Previous Article in Journal
Previous Article in Special Issue
Dimethyl 2,2′-[Carbonylbis(azanediyl)](2S,2′S)-bis[3-(4-hydroxyphenyl)propanoate]
Article Menu

Export Article

Open AccessShort Note
Molbank 2018, 2018(1), M988; doi:10.3390/M988


Department of Chemistry, Life Sciences and Environmental Sustainability (SCVSA), University of Parma, Parco Area delle Scienze 17/A, 43124 Parma, Italy
Author to whom correspondence should be addressed.
Received: 20 February 2018 / Revised: 9 March 2018 / Accepted: 10 March 2018 / Published: 12 March 2018
(This article belongs to the Special Issue Molecules from Catalytic Processes)
View Full-Text   |   Download PDF [4383 KB, uploaded 13 March 2018]   |  


The title compound—cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5-isopropoxy-9H-tribenzo[b,f]azepine—was synthesized in 83% isolated yield by a palladium-catalyzed one-pot strategy from 1-iodo-2-isopropoxybenzene and ortho-bromoaniline. The azepine derivative was fully characterized (FT-IR, MS, 1H and 13C-NMR, elemental analysis) and all proton and carbon signals have been completely assigned by 2D NMR experiments. View Full-Text
Keywords: palladium; norbornene; benzo[b,f]azepine; C-C and C-N couplings; multicomponent; one-pot reaction palladium; norbornene; benzo[b,f]azepine; C-C and C-N couplings; multicomponent; one-pot reaction

This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).

Supplementary materials

Scifeed alert for new publications

Never miss any articles matching your research from any publisher
  • Get alerts for new papers matching your research
  • Find out the new papers from selected authors
  • Updated daily for 49'000+ journals and 6000+ publishers
  • Define your Scifeed now

SciFeed Share & Cite This Article

MDPI and ACS Style

Casnati, A.; Motti, E.; Ca’, N.D. Cis,exo-1,2,3,4,4a,13b-hexahydro-1,4-methano-5-isopropoxy-9H-tribenzo[b,f]azepine. Molbank 2018, 2018, M988.

Show more citation formats Show less citations formats

Note that from the first issue of 2016, MDPI journals use article numbers instead of page numbers. See further details here.

Related Articles

Article Metrics

Article Access Statistics



[Return to top]
Molbank EISSN 1422-8599 Published by MDPI AG, Basel, Switzerland RSS E-Mail Table of Contents Alert
Back to Top