Next Article in Journal
Reaction of Nitrilimines with 2-Substituted Aza-heterocycles. Synthesis of Pyrrolo[1,2-a]pyridine and Pyrimido[2,1-d]1,2,3,5- tetrazine
Next Article in Special Issue
Synthesis and Characterization of (Z)-5-Arylmethylidene-rhodanines with Photosynthesis-Inhibiting Properties
Previous Article in Journal
Preparation of Second Generation Ionic Liquids by Efficient Solvent-Free Alkylation of N-Heterocycles with Chloroalkanes
Previous Article in Special Issue
Substitutions of Fluorine Atoms and Phenoxy Groups in the Synthesis of Quinoxaline 1,4-di-N-oxide Derivatives
Molecules 2008, 13(1), 157-169; doi:10.3390/molecules13010157
Article

The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation

1,*  and 2
Received: 26 December 2007; in revised form: 21 January 2008 / Accepted: 22 January 2008 / Published: 25 January 2008
(This article belongs to the Special Issue ECSOC-11)
Download PDF [89 KB, uploaded 18 June 2014]
Abstract: Unsubstituted cyclic imides were synthesized from a series of cyclic anhydrides,hydroxylamine hydrochloride (NH2OH·HCl), and 4-N,N-dimethylamino-pyridine (DMAP,base catalyst) under microwave irradiation in monomode and multimode microwaves. Thisnovel microwave synthesis produced high yields of the unsubstituted cyclic imides forboth the monomode (61 - 81%) and multimode (84 - 97%) microwaves.
Keywords: Hydroxylamine·HCl; unsubstituted cyclic imides; DMAP; microwaves. Hydroxylamine·HCl; unsubstituted cyclic imides; DMAP; microwaves.
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Export to BibTeX |
EndNote


MDPI and ACS Style

Benjamin, E.; Hijji, Y. The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation. Molecules 2008, 13, 157-169.

AMA Style

Benjamin E, Hijji Y. The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation. Molecules. 2008; 13(1):157-169.

Chicago/Turabian Style

Benjamin, Ellis; Hijji, Yousef. 2008. "The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation." Molecules 13, no. 1: 157-169.


Molecules EISSN 1420-3049 Published by MDPI AG, Basel, Switzerland RSS E-Mail Table of Contents Alert