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Molbank 2013, 2013(3), M803; doi:10.3390/M803

N-(2-Chloro-5-cyanophenyl)-4,4,4-trifluorobutanamide

1
Center for Advanced Materials, Department of Chemistry, Tumkur University, Tumkur-572103, India
2
Tadimety Aromatics Pvt. Ltd, Hirehalli Industrial Area, Tumkur-572168, India
*
Author to whom correspondence should be addressed.
Received: 27 May 2013 / Revised: 19 June 2013 / Accepted: 20 June 2013 / Published: 28 June 2013
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Abstract

N-(2-Chloro-5-cyanophenyl)-4,4,4-trifluorobutanamide (3) was synthesized by reacting 4,4,4-trifluorobutanoic acid (1) with 2-amino-4-chlorobenzonitrile (2) in the presence of triethylamine and propylphosphonic anhydride in ethyl acetate. Character­ization of the compound was done by IR, 1H-NMR, 13C-NMR, LC-MS and CHN analysis.
Keywords: N-(2-chloro-5-cyanophenyl)-4,4,4-trifluorobutanamide; propylphosphonic anhydride; 4,4,4-trifluorobutanoic acid; 2-amino-4-chlorobenzonitrile. N-(2-chloro-5-cyanophenyl)-4,4,4-trifluorobutanamide; propylphosphonic anhydride; 4,4,4-trifluorobutanoic acid; 2-amino-4-chlorobenzonitrile.
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This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Manojkumar, K.E.; Sreenivasa, S.; Shivaraja, G.; Rao, T.M.C. N-(2-Chloro-5-cyanophenyl)-4,4,4-trifluorobutanamide. Molbank 2013, 2013, M803.

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