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Molecules 2009, 14(1), 474-479; doi:10.3390/molecules14010474
Article

Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative Yields

 and *
Organic Chemistry Research Laboratory, Department of Chemistry, Iran University of Science and Technology, 16846 Tehran, Iran
* Author to whom correspondence should be addressed.
Received: 26 November 2008 / Revised: 13 January 2009 / Accepted: 14 January 2009 / Published: 19 January 2009
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Abstract

Solvent-free synthesis of pyrano[2,3-d]pyrimidine-2,4(1H,3H)-diones by ball-milling and without any catalyst is described. This method provides several advantages such as being environmentally friendly, using a simple workup procedure, and affording high yields.
Keywords: Solvent-free reaction; Barbituric acid; Pyrimidinediones; Heterocyclic compounds; Ball-milling Solvent-free reaction; Barbituric acid; Pyrimidinediones; Heterocyclic compounds; Ball-milling
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Mashkouri, S.; Reza Naimi-Jamal, M. Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative Yields. Molecules 2009, 14, 474-479.

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