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Materials 2014, 7(5), 3427-3434; doi:10.3390/ma7053427

Annealing Effect on the Structural and Optical Properties of Sputter-Grown Bismuth Titanium Oxide Thin Films

1
Grupo de ciencia de materiales y superficies, Universidad Nacional de Colombia, Bogotá AA 14490, Colombia
2
Centro Internacional de Física (CIF), Bogotá AA 14490, Colombia
3
Grupo de Análisis de Fallas, Integridad y Superficies (AFIS), Universidad Nacional de Colombia, Bogotá AA 14490, Colombia
4
Physics, Chemistry, Mathematics Computational Applications (PCM), Universidad Nacional de Colombia, Manizales AA 127, Colombia
5
Laser Processing Group, Instituto de Optica, CSIC, c/Serrano 121, Madrid 28006, Spain
*
Author to whom correspondence should be addressed.
Received: 22 January 2014 / Revised: 25 March 2014 / Accepted: 28 March 2014 / Published: 30 April 2014
(This article belongs to the Section Structure Analysis and Characterization)
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Abstract

The aim of this work is to assess the evolution of the structural and optical properties of BixTiyOz films grown by rf magnetron sputtering upon post-deposition annealing treatments in order to obtain good quality films with large grain size, low defect density and high refractive index similar to that of single crystals. Films with thickness in the range of 220–250 nm have been successfully grown. After annealing treatment at 600 °C the films show excellent transparency and full crystallization. It is shown that to achieve larger crystallite sizes, up to 17 nm, it is better to carry the annealing under dry air than under oxygen atmosphere, probably because the nucleation rate is reduced. The refractive index of the films is similar under both atmospheres and it is very high (n =2.5 at 589 nm). However it is still slightly lower than that of the single crystal value due to the polycrystalline morphology of the thin films. View Full-Text
Keywords: thin films; optical characterization; refractive index thin films; optical characterization; refractive index
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Alfonso, J.E.; Olaya, J.J.; Bedoya-Hincapié, C.M.; Toudert, J.; Serna, R. Annealing Effect on the Structural and Optical Properties of Sputter-Grown Bismuth Titanium Oxide Thin Films. Materials 2014, 7, 3427-3434.

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