Molecules 2006, 11(12), 953-958; doi:10.3390/11120953
Communication

Synthesis and Characterization of Dimethacrylate Monomer with High Molecular Weight for Root Canal Filling Materials

1,* email, 1email, 2email, 2email and 1email
Received: 18 November 2006; in revised form: 4 December 2006 / Accepted: 4 December 2006 / Published: 7 December 2006
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Abstract: A new dimethacrylate monomer 9,9'-bis[4-(2'-hydroxy-3'-methacryloyloxy-propoxy)phenyl] fluorene (3) with a molecular weight of 634 was synthesized in 51.4%yield by addition of a glycidyl ether group to 9,9'-bis(4-hydroxyphenyl) fluorene (1) bythe reaction of compound 1 with epichlorohydrin, and then introducing the methacrylatemoiety by the reaction of the epoxy group with methacrylic acid. The structure ofmonomer 3 was confirmed by FT-IR, 1H-NMR, mass spectra and elemental analysis.
Keywords: Dimethacrylates; high molecular weight; synthesis; characterization.
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MDPI and ACS Style

Liu, F.; He, J.-W.; Lin, Z.-M.; Ling, J.-Q.; Jia, D.-M. Synthesis and Characterization of Dimethacrylate Monomer with High Molecular Weight for Root Canal Filling Materials. Molecules 2006, 11, 953-958.

AMA Style

Liu F, He J-W, Lin Z-M, Ling J-Q, Jia D-M. Synthesis and Characterization of Dimethacrylate Monomer with High Molecular Weight for Root Canal Filling Materials. Molecules. 2006; 11(12):953-958.

Chicago/Turabian Style

Liu, Fang; He, Jing-wie; Lin, Zheng-mei; Ling, Jun-qi; Jia, De-min. 2006. "Synthesis and Characterization of Dimethacrylate Monomer with High Molecular Weight for Root Canal Filling Materials." Molecules 11, no. 12: 953-958.

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