Next Article in Journal
Nα-Urocanylhistamine: A Natural Histamine Derivative
Previous Article in Journal
Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant
Molecules 2002, 7(11), 810-812; doi:10.3390/71100810
Article

Easy Preparation of [Bis(trifluoroacetoxy)iodo]arenes from Iodoarenes, with Sodium Percarbonate as the Oxidant

 and *
Chair and Laboratory of Organic Chemistry, Faculty of Pharmacy, Medical University, PL 02-097, 1 Banacha Street, Warsaw, Poland
* Author to whom correspondence should be addressed.
Received: 15 October 2002 / Revised: 21 October 2002 / Accepted: 21 October 2002 / Published: 30 November 2002
View Full-Text   |   Download PDF [17 KB, uploaded 18 June 2014]   |   Browse Figure

Abstract

Easy and effective preparations of the nearly pure [bis(trifluoroacetoxy)-iodo]arenes, ArI(OCOCF)3, from some iodoarenes, ArI, are reported, using an anhydrous sodium percarbonate/(CF3CO)2O/CH2Cl2 system. The colorless, freshly prepared ArI(OCOCF3)2 thus obtained were 98-99% pure (by iodometry).
Keywords: [Bis(trifluoroacetoxy)iodo]arenes from iodoarenes; sodium percarbonate as oxidant [Bis(trifluoroacetoxy)iodo]arenes from iodoarenes; sodium percarbonate as oxidant
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).
SciFeed

Share & Cite This Article

Further Mendeley | CiteULike
Export to BibTeX |
EndNote |
RIS
MDPI and ACS Style

Kazmierczak, P.; Skulski, L. Easy Preparation of [Bis(trifluoroacetoxy)iodo]arenes from Iodoarenes, with Sodium Percarbonate as the Oxidant. Molecules 2002, 7, 810-812.

View more citation formats

Related Articles

Article Metrics

For more information on the journal, click here

Comments

[Return to top]
Molecules EISSN 1420-3049 Published by MDPI AG, Basel, Switzerland RSS E-Mail Table of Contents Alert