Next Article in Journal
Synthesis of 4-[10H-Phenothiazin-10-yl(1H-tetrazol-5-yl)-methyl]phenol
Previous Article in Journal
Regioselective Alkylation of an Oxonaphthalene-Annelated Pyrrol System
Molbank 2009, 2009(3), M620; doi:10.3390/M620
Short Note

5-Chloro-4-iodo-1,3-dimethyl-1H-pyrazole

1,2, 1, 2 and 1,*
1 Department of Drug and Natural Product Synthesis, Faculty of Life Sciences, University of Vienna, Althanstrasse 14, A-1090 Vienna, Austria 2 Institute of Synthetic Chemistry, Kaunas University of Technology, Radvilenu pl. 19, LT-50254 Kaunas, Lithuania
* Author to whom correspondence should be addressed.
Received: 14 September 2009 / Accepted: 18 September 2009 / Published: 21 September 2009
Download PDF [141 KB, uploaded 21 September 2009]

Abstract

Reaction of 5-chloro-1,3-dimethyl-1H-pyrazole with I2/HIO3 in refluxing acetic acid gives the title compound in good yield. Detailed spectroscopic data (1H NMR, 13C NMR, 15N NMR, IR, MS) are presented.
Keywords: pyrazole; iodination; NMR spectroscopy pyrazole; iodination; NMR spectroscopy
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Supplements

Share & Cite This Article

Further Mendeley | CiteULike
Export to BibTeX |
EndNote
MDPI and ACS Style

Vilkauskaitė, G.; Eller, G.A.; Šačkus, A.; Holzer, W. 5-Chloro-4-iodo-1,3-dimethyl-1H-pyrazole. Molbank 2009, 2009, M620.

View more citation formats

Article Metrics

For more information on the journal, click here

Comments

Cited By

[Return to top]
Molbank EISSN 1422-8599 Published by MDPI AG, Basel, Switzerland RSS E-Mail Table of Contents Alert