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Crystals 2012, 2(1), 90-95; doi:10.3390/cryst2010090

Synthesis and Molecular Structure of tert-Butyl 4-(2-tert-butoxy-2-oxoethyl)piperazine-1-carboxylate

1
Institut für Radiopharmazie, Helmholtz-Zentrum Dresden-Rossendorf, Bautzner Landstraße 400, D 01328 Dresden, Germany
2
Institut für Chemie, Anorganische Festkörperchemie, Albert-Einstein-Straße 3a, D 18059 Rostock, Germany
*
Author to whom correspondence should be addressed.
Received: 20 December 2011 / Revised: 30 January 2012 / Accepted: 31 January 2012 / Published: 6 February 2012
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Abstract

The crystal and molecular structure of tert-butyl 4-(2-tert-butoxy-2-oxoethyl)-piperazine-1-carboxylate is reported. The title compound crystallizes from a petroleum ether/ethyl acetate mixture in the monoclinic space group P 21/c with four molecules in the unit cell. The unit cell parameters are: a = 8.4007(2) Å, b = 16.4716(4) Å, c = 12.4876(3) Å; β = 90.948(1)° and V = 1727.71(7) Å3. Bond lengths and angles of this piperazine-carboxylate are typical.
Keywords: piperazines; building blocks; X-ray structure piperazines; building blocks; X-ray structure
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Mamat, C.; Flemming, A.; Köckerling, M. Synthesis and Molecular Structure of tert-Butyl 4-(2-tert-butoxy-2-oxoethyl)piperazine-1-carboxylate. Crystals 2012, 2, 90-95.

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