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Department of Drug and Natural Product Synthesis, Faculty of Life Sciences, University of Vienna, Althanstrasse 14, A-1090 Vienna, Austria
Institute of Synthetic Chemistry, Kaunas University of Technology, Radvilenu pl. 19, LT-50254 Kaunas, Lithuania
* Author to whom correspondence should be addressed.
Received: 14 September 2009; Accepted: 18 September 2009 / Published: 21 September 2009
Abstract: Reaction of 5-chloro-1,3-dimethyl-1H-pyrazole with I2/HIO3 in refluxing acetic acid gives the title compound in good yield. Detailed spectroscopic data (1H NMR, 13C NMR, 15N NMR, IR, MS) are presented.
Keywords: pyrazole; iodination; NMR spectroscopy
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Vilkauskaitė, G.; Eller, G.A.; Šačkus, A.; Holzer, W. 5-Chloro-4-iodo-1,3-dimethyl-1H-pyrazole. Molbank 2009, 2009, M620.
Vilkauskaitė G, Eller GA, Šačkus A, Holzer W. 5-Chloro-4-iodo-1,3-dimethyl-1H-pyrazole. Molbank. 2009; 2009(3):M620.
Vilkauskaitė, Gytė; Eller, Gernot A.; Šačkus, Algirdas; Holzer, Wolfgang. 2009. "5-Chloro-4-iodo-1,3-dimethyl-1H-pyrazole." Molbank 2009, no. 3: M620.