Next Article in Journal
Synthesis and Spectroscopic Characterisation of N-Alkyl Quaternary Ammonium Salts Typical Precursors of Cyanines
Previous Article in Journal
Alkaloids Induce Programmed Cell Death in Bloodstream Forms of Trypanosomes (Trypanosoma b. brucei)
Molecules 2002, 7(2), 315-319; doi:10.3390/70200315
Article

Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one

*  and
Received: 23 January 2002 / Revised: 25 February 2002 / Accepted: 26 February 2002 / Published: 28 February 2002
Download PDF [26 KB, uploaded 18 June 2014]

Abstract

The synthesis of a new spirolactone is described. The title compound is obtained as a white solid in 46% yield from 3-(4-hydroxy-2-methoxyphenyl)propanoic acid using [Bis(trifluoroacetoxy)iodo]benzene (PIFA) as the oxidant.
Keywords: Spiroannulation; oxidation; phenol; spirolactone; PIFA Spiroannulation; oxidation; phenol; spirolactone; PIFA
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Share & Cite This Article

Further Mendeley | CiteULike
Export to BibTeX |
EndNote
MDPI and ACS Style

Plourde, G.L.; Fisher, B.B. Synthesis of 6-Methoxy-1-oxaspiro[4,5]deca-6,9-diene-8-one. Molecules 2002, 7, 315-319.

View more citation formats

Related Articles

Article Metrics

For more information on the journal, click here

Comments

Cited By

[Return to top]
Molecules EISSN 1420-3049 Published by MDPI AG, Basel, Switzerland RSS E-Mail Table of Contents Alert