6-(4-(2-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-10-oxa-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione)

doi:10.3390/M638

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Molbank 2009, 2009(4), M638; doi:10.3390/M638

Short Note

6-(4-(2-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-10-oxa-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione)

David M. Gooden

Small Molecule Synthesis Facility, Duke University, Durham, NC 27708, USA

Received: 9 October 2009 / Accepted: 2 November 2009 / Published: 5 November 2009

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Abstract: Microwave irradiation of maleimide with an excess of furan in water exclusively yields the corresponding exo-cycloadduct in good yield (87%) in 1 hour at 90 oC. Alkylation of the imido nitrogen with tetraethylene glycol under Mitsunobu conditions gives the ROMP monomer in 81% yield.

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Cite This Article

MDPI and ACS Style

Gooden, D.M. 6-(4-(2-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-10-oxa-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione). Molbank 2009, 2009, M638.

AMA Style

Gooden D.M. 6-(4-(2-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-10-oxa-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione). Molbank. 2009; 2009(4):M638.

Chicago/Turabian Style

Gooden, David M. 2009. "6-(4-(2-{2-[2-(2-Hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-10-oxa-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione)." Molbank 2009, no. 4: M638.

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