fiber (3), two coherent laser beams to the flow explorer (2). These beams intersect in the assumed point after crossing the lens system in the front part of the flow explorer (2). Positioning the intersecting beam in the assumed points is provided by the stepper motor controller (6) sending the signals, through the wires (7), to the spindle drives; these drivers shift assembled elements of linear stroke (8) along x, y, and z axis. It turned out that milk is the most effective seeding substance.

Materials and Methods
The presented experimental investigations are carried out with an existing pipeline [22] that is shown as an internal loop in Figure 3. A researcher plugs in a pump (10) supplying water, through a discharge pipe (11), an upper tank (12), and an inlet pipe (13), to a transparent pipe (15). When the upper tank (12) is full and water is overflowing the brim of a pipe (22), and returning to a bottom tank (21), a valve (16) is opening. Then the assumed flow is fixed using the needle valve (19) and the flow meter (20). Afterwards the researcher runs a computer program, which sends out the proper signals to the Burst Spectrum Analyzer (BSA) (5) and the stepper motor controller (6). BSA (5) sends, through an optical fiber (3), two coherent laser beams to the flow explorer (2). These beams intersect in the assumed point after crossing the lens system in the front part of the flow explorer (2). Positioning the intersecting beam in the assumed points is provided by the stepper motor controller (6) sending the signals, through the wires (7), to the spindle drives; these drivers shift assembled elements of linear stroke (8) along x, y, and z axis. It turned out that milk is the most effective seeding substance.
Forasmuch as the velocity profile of the laminar flow is derived theoretically, and proved experimentally, it is used as a benchmark for the fluids flow velocity measurements; a velocity profile is determined with a Hagen-Poiseuille equation where ∂p ∂x means pressure gradient, r is radial distance, and R is the internal tube radius.  Forasmuch as the velocity profile of the laminar flow is derived theoretically, and proved experimentally, it is used as a benchmark for the fluids flow velocity measurements; a velocity profile is determined with a Hagen-Poiseuille equation where means pressure gradient, r is radial distance, and R is the internal tube radius.

The Optics System Adjustment
After a connection of the system of apparatus the laser beams intersect in any point; their intersection in the desired points is obtained as follows. Figure 4 shows the laser beams refract four times, from right to left, passing three isotropic media: air, Plexiglas, and water, so the basic equations system results from the law of refraction: where na, np, nw are the refractive indexes in air, Plexiglas, and water, respectively; θa, θp, and θw, are the angles between the laser beams in these media. The angle between the laser beams in air θa is obtained from the equation where d is a distance between the laser beams in the optics, f is the focal length of the optics in air.
After solving the Equations (6)-(8) we obtain the half angles of inclination in each medium:

The Optics System Adjustment
After a connection of the system of apparatus the laser beams intersect in any point; their intersection in the desired points is obtained as follows. Figure 4 shows the laser beams refract four times, from right to left, passing three isotropic media: air, Plexiglas, and water, so the basic equations system results from the law of refraction: n a sin θ a 2 = n p sin θ p 2 , where n a , n p , n w are the refractive indexes in air, Plexiglas, and water, respectively; θ a , θ p , and θ w , are the angles between the laser beams in these media.
(11) Figure 4 shows every beam to intersect must cover a fixed length d/2 along x axis where di = 30 mm is the internal tube diameter, and w = 5 mm is the tube wall thickness. Substituting Equations (8)-(12) we obtain where a = 116.11 mm is measured with calipers. Since d, f, w, di are known from the manufacturers' data, a is measured, and the half angles are computed earlier Equation (13) is solved for ya.   The angle between the laser beams in air θ a is obtained from the equation where d is a distance between the laser beams in the optics, f is the focal length of the optics in air. After solving the Equations (6)-(8) we obtain the half angles of inclination in each medium: θ w 2 = arcsin n a n w sin θ a 2 , θ p 2 = arcsin n a n p sin θ a 2 .
(11) Figure 4 shows every beam to intersect must cover a fixed length d/2 along x axis where d i = 30 mm is the internal tube diameter, and w = 5 mm is the tube wall thickness. Substituting Equations (8)-(12) we obtain where a = 116.11 mm is measured with calipers.
Since d, f, w, d i are known from the manufacturers' data, a is measured, and the half angles are computed earlier Equation (13) is solved for y a .
Then the ordinate y l0 is read on the linear stroke element (8) shown in Figure 3. The beams intersect in the point y 1 when a distance from the optics (2) is equal to the focal length f. Thus, a base ordinate y l1 on the linear stroke element (8) is calculated from the formula Figure 5 shows the course of the beams that intersect in an assumed measurement point in water at the distance y w from the internal wall, so every beam has to cover the fixed length: Equation (16) is solved for another y a : Then the corresponding ordinate y l on the linear stroke element (8) is computed from the formula y l = y l1 + ( f − y a ). Equation (16) is solved for another ya: Then the corresponding ordinate yl on the linear stroke element (8) is computed from the formula

