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Molecules 1999, 4(10), 310-315; doi:10.3390/41000310
Article

Trimethylcyanosilane as a Convenient Reagent for the Preparation of Trimethylsilyl Enol Ethers of 1,3-Diketones

College of Pharmacy, The Ohio State University, Columbus, Ohio 43221, USA
Received: 22 August 1999 / Accepted: 12 September 1999 / Published: 10 October 1999
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Abstract

Trimethylsilyl enol ethers of 1,3-diketones are generated “in situ” or obtained in high isolated yield by the reaction of 1,3-diketones with trimethylcyanosilane in various solvents such as cyclohexane, hexane, benzene, methylene chloride, chloroform, carbon tetrachloride, and acetonitrile.
Keywords: Trimethylcyanosilane; Silylation; 1; 3-Diketones; Trimethylsilyl enol ethers Trimethylcyanosilane; Silylation; 1; 3-Diketones; Trimethylsilyl enol ethers
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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Zhuo, J.-C. Trimethylcyanosilane as a Convenient Reagent for the Preparation of Trimethylsilyl Enol Ethers of 1,3-Diketones. Molecules 1999, 4, 310-315.

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