Synthesis and Single Crystal Structures of Substituted-1,3-Selenazol-2-amines†
AbstractThe synthesis and X-ray single crystal structures of a series of new 4-substituted-1,3-selenazol-2-amines is reported. The efficient preparation of these compounds was carried out by two-component cyclization of the selenoureas with equimolar amounts of α-haloketones. The selenoureas were obtained from the reaction of Woollins’ reagent with cyanamides, followed by hydrolysis with water. All new compounds have been characterized by IR spectroscopy, multi-NMR (1H, 13C, 77Se) spectroscopy, accurate mass measurement and single crystal X-ray structure analysis. View Full-Text
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Hua, G.; Du, J.; Slawin, A.M.Z.; Woollins, J.D. Synthesis and Single Crystal Structures of Substituted-1,3-Selenazol-2-amines. Molecules 2017, 22, 46.
Hua G, Du J, Slawin AMZ, Woollins JD. Synthesis and Single Crystal Structures of Substituted-1,3-Selenazol-2-amines. Molecules. 2017; 22(1):46.Chicago/Turabian Style
Hua, Guoxiong; Du, Junyi; Slawin, Alexandra M.Z.; Woollins, J. D. 2017. "Synthesis and Single Crystal Structures of Substituted-1,3-Selenazol-2-amines." Molecules 22, no. 1: 46.
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