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Molecules 2013, 18(10), 13111-13123; doi:10.3390/molecules181013111

Synthesis and Structural Characterization of Fluorinated Thiosemicarbazones

2, 3
1 Facultad de Ciencias Químicas, Universidad Autónoma Benito Juárez de Oaxaca. Av. Universidad S/N Cinco Señores, Oaxaca de Juárez, Oaxaca 68000, Mexico 2 Facultad de Química, UNAM, Cd. Universitaria, 04510 México D.F., Mexico 3 Departamento de Química, CINVESTAV, Av. Instituto Politécnico Nacional No. 2508, San Pedro Zacatenco, México 07360, Mexico
* Author to whom correspondence should be addressed.
Received: 10 September 2013 / Revised: 10 October 2013 / Accepted: 11 October 2013 / Published: 22 October 2013
(This article belongs to the Section Organic Synthesis)
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Six new fluorinated thiosemicarbazones R‑C(R′)=N-NH-C(S)NH2 (R = 2,4-C6H3F2, R′ = H (1); R = 2,5-C6H3F2, R′ = H (2); R = 2,6-C6H3F2, R′ = H (3); R = 3,4-C6H3F2, R′ = H (4); R = 3,5-C6H3F2, R′ = H (5) and R = 4-C6H4F, R′ = C6H5, (6)) have been prepared. The molecular structures of compounds 1 to 6 have been determined.
Keywords: fluorobenzaldehyde; sulfur; thiosemicarbazones; crystal structure fluorobenzaldehyde; sulfur; thiosemicarbazones; crystal structure
This is an open access article distributed under the Creative Commons Attribution License (CC BY) which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Bautista, J.L.; Flores-Alamo, M.; Tiburcio, J.; Vieto, R.; Torrens, H. Synthesis and Structural Characterization of Fluorinated Thiosemicarbazones. Molecules 2013, 18, 13111-13123.

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