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Molecules 2013, 18(10), 13111-13123; doi:10.3390/molecules181013111
Article

Synthesis and Structural Characterization of Fluorinated Thiosemicarbazones

1
,
2, 3
,
2
 and
2,*
1 Facultad de Ciencias Químicas, Universidad Autónoma Benito Juárez de Oaxaca. Av. Universidad S/N Cinco Señores, Oaxaca de Juárez, Oaxaca 68000, Mexico 2 Facultad de Química, UNAM, Cd. Universitaria, 04510 México D.F., Mexico 3 Departamento de Química, CINVESTAV, Av. Instituto Politécnico Nacional No. 2508, San Pedro Zacatenco, México 07360, Mexico
* Author to whom correspondence should be addressed.
Received: 10 September 2013 / Revised: 10 October 2013 / Accepted: 11 October 2013 / Published: 22 October 2013
(This article belongs to the Section Organic Synthesis)
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Abstract

Six new fluorinated thiosemicarbazones R‑C(R′)=N-NH-C(S)NH2 (R = 2,4-C6H3F2, R′ = H (1); R = 2,5-C6H3F2, R′ = H (2); R = 2,6-C6H3F2, R′ = H (3); R = 3,4-C6H3F2, R′ = H (4); R = 3,5-C6H3F2, R′ = H (5) and R = 4-C6H4F, R′ = C6H5, (6)) have been prepared. The molecular structures of compounds 1 to 6 have been determined.
Keywords: fluorobenzaldehyde; sulfur; thiosemicarbazones; crystal structure fluorobenzaldehyde; sulfur; thiosemicarbazones; crystal structure
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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Bautista, J.L.; Flores-Alamo, M.; Tiburcio, J.; Vieto, R.; Torrens, H. Synthesis and Structural Characterization of Fluorinated Thiosemicarbazones. Molecules 2013, 18, 13111-13123.

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