Crystals 2012, 2(2), 176-181; doi:10.3390/cryst2020176
Communication

The Synthesis and Molecular Structure of 2-(4-Methoxybenzyl)-4-nitro-2H-indazole

1, 2email and 1,* email
Received: 23 December 2011; in revised form: 21 February 2012 / Accepted: 23 March 2012 / Published: 10 April 2012
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Abstract: Two novel indazole derivatives protected with p-methoxybenzyl group were synthesized and characterized. The crystal and molecular structure of 2-(4-methoxybenzyl)-4-nitro-2H-indazole as one out of the two regioisomers is reported. The compound was obtained from a saturated petroleum ether/ethyl acetate mixture and crystallizes in the triclinic space group P`1. The unit cell parameters are: a = 6.8994(1) Å, b = 9.8052(2) Å, c = 11.1525(2) Å; α = 71.729(1)°, β = 79.436(1)°, γ = 74.349(1)° and V = 685.83(2) Å3. There are two independent molecules found in the asymmetric unit.
Keywords: indazoles; protecting group; p-methoxy benzyl; X-ray structure
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MDPI and ACS Style

Ebert, K.; Köckerling, M.; Mamat, C. The Synthesis and Molecular Structure of 2-(4-Methoxybenzyl)-4-nitro-2H-indazole. Crystals 2012, 2, 176-181.

AMA Style

Ebert K, Köckerling M, Mamat C. The Synthesis and Molecular Structure of 2-(4-Methoxybenzyl)-4-nitro-2H-indazole. Crystals. 2012; 2(2):176-181.

Chicago/Turabian Style

Ebert, Kristin; Köckerling, Martin; Mamat, Constantin. 2012. "The Synthesis and Molecular Structure of 2-(4-Methoxybenzyl)-4-nitro-2H-indazole." Crystals 2, no. 2: 176-181.

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