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Molecules 2002, 7(11), 810-812; doi:10.3390/71100810

Easy Preparation of [Bis(trifluoroacetoxy)iodo]arenes from Iodoarenes, with Sodium Percarbonate as the Oxidant

Chair and Laboratory of Organic Chemistry, Faculty of Pharmacy, Medical University, PL 02-097, 1 Banacha Street, Warsaw, Poland
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Received: 15 October 2002 / Revised: 21 October 2002 / Accepted: 21 October 2002 / Published: 30 November 2002
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Abstract

Easy and effective preparations of the nearly pure [bis(trifluoroacetoxy)-iodo]arenes, ArI(OCOCF)3, from some iodoarenes, ArI, are reported, using an anhydrous sodium percarbonate/(CF3CO)2O/CH2Cl2 system. The colorless, freshly prepared ArI(OCOCF3)2 thus obtained were 98-99% pure (by iodometry).
Keywords: [Bis(trifluoroacetoxy)iodo]arenes from iodoarenes; sodium percarbonate as oxidant [Bis(trifluoroacetoxy)iodo]arenes from iodoarenes; sodium percarbonate as oxidant
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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MDPI and ACS Style

Kazmierczak, P.; Skulski, L. Easy Preparation of [Bis(trifluoroacetoxy)iodo]arenes from Iodoarenes, with Sodium Percarbonate as the Oxidant. Molecules 2002, 7, 810-812.

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