Uncerainty Estimation
Overall uncertainty estimation follows the Moffat [23] approach. A fixed error Binst is equal to a difference of a benchmark laminar velocity vb (yi) and a mean of 30 velocity measurements Standard deviation σ for the arithmetic mean An overall uncertainty value δv (yi) is the square root of outsummed squares of the fixed error and doubled standard deviation because 95% confidence level is assumed.
The inverse of the squared the overall uncertainty value is a weight wi Since, in the lack of a flow, both velocities equal zero, a weighted regression line must cross origin; for that reason, the intercept b = 0 and the slope a is obtained with a formula [24]:

Uncerainty Estimation
Overall uncertainty estimation follows the Moffat [23] approach. A fixed error B inst is equal to a difference of a benchmark laminar velocity v b (y i ) and a mean of 30 velocity measurements v m (y i ) in each point of an ordinate y i along the tube diameter: Standard deviation σ for the arithmetic mean v m (y i ) is defined by an equation An overall uncertainty value δ v (y i ) is the square root of outsummed squares of the fixed error and doubled standard deviation because 95% confidence level is assumed.
The inverse of the squared the overall uncertainty value is a weight w i Since, in the lack of a flow, both velocities equal zero, a weighted regression line must cross origin; for that reason, the intercept b = 0 and the slope a is obtained with a formula [24]: and Pearson's correlation coefficient r is determined using an equation [24]:

Results and Discussion
The researcher adjusts the linear stroke element (8) at the location computed from Equation (18) for each of 31 measurement points along the diameter of the tube (15), and carries out the velocity measurements in these points; then, the researcher repeats the  Figure 6 shows the velocity profile from the averaged experimental results compared with the benchmark laminar flow for Re = 2137.

Results and Discussion
The researcher adjusts the linear stroke element (8) at the location computed from Equation (18) for each of 31 measurement points along the diameter of the tube (15), and carries out the velocity measurements in these points; then, the researcher repeats the measurement procedure 29 times. Figure 6 shows the velocity profile from the averaged experimental results compared with the benchmark laminar flow for Re = 2137. To assess quality of the experiments the regression line computed from Equation (23) is plotted in Figure 7 with the Pearson's coefficient value computed from Equation (24). To assess quality of the experiments the regression line computed from Equation (23) is plotted in Figure 7 with the Pearson's coefficient value computed from Equation (24). The great discrepancies occur in a close vicinity to one tube wall where the velocities in laminar flow vb are close to zero, and the measured velocities vm are about 30 times higher (cf. Figure 7); it may result from the thinner wall in this place, which, unfortunately, may not be checked with the simple measurements because of the long distance from the tube ends. Figure 8 shows an impact of radial distance determination on the velocity profile measurements; there are plotted vertical errors bars that are the differences between radial distance of the measured velocity and the coordinate of laminar velocity profile. The dif-  The great discrepancies occur in a close vicinity to one tube wall where the velocities in laminar flow v b are close to zero, and the measured velocities v m are about 30 times higher (cf. Figure 7); it may result from the thinner wall in this place, which, unfortunately, Energies 2021, 14, 3847 9 of 11 may not be checked with the simple measurements because of the long distance from the tube ends. Figure 8 shows an impact of radial distance determination on the velocity profile measurements; there are plotted vertical errors bars that are the differences between radial distance of the measured velocity and the coordinate of laminar velocity profile. The differences in the first half of the diameter that is closer to the LDA system, which corresponds to the lower part of Figure 8, are significantly less than in the second half beyond the tube axis; the one exception is the first point that was discussed above. The bigger discrepancies arise when the measurement volume approaches the axis, and the maximum is reached 6 mm beyond the tube axis (r/R = 0.4). Summarizing the discrepancies, between the benchmark laminar flow profile and the measured velocity profile, are an uncertain combination of the velocity and radial distance determination.

Conclusions
For as much as the gradient of the regression line is almost one, and the Pearson's correlation coefficient is greater than minimal value, which is equal to 0.3557 for 29 degrees of freedom at 95% confidence level, it might be said, in conclusion, that the preliminary experiments are performed in a proper way, and the high quality of the further principal research may be maintained.

Funding:
The paper was prepared at Students' Scientific Society "Heat Engineer" at Bialystok University of Technology and were financed by this university. The research was carried out at the Bialystok University of Technology at the Department of HVAC Engineering as the project WZ/WB-IIŚ/4/2019 and was subsidised by the Ministry of Science and Higher Education of the Republic of Poland from funding for statutory R&D activities. The research was conducted using equipment which was purchased thanks to either "INNO-EKO-TECH" Innovative research and didactic centre for alternative energy sources, energy efficient construction and environmental protectionproject implemented by the Technical University of Bialystok (PB), co-funded by the European Union through the European Regional Development Fund under the Programme Infrastructure and The errors in radial distance determination may be caused by other tube thickness in the measurement cross section, such as a non-circular cross section caused by several years of usage in the set-up, inappropriate adjustment of the element of linear stroke, different value of the refractive index, which might have been changed by the seeding particles.
Summarizing the discrepancies, between the benchmark laminar flow profile and the measured velocity profile, are an uncertain combination of the velocity and radial distance determination.

Conclusions
For as much as the gradient of the regression line is almost one, and the Pearson's correlation coefficient is greater than minimal value, which is equal to 0.3557 for 29 degrees of freedom at 95% confidence level, it might be said, in conclusion, that the preliminary experiments are performed in a proper way, and the high quality of the further principal research may be maintained.