Molecules 2008, 13(1), 157-169; doi:10.3390/molecules13010157
Article

The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation

Received: 26 December 2007; in revised form: 21 January 2008 / Accepted: 22 January 2008 / Published: 25 January 2008
(This article belongs to the Special Issue ECSOC-11)
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Abstract: Unsubstituted cyclic imides were synthesized from a series of cyclic anhydrides,hydroxylamine hydrochloride (NH2OH·HCl), and 4-N,N-dimethylamino-pyridine (DMAP,base catalyst) under microwave irradiation in monomode and multimode microwaves. Thisnovel microwave synthesis produced high yields of the unsubstituted cyclic imides forboth the monomode (61 - 81%) and multimode (84 - 97%) microwaves.
Keywords: Hydroxylamine·HCl; unsubstituted cyclic imides; DMAP; microwaves.
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MDPI and ACS Style

Benjamin, E.; Hijji, Y. The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation. Molecules 2008, 13, 157-169.

AMA Style

Benjamin E, Hijji Y. The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation. Molecules. 2008; 13(1):157-169.

Chicago/Turabian Style

Benjamin, Ellis; Hijji, Yousef. 2008. "The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation." Molecules 13, no. 1: 157-169.

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