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Crystals 2012, 2(1), 90-95; doi:10.3390/cryst2010090
Communication

Synthesis and Molecular Structure of tert-Butyl 4-(2-tert-butoxy-2-oxoethyl)piperazine-1-carboxylate

1,* , 2 and 2
1 Institut für Radiopharmazie, Helmholtz-Zentrum Dresden-Rossendorf, Bautzner Landstraße 400, D 01328 Dresden, Germany 2 Institut für Chemie, Anorganische Festkörperchemie, Albert-Einstein-Straße 3a, D 18059 Rostock, Germany
* Author to whom correspondence should be addressed.
Received: 20 December 2011 / Revised: 30 January 2012 / Accepted: 31 January 2012 / Published: 6 February 2012
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Abstract

The crystal and molecular structure of tert-butyl 4-(2-tert-butoxy-2-oxoethyl)-piperazine-1-carboxylate is reported. The title compound crystallizes from a petroleum ether/ethyl acetate mixture in the monoclinic space group P 21/c with four molecules in the unit cell. The unit cell parameters are: a = 8.4007(2) Å, b = 16.4716(4) Å, c = 12.4876(3) Å; β = 90.948(1)° and V = 1727.71(7) Å3. Bond lengths and angles of this piperazine-carboxylate are typical.
Keywords: piperazines; building blocks; X-ray structure piperazines; building blocks; X-ray structure
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Mamat, C.; Flemming, A.; Köckerling, M. Synthesis and Molecular Structure of tert-Butyl 4-(2-tert-butoxy-2-oxoethyl)piperazine-1-carboxylate. Crystals 2012, 2, 90-95.

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