Molbank2015, 2015(2), M854; doi:10.3390/M854 (registering DOI) - published 17 April 2015 Show/Hide Abstract
Abstract: The title compound was prepared by inducing amide bond formation between methyl 2-[(2-aminophenyl)ethynyl]benzoate and 2-[(2-acetamidophenyl)ethynyl]benzoic acid in the presence of dichlorotriphenylphosphorane. The structure of the synthesized compound was determined on the basis of its 1H-nuclear magnetic resonance (NMR), 13C-NMR, and mass spectral data. Furthermore, the compound’s crystal structure is also reported.
Molbank2015, 2015(2), M852; doi:10.3390/M852 - published 2 April 2015 Show/Hide Abstract
Abstract: A novel N-benzyl-(3E,5E)-3,5-bis(2-hydroxybenzylidene)-4-piperidone (3), was synthesized in good yield by a condensation reaction of 2-hydroxybenzaldehyde (1) and N-benzyl-4-piperidone (2) under microwave irradiation in the presence of 10% NaOH solution. The chemical structure was assigned on the basis of UV-visible, IR, 1H-NMR, 13C-NMR and mass spectral data.
Molbank2015, 2015(2), M851; doi:10.3390/M851 - published 1 April 2015 Show/Hide Abstract
Abstract: We report the synthesis of [(3-chlorobenzamido)methyl]triethylammonium chloride in a reaction of N-(chloromethyl)-3-chlorobenzamide and triethylamine in dry acetone. The structure of the newly synthesized compound was characterized with 1H-NMR, 13C-NMR, FTIR and Mass spectroscopy.
Molbank2015, 2015(2), M850; doi:10.3390/M850 - published 30 March 2015 Show/Hide Abstract
Abstract: The title indole-based compound that enforces tripodal topology and is potential applicable for the use as artificial receptor, was prepared by a simple reaction of 1,3,5-benzenetricarbonyl trichloride with 5-methoxytryptamine. The compound was characterized by elemental analysis, 1H-NMR, 13C-NMR and mass spectrometry.
Molbank2015, 2015(1), M849; doi:10.3390/M849 - published 18 March 2015 Show/Hide Abstract
Abstract: The title compound (2) was prepared in high yield by catalytic transfer hydrogenation of the 6-nitro precursor (1), using hydrazine hydrate as the hydrogen source. Under the conditions employed, the ester groups remain unaffected. The new compound was fully characterised by elemental analysis, 1H-NMR, 13C-NMR, MS and HRMS data.