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- re-usable
Molbank 2010, 2010(1), M661; doi:10.3390/M661
Short Note
(2-Chlorophenyl)-3-methylchromeno[2,3-c]pyrazol-4(1H)-one
Department of Drug and Natural Product Synthesis, Faculty of Life Sciences, University of Vienna, Althanstrasse 14, A-1090 Vienna, Austria
* Author to whom correspondence should be addressed.
Received: 9 February 2010 / Accepted: 8 March 2010 / Published: 9 March 2010
Abstract: The title compound was prepared by treatment of 1-(2-chlorophenyl)-3-methyl-2-pyrazolin-5-one with 2-chlorobenzoyl chloride / Ca(OH)2 in 1,4-dioxane and subsequent cyclization of the thus obtained 4-aroyl-5-hydroxypyrazole with sodium hydride in dry DMF. Detailed spectroscopic data (1H NMR, 13C NMR, 15N NMR, IR, MS) are presented.
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MDPI and ACS Style
Batezila, G.; Holzer, W. (2-Chlorophenyl)-3-methylchromeno[2,3-c]pyrazol-4(1H)-one. Molbank 2010, 2010, M661.
AMA StyleBatezila G., Holzer W. (2-Chlorophenyl)-3-methylchromeno[2,3-c]pyrazol-4(1H)-one. Molbank. 2010; 2010(1):M661.
Chicago/Turabian StyleBatezila, Giselle; Holzer, Wolfgang. 2010. "(2-Chlorophenyl)-3-methylchromeno[2,3-c]pyrazol-4(1H)-one." Molbank 2010, no. 1: M661.
Molbank
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